Introduction of solid-phase microextraction as a high-throughput sample preparation tool in laboratory analysis of prohibited substances

•Thin-film SPME–LC–MS protocol offers fully quantitative analysis.•110 doping substances and metabolites were quantified.•C18 coating facilitated extraction of compounds with a wide range of polarities.•Automated 96-blade system allows high-throughput sample preparation.•Sample preparation time was...

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Veröffentlicht in:	Analytica chimica acta 2014-01, Vol.809, p.69-81
Hauptverfasser:	Boyacı, Ezel, Gorynski, Krzysztof, Rodriguez-Lafuente, Angel, Bojko, Barbara, Pawliszyn, Janusz
Format:	Artikel
Sprache:	eng
Schlagworte:	Adult Chromatography Chromatography, High Pressure Liquid Criteria Doping Doping in Sports Drugs Extraction Female High-Throughput Screening Assays - instrumentation Humans Liquids Male Mass Spectrometry Multiwell high throughput system Organic Chemicals - urine Quantitative analysis Quantitative determinations Solid phase microextraction Solid Phase Microextraction - instrumentation Substance Abuse Detection - instrumentation Substance Abuse Detection - methods
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