Preparation of ZnO thin films by MO-CVD using fibrous bis (acetylacetonato) zinc (II) and ozone

The fibrous bis (acetylacetonato) zinc (II) (Zn(C5H7O2)2·xH2O) was prepared with novel apparatus involved the vaporization and the recrystallization, and was investigated by differential thermal analysis (DTA), flourier transform infrared spectroscopy (FT-IR) with attenuated total reflection (ATR),...

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Veröffentlicht in:Journal of physics. Conference series 2013-03, Vol.417 (1), p.12059-6
Hauptverfasser: Haga, K, Abe, S, Takizawa, Y, Yubuta, K, Shishido, T
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container_issue 1
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container_title Journal of physics. Conference series
container_volume 417
creator Haga, K
Abe, S
Takizawa, Y
Yubuta, K
Shishido, T
description The fibrous bis (acetylacetonato) zinc (II) (Zn(C5H7O2)2·xH2O) was prepared with novel apparatus involved the vaporization and the recrystallization, and was investigated by differential thermal analysis (DTA), flourier transform infrared spectroscopy (FT-IR) with attenuated total reflection (ATR), and the inductively coupled plasma optical emission spectroscopy (ICP-OES). The zinc oxide (ZnO) films were prepared by the low-pressure CVD (LP-CVD) using the fibrous Zn(C5H7O2)2·xH2O and ozone(O3). The DTA curve of the fibrous material with a wide-ranging endothermic peak under 100°C according to desorption of the hydrated water separated to two peaks decreasing in the evaporation temperature. The resistivity of the ZnO films has changed widely from 104 to 108 Ωcm by the fibrous material with a different preparation condition.
doi_str_mv 10.1088/1742-6596/417/1/012059
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source IOP Publishing Free Content; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; IOPscience extra; Alma/SFX Local Collection; Free Full-Text Journals in Chemistry
subjects Chemical vapor deposition
Differential thermal analysis
Endothermic reactions
Inductively coupled plasma
Infrared analysis
Infrared spectroscopy
Low pressure
Molybdenum
Optical emission spectroscopy
Ozone
Physics
Recrystallization
Spectrum analysis
Thin films
Vaporization
Zinc
Zinc oxide
Zinc oxides
title Preparation of ZnO thin films by MO-CVD using fibrous bis (acetylacetonato) zinc (II) and ozone
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