Making EBSD on water ice routine
Summary Electron backscatter diffraction (EBSD) on ice is a decade old. We have built upon previous work to select and develop methods of sample preparation and analysis that give >90% success rate in obtaining high‐quality EBSD maps, for the whole surface area (potentially) of low porosity (
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| Veröffentlicht in: | Journal of microscopy (Oxford) 2015-09, Vol.259 (3), p.237-256 |
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| container_title | Journal of microscopy (Oxford) |
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| creator | PRIOR, D.J. LILLY, K. SEIDEMANN, M. VAUGHAN, M. BECROFT, L. EASINGWOOD, R. DIEBOLD, S. OBBARD, R. DAGHLIAN, C. BAKER, I. CASWELL, T. GOLDING, N. GOLDSBY, D. DURHAM, W.B. PIAZOLO, S. WILSON, C.J.L. |
| description | Summary
Electron backscatter diffraction (EBSD) on ice is a decade old. We have built upon previous work to select and develop methods of sample preparation and analysis that give >90% success rate in obtaining high‐quality EBSD maps, for the whole surface area (potentially) of low porosity ( |
| doi_str_mv | 10.1111/jmi.12258 |
| format | Article |
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Electron backscatter diffraction (EBSD) on ice is a decade old. We have built upon previous work to select and develop methods of sample preparation and analysis that give >90% success rate in obtaining high‐quality EBSD maps, for the whole surface area (potentially) of low porosity (<15%) water ice samples, including very fine‐grained (<10 μm) and very large (up to 70 mm by 30 mm) samples. We present and explain two new methods of removing frost and providing a damage‐free surface for EBSD: pressure cycle sublimation and ‘ironing’. In general, the pressure cycle sublimation method is preferred as it is easier, faster and does not generate significant artefacts. We measure the thermal effects of sample preparation, transfer and storage procedures and model the likelihood of these modifying sample microstructures. We show results from laboratory ice samples, with a wide range of microstructures, to illustrate effectiveness and limitations of EBSD on ice and its potential applications. The methods we present can be implemented, with a modest investment, on any scanning electron microscope system with EBSD, a cryostage and a variable pressure capability.
Lay description
Electron backscatter diffraction (EBSD) provides a way generating quantitative microstructure: detailed maps of the distribution of crystal orientations. EBSD of ice is valuable in understanding how the microstructure of ice relates to its physical properties and in constraining the processes (deformation, grain growth, recrystallization, change of crystal form, etc.) that have generated the ice microstructures. EBSD of ice can help us understand terrestrial ice systems, ice on the moons of outer planets and ice in engineering and bioscience. We detail the methods of sample preparation and analysis that make EBSD on water ice samples, including very fine‐grained (<10 μm) and very large (up to 70 mm by 30 mm) samples, routine. We use experiments and modelling to ensure that warming during preparation has not modified sample microstructures significantly. We show EBSD results from laboratory ice samples, with a wide range of microstructures, to illustrate effectiveness and limitations of EBSD on ice and its potential applications.</description><identifier>ISSN: 0022-2720</identifier><identifier>EISSN: 1365-2818</identifier><identifier>DOI: 10.1111/jmi.12258</identifier><identifier>PMID: 25925223</identifier><identifier>CODEN: JMICAR</identifier><language>eng</language><publisher>England: Wiley Subscription Services, Inc</publisher><subject>Cryo‐SEM ; EBSD ; Ice</subject><ispartof>Journal of microscopy (Oxford), 2015-09, Vol.259 (3), p.237-256</ispartof><rights>2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society</rights><rights>2015 The Authors Journal of Microscopy © 2015 Royal Microscopical Society.</rights><rights>Journal compilation © 2015 Royal Microscopical Society</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c5248-54d92758960942853a87954eb11dd177d9be661f6a326c1aad18add7638f609a3</citedby><cites>FETCH-LOGICAL-c5248-54d92758960942853a87954eb11dd177d9be661f6a326c1aad18add7638f609a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1111%2Fjmi.12258$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1111%2Fjmi.12258$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,1427,27903,27904,45553,45554,46387,46811</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25925223$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>PRIOR, D.J.</creatorcontrib><creatorcontrib>LILLY, K.</creatorcontrib><creatorcontrib>SEIDEMANN, M.</creatorcontrib><creatorcontrib>VAUGHAN, M.</creatorcontrib><creatorcontrib>BECROFT, L.</creatorcontrib><creatorcontrib>EASINGWOOD, R.</creatorcontrib><creatorcontrib>DIEBOLD, S.</creatorcontrib><creatorcontrib>OBBARD, R.</creatorcontrib><creatorcontrib>DAGHLIAN, C.</creatorcontrib><creatorcontrib>BAKER, I.</creatorcontrib><creatorcontrib>CASWELL, T.</creatorcontrib><creatorcontrib>GOLDING, N.</creatorcontrib><creatorcontrib>GOLDSBY, D.</creatorcontrib><creatorcontrib>DURHAM, W.B.</creatorcontrib><creatorcontrib>PIAZOLO, S.</creatorcontrib><creatorcontrib>WILSON, C.J.L.</creatorcontrib><title>Making EBSD on water ice routine</title><title>Journal of microscopy (Oxford)</title><addtitle>J Microsc</addtitle><description>Summary
Electron backscatter diffraction (EBSD) on ice is a decade old. We have built upon previous work to select and develop methods of sample preparation and analysis that give >90% success rate in obtaining high‐quality EBSD maps, for the whole surface area (potentially) of low porosity (<15%) water ice samples, including very fine‐grained (<10 μm) and very large (up to 70 mm by 30 mm) samples. We present and explain two new methods of removing frost and providing a damage‐free surface for EBSD: pressure cycle sublimation and ‘ironing’. In general, the pressure cycle sublimation method is preferred as it is easier, faster and does not generate significant artefacts. We measure the thermal effects of sample preparation, transfer and storage procedures and model the likelihood of these modifying sample microstructures. We show results from laboratory ice samples, with a wide range of microstructures, to illustrate effectiveness and limitations of EBSD on ice and its potential applications. The methods we present can be implemented, with a modest investment, on any scanning electron microscope system with EBSD, a cryostage and a variable pressure capability.
Lay description
Electron backscatter diffraction (EBSD) provides a way generating quantitative microstructure: detailed maps of the distribution of crystal orientations. EBSD of ice is valuable in understanding how the microstructure of ice relates to its physical properties and in constraining the processes (deformation, grain growth, recrystallization, change of crystal form, etc.) that have generated the ice microstructures. EBSD of ice can help us understand terrestrial ice systems, ice on the moons of outer planets and ice in engineering and bioscience. We detail the methods of sample preparation and analysis that make EBSD on water ice samples, including very fine‐grained (<10 μm) and very large (up to 70 mm by 30 mm) samples, routine. We use experiments and modelling to ensure that warming during preparation has not modified sample microstructures significantly. We show EBSD results from laboratory ice samples, with a wide range of microstructures, to illustrate effectiveness and limitations of EBSD on ice and its potential applications.</description><subject>Cryo‐SEM</subject><subject>EBSD</subject><subject>Ice</subject><issn>0022-2720</issn><issn>1365-2818</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNp10D1PwzAQBmALgWgpDPwBFIkFhrT2Of7ICKVAUSsGYLbc2EEu-Sh2o6r_npQUBiRuueW5V6cXoXOCh6Sd0bJ0QwLA5AHqE8pZDJLIQ9THGCAGAbiHTkJYYowlk_gY9YClwABoH0Vz_eGq92hy-3IX1VW00WvrI5fZyNfN2lX2FB3lugj2bL8H6O1-8jp-jGfPD9PxzSzOGCQyZolJQTCZcpwmIBnVUqQssQtCjCFCmHRhOSc51xR4RrQ2RGpjBKcyb080HaCrLnfl68_GhrUqXchsUejK1k1QRGCWCM4lbunlH7qsG1-13-1UQhlP-E5ddyrzdQje5mrlXan9VhGsdrWptjb1XVtrL_aJzaK05lf-9NSCUQc2rrDb_5PU03zaRX4BR31x9g</recordid><startdate>201509</startdate><enddate>201509</enddate><creator>PRIOR, D.J.</creator><creator>LILLY, K.</creator><creator>SEIDEMANN, M.</creator><creator>VAUGHAN, M.</creator><creator>BECROFT, L.</creator><creator>EASINGWOOD, R.</creator><creator>DIEBOLD, S.</creator><creator>OBBARD, R.</creator><creator>DAGHLIAN, C.</creator><creator>BAKER, I.</creator><creator>CASWELL, T.</creator><creator>GOLDING, N.</creator><creator>GOLDSBY, D.</creator><creator>DURHAM, W.B.</creator><creator>PIAZOLO, S.</creator><creator>WILSON, C.J.L.</creator><general>Wiley Subscription Services, Inc</general><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>7X8</scope></search><sort><creationdate>201509</creationdate><title>Making EBSD on water ice routine</title><author>PRIOR, D.J. ; LILLY, K. ; SEIDEMANN, M. ; VAUGHAN, M. ; BECROFT, L. ; EASINGWOOD, R. ; DIEBOLD, S. ; OBBARD, R. ; DAGHLIAN, C. ; BAKER, I. ; CASWELL, T. ; GOLDING, N. ; GOLDSBY, D. ; DURHAM, W.B. ; PIAZOLO, S. ; WILSON, C.J.L.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c5248-54d92758960942853a87954eb11dd177d9be661f6a326c1aad18add7638f609a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>Cryo‐SEM</topic><topic>EBSD</topic><topic>Ice</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>PRIOR, D.J.</creatorcontrib><creatorcontrib>LILLY, K.</creatorcontrib><creatorcontrib>SEIDEMANN, M.</creatorcontrib><creatorcontrib>VAUGHAN, M.</creatorcontrib><creatorcontrib>BECROFT, L.</creatorcontrib><creatorcontrib>EASINGWOOD, R.</creatorcontrib><creatorcontrib>DIEBOLD, S.</creatorcontrib><creatorcontrib>OBBARD, R.</creatorcontrib><creatorcontrib>DAGHLIAN, C.</creatorcontrib><creatorcontrib>BAKER, I.</creatorcontrib><creatorcontrib>CASWELL, T.</creatorcontrib><creatorcontrib>GOLDING, N.</creatorcontrib><creatorcontrib>GOLDSBY, D.</creatorcontrib><creatorcontrib>DURHAM, W.B.</creatorcontrib><creatorcontrib>PIAZOLO, S.</creatorcontrib><creatorcontrib>WILSON, C.J.L.</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of microscopy (Oxford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>PRIOR, D.J.</au><au>LILLY, K.</au><au>SEIDEMANN, M.</au><au>VAUGHAN, M.</au><au>BECROFT, L.</au><au>EASINGWOOD, R.</au><au>DIEBOLD, S.</au><au>OBBARD, R.</au><au>DAGHLIAN, C.</au><au>BAKER, I.</au><au>CASWELL, T.</au><au>GOLDING, N.</au><au>GOLDSBY, D.</au><au>DURHAM, W.B.</au><au>PIAZOLO, S.</au><au>WILSON, C.J.L.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Making EBSD on water ice routine</atitle><jtitle>Journal of microscopy (Oxford)</jtitle><addtitle>J Microsc</addtitle><date>2015-09</date><risdate>2015</risdate><volume>259</volume><issue>3</issue><spage>237</spage><epage>256</epage><pages>237-256</pages><issn>0022-2720</issn><eissn>1365-2818</eissn><coden>JMICAR</coden><abstract>Summary
Electron backscatter diffraction (EBSD) on ice is a decade old. We have built upon previous work to select and develop methods of sample preparation and analysis that give >90% success rate in obtaining high‐quality EBSD maps, for the whole surface area (potentially) of low porosity (<15%) water ice samples, including very fine‐grained (<10 μm) and very large (up to 70 mm by 30 mm) samples. We present and explain two new methods of removing frost and providing a damage‐free surface for EBSD: pressure cycle sublimation and ‘ironing’. In general, the pressure cycle sublimation method is preferred as it is easier, faster and does not generate significant artefacts. We measure the thermal effects of sample preparation, transfer and storage procedures and model the likelihood of these modifying sample microstructures. We show results from laboratory ice samples, with a wide range of microstructures, to illustrate effectiveness and limitations of EBSD on ice and its potential applications. The methods we present can be implemented, with a modest investment, on any scanning electron microscope system with EBSD, a cryostage and a variable pressure capability.
Lay description
Electron backscatter diffraction (EBSD) provides a way generating quantitative microstructure: detailed maps of the distribution of crystal orientations. EBSD of ice is valuable in understanding how the microstructure of ice relates to its physical properties and in constraining the processes (deformation, grain growth, recrystallization, change of crystal form, etc.) that have generated the ice microstructures. EBSD of ice can help us understand terrestrial ice systems, ice on the moons of outer planets and ice in engineering and bioscience. We detail the methods of sample preparation and analysis that make EBSD on water ice samples, including very fine‐grained (<10 μm) and very large (up to 70 mm by 30 mm) samples, routine. We use experiments and modelling to ensure that warming during preparation has not modified sample microstructures significantly. We show EBSD results from laboratory ice samples, with a wide range of microstructures, to illustrate effectiveness and limitations of EBSD on ice and its potential applications.</abstract><cop>England</cop><pub>Wiley Subscription Services, Inc</pub><pmid>25925223</pmid><doi>10.1111/jmi.12258</doi><tpages>20</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Cryo‐SEM EBSD Ice |
| title | Making EBSD on water ice routine |
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