The Liquidus Temperature of Nuclear Waste Glasses: An International Round-Robin Study
Eight institutions from four countries participated in a round‐robin study to determine the precision and bias of a liquidus temperature (TL) procedure for waste glasses being adopted by ASTM International as ASTM C 1720‐11. The participants of the round‐robin study were asked to measure three diffe...
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| Veröffentlicht in: | International Journal of Applied Glass Science, 2(4):321-333 2(4):321-333, 2011-12, Vol.2 (4), p.321-333 |
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| creator | Riley, Brian J. Hrma, Pavel R. Vienna, John D. Schweiger, Michael J. Rodriguez, Carmen P. Crum, Jarrod V. Lang, Jesse B. Marra, James C. Johnson, Fabienne C. Peeler, David K. Leonelli, Cristina Ferrari, Anna Maria Lancellotti, Isabella Dussossoy, Jean-Luc Hand, Russell J. Schofield, James M. Connelly, Andrew J. Short, Rick Harrison, Mike T. |
| description | Eight institutions from four countries participated in a round‐robin study to determine the precision and bias of a liquidus temperature (TL) procedure for waste glasses being adopted by ASTM International as ASTM C 1720‐11. The participants of the round‐robin study were asked to measure three different glasses with one or a combination of the following TL measurement methods: a gradient temperature (GT) method, a uniform temperature (UT) method, and/or a crystal fraction extrapolation (CF) method. The TL values reported by different institutions are generally consistent. The precision of TL measurements with each method was evaluated and is presented herein. The round‐robin glasses were all previously studied at Pacific Northwest National Laboratory and included ARG‐1 (Glass A), Zr‐9 (Glass B), and AmCm2‐19 (Glass C), with measured TL values spanning the temperature range of 960–1240°C. A precision (i.e., standard deviation) for TL has been obtained from the data, even though the data were not acquired for all three glasses using all three methods from each participating organization. Also, the article provides a brief overview and the importance of the TL measurement. |
| doi_str_mv | 10.1111/j.2041-1294.2011.00063.x |
| format | Article |
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(PNNL), Richland, WA (United States)</creatorcontrib><description>Eight institutions from four countries participated in a round‐robin study to determine the precision and bias of a liquidus temperature (TL) procedure for waste glasses being adopted by ASTM International as ASTM C 1720‐11. The participants of the round‐robin study were asked to measure three different glasses with one or a combination of the following TL measurement methods: a gradient temperature (GT) method, a uniform temperature (UT) method, and/or a crystal fraction extrapolation (CF) method. The TL values reported by different institutions are generally consistent. The precision of TL measurements with each method was evaluated and is presented herein. The round‐robin glasses were all previously studied at Pacific Northwest National Laboratory and included ARG‐1 (Glass A), Zr‐9 (Glass B), and AmCm2‐19 (Glass C), with measured TL values spanning the temperature range of 960–1240°C. A precision (i.e., standard deviation) for TL has been obtained from the data, even though the data were not acquired for all three glasses using all three methods from each participating organization. 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(PNNL), Richland, WA (United States)</creatorcontrib><title>The Liquidus Temperature of Nuclear Waste Glasses: An International Round-Robin Study</title><title>International Journal of Applied Glass Science, 2(4):321-333</title><addtitle>Int J Appl Glass Sci</addtitle><description>Eight institutions from four countries participated in a round‐robin study to determine the precision and bias of a liquidus temperature (TL) procedure for waste glasses being adopted by ASTM International as ASTM C 1720‐11. The participants of the round‐robin study were asked to measure three different glasses with one or a combination of the following TL measurement methods: a gradient temperature (GT) method, a uniform temperature (UT) method, and/or a crystal fraction extrapolation (CF) method. The TL values reported by different institutions are generally consistent. The precision of TL measurements with each method was evaluated and is presented herein. The round‐robin glasses were all previously studied at Pacific Northwest National Laboratory and included ARG‐1 (Glass A), Zr‐9 (Glass B), and AmCm2‐19 (Glass C), with measured TL values spanning the temperature range of 960–1240°C. A precision (i.e., standard deviation) for TL has been obtained from the data, even though the data were not acquired for all three glasses using all three methods from each participating organization. Also, the article provides a brief overview and the importance of the TL measurement.</description><subject>ASTM</subject><subject>Design of experiments</subject><subject>Extrapolation</subject><subject>Glass</subject><subject>Liquidus</subject><subject>liquidus temperature</subject><subject>Measurement methods</subject><subject>Northwest</subject><subject>round robin</subject><subject>Standard deviation</subject><subject>Zirconium</subject><issn>2041-1286</issn><issn>2041-1294</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqNkc1uEzEYRUcIJKrSd7BYsZngv_HYSCyiQkNQVKqQ0qXler5RHSZ2antE8vY4DMoWvPGVfI4X91YVInhGynm_nVHMSU2o4iURMsMYCzY7vKguzg8vz1mK19VVStsCYSalUPKiut88AVq559F1Y0Ib2O0hmjxGQKFHt6MdwET0YFIGtBhMSpA-oLlHS58hepNd8GZA6zD6rl6HR-fR9zx2xzfVq94MCa7-3pfV_c3nzfWXevVtsbyer2rLFWc1ZS1jVjHRt5Rj01vKSUtwxxpqhTDAWW85FZIq0ogGqHpsOi4bDl2vsO0Yu6zeTv-GlJ1O1mWwTzZ4DzZrgptW0qZA7yZoH8PzCCnrnUsWhsF4CGPSRCha6pCluX-imGCpBOe0oHJCbQwpRej1PrqdiccC6dM4eqtPvevTBvo0jv4zjj4U9eOk_nIDHP_b08uv80VJxa8n35VZDmffxJ9atKxt9MPtQt_9-LS-a4nSa_Yb-AOhaA</recordid><startdate>201112</startdate><enddate>201112</enddate><creator>Riley, Brian J.</creator><creator>Hrma, Pavel R.</creator><creator>Vienna, John D.</creator><creator>Schweiger, Michael J.</creator><creator>Rodriguez, Carmen P.</creator><creator>Crum, Jarrod V.</creator><creator>Lang, Jesse B.</creator><creator>Marra, James C.</creator><creator>Johnson, Fabienne C.</creator><creator>Peeler, David K.</creator><creator>Leonelli, Cristina</creator><creator>Ferrari, Anna Maria</creator><creator>Lancellotti, Isabella</creator><creator>Dussossoy, Jean-Luc</creator><creator>Hand, Russell J.</creator><creator>Schofield, James M.</creator><creator>Connelly, Andrew J.</creator><creator>Short, Rick</creator><creator>Harrison, Mike T.</creator><general>Blackwell Publishing Ltd</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>OTOTI</scope></search><sort><creationdate>201112</creationdate><title>The Liquidus Temperature of Nuclear Waste Glasses: An International Round-Robin Study</title><author>Riley, Brian J. ; Hrma, Pavel R. ; Vienna, John D. ; Schweiger, Michael J. ; Rodriguez, Carmen P. ; Crum, Jarrod V. ; Lang, Jesse B. ; Marra, James C. ; Johnson, Fabienne C. ; Peeler, David K. ; Leonelli, Cristina ; Ferrari, Anna Maria ; Lancellotti, Isabella ; Dussossoy, Jean-Luc ; Hand, Russell J. ; Schofield, James M. ; Connelly, Andrew J. ; Short, Rick ; Harrison, Mike T.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4943-23733c936f7240afc241710d352c66ae43fc4268291565e29b5d4854edf90cd33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>ASTM</topic><topic>Design of experiments</topic><topic>Extrapolation</topic><topic>Glass</topic><topic>Liquidus</topic><topic>liquidus temperature</topic><topic>Measurement methods</topic><topic>Northwest</topic><topic>round robin</topic><topic>Standard deviation</topic><topic>Zirconium</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Riley, Brian J.</creatorcontrib><creatorcontrib>Hrma, Pavel R.</creatorcontrib><creatorcontrib>Vienna, John D.</creatorcontrib><creatorcontrib>Schweiger, Michael J.</creatorcontrib><creatorcontrib>Rodriguez, Carmen P.</creatorcontrib><creatorcontrib>Crum, Jarrod V.</creatorcontrib><creatorcontrib>Lang, Jesse B.</creatorcontrib><creatorcontrib>Marra, James C.</creatorcontrib><creatorcontrib>Johnson, Fabienne C.</creatorcontrib><creatorcontrib>Peeler, David K.</creatorcontrib><creatorcontrib>Leonelli, Cristina</creatorcontrib><creatorcontrib>Ferrari, Anna Maria</creatorcontrib><creatorcontrib>Lancellotti, Isabella</creatorcontrib><creatorcontrib>Dussossoy, Jean-Luc</creatorcontrib><creatorcontrib>Hand, Russell J.</creatorcontrib><creatorcontrib>Schofield, James M.</creatorcontrib><creatorcontrib>Connelly, Andrew J.</creatorcontrib><creatorcontrib>Short, Rick</creatorcontrib><creatorcontrib>Harrison, Mike T.</creatorcontrib><creatorcontrib>Pacific Northwest National Lab. 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(PNNL), Richland, WA (United States)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The Liquidus Temperature of Nuclear Waste Glasses: An International Round-Robin Study</atitle><jtitle>International Journal of Applied Glass Science, 2(4):321-333</jtitle><addtitle>Int J Appl Glass Sci</addtitle><date>2011-12</date><risdate>2011</risdate><volume>2</volume><issue>4</issue><spage>321</spage><epage>333</epage><pages>321-333</pages><issn>2041-1286</issn><eissn>2041-1294</eissn><abstract>Eight institutions from four countries participated in a round‐robin study to determine the precision and bias of a liquidus temperature (TL) procedure for waste glasses being adopted by ASTM International as ASTM C 1720‐11. The participants of the round‐robin study were asked to measure three different glasses with one or a combination of the following TL measurement methods: a gradient temperature (GT) method, a uniform temperature (UT) method, and/or a crystal fraction extrapolation (CF) method. The TL values reported by different institutions are generally consistent. The precision of TL measurements with each method was evaluated and is presented herein. The round‐robin glasses were all previously studied at Pacific Northwest National Laboratory and included ARG‐1 (Glass A), Zr‐9 (Glass B), and AmCm2‐19 (Glass C), with measured TL values spanning the temperature range of 960–1240°C. A precision (i.e., standard deviation) for TL has been obtained from the data, even though the data were not acquired for all three glasses using all three methods from each participating organization. Also, the article provides a brief overview and the importance of the TL measurement.</abstract><cop>United States</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1111/j.2041-1294.2011.00063.x</doi><tpages>13</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | ASTM Design of experiments Extrapolation Glass Liquidus liquidus temperature Measurement methods Northwest round robin Standard deviation Zirconium |
| title | The Liquidus Temperature of Nuclear Waste Glasses: An International Round-Robin Study |
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