Use of InSitu Atomic Force Microscopy to Follow Phase Changes at Crystal Surfaces in Real Time

Use of InSitu Atomic Force Microscopy to Follow Phase Changes at Crystal Surfaces in Real Time

AFM of cocrystals: Atomic force microscopy can be used to observe phase changes at crystal surfaces where the transformation is accompanied by a change in the spacing between layers of molecules. The conversion of a metastable polymorph of the caffeine-glutaric acid cocrystal into the thermodynamica...

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Veröffentlicht in:Angewandte Chemie International Edition 2013-09, Vol.52 (40), p.10541-10544
Hauptverfasser: Thakuria, Ranjit, Eddleston, Mark D, Chow, Ernest H H, Lloyd, Gareth O, Aldous, Barry J, Krzyzaniak, Joseph F, Bond, Andrew D, Jones, William
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Sprache:eng
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Atomic force microscopy
Conversion
Crystal surfaces
Phase transformations
Pictures
Real time
Transformations
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container_end_page 10544
container_issue 40
container_start_page 10541
container_title Angewandte Chemie International Edition
container_volume 52
creator Thakuria, Ranjit
Eddleston, Mark D
Chow, Ernest H H
Lloyd, Gareth O
Aldous, Barry J
Krzyzaniak, Joseph F
Bond, Andrew D
Jones, William
description AFM of cocrystals: Atomic force microscopy can be used to observe phase changes at crystal surfaces where the transformation is accompanied by a change in the spacing between layers of molecules. The conversion of a metastable polymorph of the caffeine-glutaric acid cocrystal into the thermodynamically stable form was analyzed continuously in situ using intermittent-contact-mode atomic force microscopy.
doi_str_mv 10.1002/anie.201302532
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source Wiley Online Library Journals Frontfile Complete
subjects Atomic force microscopy
Conversion
Crystal surfaces
Phase transformations
Pictures
Real time
Transformations
title Use of InSitu Atomic Force Microscopy to Follow Phase Changes at Crystal Surfaces in Real Time
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