Functionalization of SLS parts for application as SERS substrates in chemical analysis: Preliminary results
Purpose - This paper aims to demonstrate the functionalization of polyamide parts made by selective laser sintering (SLS) for application as substrates for chemical analysis by surface-enhanced Raman scattering (SERS). Design/methodology/approach - Fabrication of Nylon 12 (Duraform PA®) samples usin...
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| Veröffentlicht in: | Rapid prototyping journal 2014-06, Vol.20 (4), p.280-284 |
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| creator | de Oliveira Setti, Grazielle Fernandes de Oliveira, Marcelo Alves Maia, Izaque Vicente Lopes da Silva, Jorge Joanni, Ednan |
| description | Purpose - This paper aims to demonstrate the functionalization of polyamide parts made by selective laser sintering (SLS) for application as substrates for chemical analysis by surface-enhanced Raman scattering (SERS). Design/methodology/approach - Fabrication of Nylon 12 (Duraform PA®) samples using two laser power levels and deposition of a layer of gold-coated zinc oxide nanostructures. Performance of these substrates in the detection of a known compound was tested by Raman spectroscopy. Findings - The hydrothermal synthesis proved to be a good method for functionalizing the surface of polyamide parts made by the SLS process. By varying the synthesis temperature, ZnO nanoparticles and nanorods attached to the sample surfaces could be obtained. The degree of sample sintering had an effect on the growth of the nanostructures. The gold-coated functionalized surfaces enhanced the Raman signal from crystal violet by more than three orders of magnitude. ZnO nanorods grown on well-sintered SLS parts showed the best performance from the set of samples tested in this work. Originality/value - ZnO nanostructures were grown directly on untreated surfaces of SLS-made polyamide. These substrates were used for chemical analysis by SERS. |
| doi_str_mv | 10.1108/RPJ-08-2012-0071 |
| format | Article |
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Design/methodology/approach - Fabrication of Nylon 12 (Duraform PA®) samples using two laser power levels and deposition of a layer of gold-coated zinc oxide nanostructures. Performance of these substrates in the detection of a known compound was tested by Raman spectroscopy. Findings - The hydrothermal synthesis proved to be a good method for functionalizing the surface of polyamide parts made by the SLS process. By varying the synthesis temperature, ZnO nanoparticles and nanorods attached to the sample surfaces could be obtained. The degree of sample sintering had an effect on the growth of the nanostructures. The gold-coated functionalized surfaces enhanced the Raman signal from crystal violet by more than three orders of magnitude. ZnO nanorods grown on well-sintered SLS parts showed the best performance from the set of samples tested in this work. Originality/value - ZnO nanostructures were grown directly on untreated surfaces of SLS-made polyamide. 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Design/methodology/approach - Fabrication of Nylon 12 (Duraform PA®) samples using two laser power levels and deposition of a layer of gold-coated zinc oxide nanostructures. Performance of these substrates in the detection of a known compound was tested by Raman spectroscopy. Findings - The hydrothermal synthesis proved to be a good method for functionalizing the surface of polyamide parts made by the SLS process. By varying the synthesis temperature, ZnO nanoparticles and nanorods attached to the sample surfaces could be obtained. The degree of sample sintering had an effect on the growth of the nanostructures. The gold-coated functionalized surfaces enhanced the Raman signal from crystal violet by more than three orders of magnitude. ZnO nanorods grown on well-sintered SLS parts showed the best performance from the set of samples tested in this work. Originality/value - ZnO nanostructures were grown directly on untreated surfaces of SLS-made polyamide. These substrates were used for chemical analysis by SERS.</description><subject>3-D printers</subject><subject>Additive manufacturing</subject><subject>Advantages</subject><subject>Analytical chemistry</subject><subject>Aqueous solutions</subject><subject>Chemical analysis</subject><subject>Gold</subject><subject>Lasers</subject><subject>Methods</subject><subject>Microscopy</subject><subject>Nanoparticles</subject><subject>Nanorods</subject><subject>Nanostructure</subject><subject>Nylon 12</subject><subject>Polyamide resins</subject><subject>Polymers</subject><subject>Power</subject><subject>Raman scattering</subject><subject>Rapid prototyping</subject><subject>Spectrum analysis</subject><subject>Synthesis</subject><subject>Temperature</subject><subject>Zinc oxide</subject><subject>Zinc oxides</subject><issn>1355-2546</issn><issn>1758-7670</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNpdkD1PwzAQhi0EEqWwM1piYTHYTs6OR1S1fKgSqAFWy3VskSpNgp0M5dfjqExM90r36L3Tg9A1o3eM0eJ-8_ZCaEE4ZZxQKtkJmjEJBZFC0tOUMwDCIRfn6CLGHU1YDnSGPldja4e6a01T_5gp4M7jcl3i3oQhYt8FbPq-qe1xaSIul5sSx3Ebh2AGF3HdYvvl9olosEk9h1jHS3TmTRPd1d-co4_V8n3xRNavj8-LhzWxHORApNkWOVQqZ-DBgap8xVwGtmCOAgAHy6Tc5opxL7ziyhjvqKqYVKaQPMuyObo99vah-x5dHPS-jtY1jWldN0bNJFUyZ-lIQm_-obtuDOnfRAnBRQ5CqkTRI2VDF2NwXveh3ptw0IzqSbROonUak2g9ic5-AedPb7w</recordid><startdate>20140610</startdate><enddate>20140610</enddate><creator>de Oliveira Setti, Grazielle</creator><creator>Fernandes de Oliveira, Marcelo</creator><creator>Alves Maia, Izaque</creator><creator>Vicente Lopes da Silva, Jorge</creator><creator>Joanni, Ednan</creator><general>Emerald Group Publishing Limited</general><scope>AAYXX</scope><scope>CITATION</scope><scope>0U~</scope><scope>1-H</scope><scope>7TB</scope><scope>7WY</scope><scope>7WZ</scope><scope>7XB</scope><scope>8AO</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FR3</scope><scope>F~G</scope><scope>HCIFZ</scope><scope>K6~</scope><scope>L.-</scope><scope>L.0</scope><scope>L6V</scope><scope>M0C</scope><scope>M7S</scope><scope>PQBIZ</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>Q9U</scope><scope>S0W</scope></search><sort><creationdate>20140610</creationdate><title>Functionalization of SLS parts for application as SERS substrates in chemical analysis</title><author>de Oliveira Setti, Grazielle ; 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Design/methodology/approach - Fabrication of Nylon 12 (Duraform PA®) samples using two laser power levels and deposition of a layer of gold-coated zinc oxide nanostructures. Performance of these substrates in the detection of a known compound was tested by Raman spectroscopy. Findings - The hydrothermal synthesis proved to be a good method for functionalizing the surface of polyamide parts made by the SLS process. By varying the synthesis temperature, ZnO nanoparticles and nanorods attached to the sample surfaces could be obtained. The degree of sample sintering had an effect on the growth of the nanostructures. The gold-coated functionalized surfaces enhanced the Raman signal from crystal violet by more than three orders of magnitude. ZnO nanorods grown on well-sintered SLS parts showed the best performance from the set of samples tested in this work. Originality/value - ZnO nanostructures were grown directly on untreated surfaces of SLS-made polyamide. 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| subjects | 3-D printers Additive manufacturing Advantages Analytical chemistry Aqueous solutions Chemical analysis Gold Lasers Methods Microscopy Nanoparticles Nanorods Nanostructure Nylon 12 Polyamide resins Polymers Power Raman scattering Rapid prototyping Spectrum analysis Synthesis Temperature Zinc oxide Zinc oxides |
| title | Functionalization of SLS parts for application as SERS substrates in chemical analysis: Preliminary results |
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