New Insights on the Morphology of Nanocomposite Prepared by In Situ Emulsion Polymerization
In order to better understand the morphology and properties of polymer nanocomposites it is necessary to conduct their characterization by Transmission Electron Microscopy (TEM). This work shows a technique through which the nanocomposite powder is mixed with a resin, and after cured, thin sections...
Gespeichert in:
| Veröffentlicht in: | Applied Mechanics and Materials 2015-07, Vol.775 (Engineering Solutions for Industrial Production), p.170-175 |
|---|---|
| Hauptverfasser: | , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 175 |
|---|---|
| container_issue | Engineering Solutions for Industrial Production |
| container_start_page | 170 |
| container_title | Applied Mechanics and Materials |
| container_volume | 775 |
| creator | Lona, Liliane Maria Ferrareso Contant, Sheila do Nascimento, Nayra Reis Neto, J.C. de Macêdo Neto, João Evangelista |
| description | In order to better understand the morphology and properties of polymer nanocomposites it is necessary to conduct their characterization by Transmission Electron Microscopy (TEM). This work shows a technique through which the nanocomposite powder is mixed with a resin, and after cured, thin sections can be obtained by ultramicrotomy. Another technique presented in this work deals with the observation of clay powder in solution. In this work High Resolution Electron Microscopy (HRTEM) was used to obtain images of the nanocomposites and clay. Images with a high level of details were showed. Through the use of such techniques, it was possible to observe two types of clay morphology in polymer matrix and its distribution. The dimensions and hexagonal layers of the natural clay used as nanofiller for the nanocomposite were also observed. The X-ray Diffraction (XRD) was used to investigate the kaolinite and nanocomposite. |
| doi_str_mv | 10.4028/www.scientific.net/AMM.775.170 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1718973001</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>3748348221</sourcerecordid><originalsourceid>FETCH-LOGICAL-c1730-d810fe6d887ceae6a2f360844b0f1151c1a752340e832ef47184f0a8baeb5aab3</originalsourceid><addsrcrecordid>eNqNkU1r3DAQhkU_oEma_yAolF7sSJYsyZfSEJImkE0CbU89CFk7yirYlivJLJtfX6VbaOgpp2GY92PgQegjJTUnjTrZbrd1sh6m7J239QT55HS1qqVsayrJK3RAhWgqyVXzGh13UjHCFGt51_E3f26k6hgT79BhSg-ECE65OkA_b2CLr6bk7zc54TDhvAG8CnHehCHc73Bw-MZMwYZxDslnwHcRZhNhjftd8eFvPi_4fFyG5Iv5Lgy7EaJ_NLms79FbZ4YEx3_nEfpxcf797LK6vv16dXZ6XVkqGanWihIHYq2UtGBAmMYxQRTnPXGUttRSI9uGcQKKNeC4pIo7YlRvoG-N6dkR-rTPnWP4tUDKevTJwjCYCcKSNC2OrjQRWqQf_pM-hCVO5TtNRSd5w0T3pPq8V9kYUorg9Bz9aOJOU6KfWOjCQv9joQsLXVjowqK0kRLwZR-Qo5lSBrt51vOyiN_FBJj-</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1697423691</pqid></control><display><type>article</type><title>New Insights on the Morphology of Nanocomposite Prepared by In Situ Emulsion Polymerization</title><source>Scientific.net Journals</source><creator>Lona, Liliane Maria Ferrareso ; Contant, Sheila ; do Nascimento, Nayra Reis ; Neto, J.C. de Macêdo ; Neto, João Evangelista</creator><creatorcontrib>Lona, Liliane Maria Ferrareso ; Contant, Sheila ; do Nascimento, Nayra Reis ; Neto, J.C. de Macêdo ; Neto, João Evangelista</creatorcontrib><description>In order to better understand the morphology and properties of polymer nanocomposites it is necessary to conduct their characterization by Transmission Electron Microscopy (TEM). This work shows a technique through which the nanocomposite powder is mixed with a resin, and after cured, thin sections can be obtained by ultramicrotomy. Another technique presented in this work deals with the observation of clay powder in solution. In this work High Resolution Electron Microscopy (HRTEM) was used to obtain images of the nanocomposites and clay. Images with a high level of details were showed. Through the use of such techniques, it was possible to observe two types of clay morphology in polymer matrix and its distribution. The dimensions and hexagonal layers of the natural clay used as nanofiller for the nanocomposite were also observed. The X-ray Diffraction (XRD) was used to investigate the kaolinite and nanocomposite.</description><identifier>ISSN: 1660-9336</identifier><identifier>ISSN: 1662-7482</identifier><identifier>ISBN: 9783038354994</identifier><identifier>ISBN: 3038354996</identifier><identifier>EISSN: 1662-7482</identifier><identifier>DOI: 10.4028/www.scientific.net/AMM.775.170</identifier><language>eng</language><publisher>Zurich: Trans Tech Publications Ltd</publisher><subject>Clay (material) ; Diffraction ; Morphology ; Nanostructure ; Transmission electron microscopy ; X-ray diffraction ; X-rays</subject><ispartof>Applied Mechanics and Materials, 2015-07, Vol.775 (Engineering Solutions for Industrial Production), p.170-175</ispartof><rights>2015 Trans Tech Publications Ltd</rights><rights>Copyright Trans Tech Publications Ltd. Jul 2015</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c1730-d810fe6d887ceae6a2f360844b0f1151c1a752340e832ef47184f0a8baeb5aab3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttps://www.scientific.net/Image/TitleCover/4058?width=600</thumbnail><link.rule.ids>314,780,784,27923,27924</link.rule.ids></links><search><creatorcontrib>Lona, Liliane Maria Ferrareso</creatorcontrib><creatorcontrib>Contant, Sheila</creatorcontrib><creatorcontrib>do Nascimento, Nayra Reis</creatorcontrib><creatorcontrib>Neto, J.C. de Macêdo</creatorcontrib><creatorcontrib>Neto, João Evangelista</creatorcontrib><title>New Insights on the Morphology of Nanocomposite Prepared by In Situ Emulsion Polymerization</title><title>Applied Mechanics and Materials</title><description>In order to better understand the morphology and properties of polymer nanocomposites it is necessary to conduct their characterization by Transmission Electron Microscopy (TEM). This work shows a technique through which the nanocomposite powder is mixed with a resin, and after cured, thin sections can be obtained by ultramicrotomy. Another technique presented in this work deals with the observation of clay powder in solution. In this work High Resolution Electron Microscopy (HRTEM) was used to obtain images of the nanocomposites and clay. Images with a high level of details were showed. Through the use of such techniques, it was possible to observe two types of clay morphology in polymer matrix and its distribution. The dimensions and hexagonal layers of the natural clay used as nanofiller for the nanocomposite were also observed. The X-ray Diffraction (XRD) was used to investigate the kaolinite and nanocomposite.</description><subject>Clay (material)</subject><subject>Diffraction</subject><subject>Morphology</subject><subject>Nanostructure</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><subject>X-rays</subject><issn>1660-9336</issn><issn>1662-7482</issn><issn>1662-7482</issn><isbn>9783038354994</isbn><isbn>3038354996</isbn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNqNkU1r3DAQhkU_oEma_yAolF7sSJYsyZfSEJImkE0CbU89CFk7yirYlivJLJtfX6VbaOgpp2GY92PgQegjJTUnjTrZbrd1sh6m7J239QT55HS1qqVsayrJK3RAhWgqyVXzGh13UjHCFGt51_E3f26k6hgT79BhSg-ECE65OkA_b2CLr6bk7zc54TDhvAG8CnHehCHc73Bw-MZMwYZxDslnwHcRZhNhjftd8eFvPi_4fFyG5Iv5Lgy7EaJ_NLms79FbZ4YEx3_nEfpxcf797LK6vv16dXZ6XVkqGanWihIHYq2UtGBAmMYxQRTnPXGUttRSI9uGcQKKNeC4pIo7YlRvoG-N6dkR-rTPnWP4tUDKevTJwjCYCcKSNC2OrjQRWqQf_pM-hCVO5TtNRSd5w0T3pPq8V9kYUorg9Bz9aOJOU6KfWOjCQv9joQsLXVjowqK0kRLwZR-Qo5lSBrt51vOyiN_FBJj-</recordid><startdate>20150701</startdate><enddate>20150701</enddate><creator>Lona, Liliane Maria Ferrareso</creator><creator>Contant, Sheila</creator><creator>do Nascimento, Nayra Reis</creator><creator>Neto, J.C. de Macêdo</creator><creator>Neto, João Evangelista</creator><general>Trans Tech Publications Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7TB</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BFMQW</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>KR7</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>7U5</scope><scope>L7M</scope></search><sort><creationdate>20150701</creationdate><title>New Insights on the Morphology of Nanocomposite Prepared by In Situ Emulsion Polymerization</title><author>Lona, Liliane Maria Ferrareso ; Contant, Sheila ; do Nascimento, Nayra Reis ; Neto, J.C. de Macêdo ; Neto, João Evangelista</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c1730-d810fe6d887ceae6a2f360844b0f1151c1a752340e832ef47184f0a8baeb5aab3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Clay (material)</topic><topic>Diffraction</topic><topic>Morphology</topic><topic>Nanostructure</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lona, Liliane Maria Ferrareso</creatorcontrib><creatorcontrib>Contant, Sheila</creatorcontrib><creatorcontrib>do Nascimento, Nayra Reis</creatorcontrib><creatorcontrib>Neto, J.C. de Macêdo</creatorcontrib><creatorcontrib>Neto, João Evangelista</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Continental Europe Database</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Civil Engineering Abstracts</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Applied Mechanics and Materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lona, Liliane Maria Ferrareso</au><au>Contant, Sheila</au><au>do Nascimento, Nayra Reis</au><au>Neto, J.C. de Macêdo</au><au>Neto, João Evangelista</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>New Insights on the Morphology of Nanocomposite Prepared by In Situ Emulsion Polymerization</atitle><jtitle>Applied Mechanics and Materials</jtitle><date>2015-07-01</date><risdate>2015</risdate><volume>775</volume><issue>Engineering Solutions for Industrial Production</issue><spage>170</spage><epage>175</epage><pages>170-175</pages><issn>1660-9336</issn><issn>1662-7482</issn><eissn>1662-7482</eissn><isbn>9783038354994</isbn><isbn>3038354996</isbn><abstract>In order to better understand the morphology and properties of polymer nanocomposites it is necessary to conduct their characterization by Transmission Electron Microscopy (TEM). This work shows a technique through which the nanocomposite powder is mixed with a resin, and after cured, thin sections can be obtained by ultramicrotomy. Another technique presented in this work deals with the observation of clay powder in solution. In this work High Resolution Electron Microscopy (HRTEM) was used to obtain images of the nanocomposites and clay. Images with a high level of details were showed. Through the use of such techniques, it was possible to observe two types of clay morphology in polymer matrix and its distribution. The dimensions and hexagonal layers of the natural clay used as nanofiller for the nanocomposite were also observed. The X-ray Diffraction (XRD) was used to investigate the kaolinite and nanocomposite.</abstract><cop>Zurich</cop><pub>Trans Tech Publications Ltd</pub><doi>10.4028/www.scientific.net/AMM.775.170</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1660-9336 |
| ispartof | Applied Mechanics and Materials, 2015-07, Vol.775 (Engineering Solutions for Industrial Production), p.170-175 |
| issn | 1660-9336 1662-7482 1662-7482 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1718973001 |
| source | Scientific.net Journals |
| subjects | Clay (material) Diffraction Morphology Nanostructure Transmission electron microscopy X-ray diffraction X-rays |
| title | New Insights on the Morphology of Nanocomposite Prepared by In Situ Emulsion Polymerization |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-08T09%3A19%3A00IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=New%20Insights%20on%20the%20Morphology%20of%20Nanocomposite%20Prepared%20by%20In%20Situ%20Emulsion%20Polymerization&rft.jtitle=Applied%20Mechanics%20and%20Materials&rft.au=Lona,%20Liliane%20Maria%20Ferrareso&rft.date=2015-07-01&rft.volume=775&rft.issue=Engineering%20Solutions%20for%20Industrial%20Production&rft.spage=170&rft.epage=175&rft.pages=170-175&rft.issn=1660-9336&rft.eissn=1662-7482&rft.isbn=9783038354994&rft.isbn_list=3038354996&rft_id=info:doi/10.4028/www.scientific.net/AMM.775.170&rft_dat=%3Cproquest_cross%3E3748348221%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1697423691&rft_id=info:pmid/&rfr_iscdi=true |