Analysis of the monosaccharide composition of water-soluble polysaccharides from Sargassum fusiforme by high performance liquid chromatography/electrospray ionisation mass spectrometry

•A precolumn derivatization LC/ESI–MS method was established for the analysis of polysaccharides in Sargassum fusiforme.•The optimisation of the pre-column derivatization process was studied.•Six monosaccharides from S. fusiforme polysaccharide were tentatively identified. Sargassum fusiforme (hijik...

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Veröffentlicht in:	Food chemistry 2014-02, Vol.145, p.976-983
Hauptverfasser:	Wu, Xiaodan, Jiang, Wei, Lu, Jiajia, Yu, Ying, Wu, Bin
Format:	Artikel
Sprache:	eng
Schlagworte:	Algae Analytic Sample Preparation Methods Antipyrine - analogs & derivatives Antipyrine - chemistry Biological and medical sciences Calibration China Chromatography, High Pressure Liquid Chromatography, Reverse-Phase Dietary Carbohydrates - analysis Edaravone Food Analysis - methods Food toxicology Functional Food - analysis HPLC–ESI–MS Hydrolysis Indicators and Reagents - chemistry Limit of Detection Medical sciences Molecular Structure Monosaccharide composition Monosaccharides - analysis Monosaccharides - chemistry Polysaccharides - chemistry Precolumn PMP derivatization Reproducibility of Results Sargassum - chemistry Sargassum fusiforme Seaweed - chemistry Spectrometry, Mass, Electrospray Ionization Tandem Mass Spectrometry Toxicology
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