Densification behavior and related phenomena of spark plasma sintered boron carbide
In this work, boron carbide ceramics were sintered in the temperature range of 1400–1600°C by spark plasma sintering (SPS). The influence of sintering temperature, heating rate, and holding time on the microstructure, densification process and physical property was studied. The heating rate was foun...
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| Veröffentlicht in: | Ceramics international 2014-04, Vol.40 (3), p.4359-4366 |
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| container_title | Ceramics international |
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| creator | Li, Xiaoguang Jiang, Dongliang Zhang, Jingxian Lin, Qingling Chen, Zhongming Huang, Zhengren |
| description | In this work, boron carbide ceramics were sintered in the temperature range of 1400–1600°C by spark plasma sintering (SPS). The influence of sintering temperature, heating rate, and holding time on the microstructure, densification process and physical property was studied. The heating rate was found to have greater influence than that of the holding time on the microstructure and the densification of boron carbide. The optimal sintering temperature was 1600°C under the heating rate higher than 100°C/min. The relative density, flexural strength, Vickers hardness and fracture toughness of the sample synthesized at 1600°C were 98.33%, 828MPa, 31GPa and 2.66±0.29MPam1/2, respectively. The densification mechanism was also investigated. |
| doi_str_mv | 10.1016/j.ceramint.2013.08.106 |
| format | Article |
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The influence of sintering temperature, heating rate, and holding time on the microstructure, densification process and physical property was studied. The heating rate was found to have greater influence than that of the holding time on the microstructure and the densification of boron carbide. The optimal sintering temperature was 1600°C under the heating rate higher than 100°C/min. The relative density, flexural strength, Vickers hardness and fracture toughness of the sample synthesized at 1600°C were 98.33%, 828MPa, 31GPa and 2.66±0.29MPam1/2, respectively. The densification mechanism was also investigated.</description><identifier>ISSN: 0272-8842</identifier><identifier>EISSN: 1873-3956</identifier><identifier>DOI: 10.1016/j.ceramint.2013.08.106</identifier><language>eng</language><publisher>Elsevier Ltd</publisher><subject>Boron carbide ; Ceramics ; Densification ; Density ; Flexural strength ; Heating rate ; Microstructure ; Sintering ; Sintering behavior ; Spark plasma sintering ; TEM ; XRD</subject><ispartof>Ceramics international, 2014-04, Vol.40 (3), p.4359-4366</ispartof><rights>2013 Elsevier Ltd and Techna Group S.r.l.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c378t-56b588c6c073838d0d9494ca608f42cb0b6931bfe8b27ee1652a471e4c68c2453</citedby><cites>FETCH-LOGICAL-c378t-56b588c6c073838d0d9494ca608f42cb0b6931bfe8b27ee1652a471e4c68c2453</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.ceramint.2013.08.106$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Li, Xiaoguang</creatorcontrib><creatorcontrib>Jiang, Dongliang</creatorcontrib><creatorcontrib>Zhang, Jingxian</creatorcontrib><creatorcontrib>Lin, Qingling</creatorcontrib><creatorcontrib>Chen, Zhongming</creatorcontrib><creatorcontrib>Huang, Zhengren</creatorcontrib><title>Densification behavior and related phenomena of spark plasma sintered boron carbide</title><title>Ceramics international</title><description>In this work, boron carbide ceramics were sintered in the temperature range of 1400–1600°C by spark plasma sintering (SPS). The influence of sintering temperature, heating rate, and holding time on the microstructure, densification process and physical property was studied. The heating rate was found to have greater influence than that of the holding time on the microstructure and the densification of boron carbide. The optimal sintering temperature was 1600°C under the heating rate higher than 100°C/min. The relative density, flexural strength, Vickers hardness and fracture toughness of the sample synthesized at 1600°C were 98.33%, 828MPa, 31GPa and 2.66±0.29MPam1/2, respectively. The densification mechanism was also investigated.</description><subject>Boron carbide</subject><subject>Ceramics</subject><subject>Densification</subject><subject>Density</subject><subject>Flexural strength</subject><subject>Heating rate</subject><subject>Microstructure</subject><subject>Sintering</subject><subject>Sintering behavior</subject><subject>Spark plasma sintering</subject><subject>TEM</subject><subject>XRD</subject><issn>0272-8842</issn><issn>1873-3956</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqFkMtOwzAURC0EEqXwCyhLNil-xXZ2oPKUKrEA1pbj3KguiR3stBJ_j6vCuqsrjebM1QxC1wQvCCbidrOwEM3g_LSgmLAFVlkXJ2hGlGQlqytximaYSloqxek5ukhpgzNYczxD7w_gk-ucNZMLvmhgbXYuxML4tojQmwnaYlyDDwN4U4SuSKOJX8XYmzSYIuWnELOlCTHT1sTGtXCJzjrTJ7j6u3P0-fT4sXwpV2_Pr8v7VWmZVFNZiaZSygqLJVNMtbitec2tEVh1nNoGN6JmpOlANVQCEFFRwyUBboWylFdsjm4OuWMM31tIkx5cstD3xkPYJp0rUiYryehxa8UJ51JW-1RxsNoYUorQ6TG6wcQfTbDeD643-n9wvR9cY5V1kcG7Awi5885B1Mk68BZaF8FOug3uWMQvXbmM6A</recordid><startdate>20140401</startdate><enddate>20140401</enddate><creator>Li, Xiaoguang</creator><creator>Jiang, Dongliang</creator><creator>Zhang, Jingxian</creator><creator>Lin, Qingling</creator><creator>Chen, Zhongming</creator><creator>Huang, Zhengren</creator><general>Elsevier Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20140401</creationdate><title>Densification behavior and related phenomena of spark plasma sintered boron carbide</title><author>Li, Xiaoguang ; Jiang, Dongliang ; Zhang, Jingxian ; Lin, Qingling ; Chen, Zhongming ; Huang, Zhengren</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c378t-56b588c6c073838d0d9494ca608f42cb0b6931bfe8b27ee1652a471e4c68c2453</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Boron carbide</topic><topic>Ceramics</topic><topic>Densification</topic><topic>Density</topic><topic>Flexural strength</topic><topic>Heating rate</topic><topic>Microstructure</topic><topic>Sintering</topic><topic>Sintering behavior</topic><topic>Spark plasma sintering</topic><topic>TEM</topic><topic>XRD</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Li, Xiaoguang</creatorcontrib><creatorcontrib>Jiang, Dongliang</creatorcontrib><creatorcontrib>Zhang, Jingxian</creatorcontrib><creatorcontrib>Lin, Qingling</creatorcontrib><creatorcontrib>Chen, Zhongming</creatorcontrib><creatorcontrib>Huang, Zhengren</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Ceramics international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Li, Xiaoguang</au><au>Jiang, Dongliang</au><au>Zhang, Jingxian</au><au>Lin, Qingling</au><au>Chen, Zhongming</au><au>Huang, Zhengren</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Densification behavior and related phenomena of spark plasma sintered boron carbide</atitle><jtitle>Ceramics international</jtitle><date>2014-04-01</date><risdate>2014</risdate><volume>40</volume><issue>3</issue><spage>4359</spage><epage>4366</epage><pages>4359-4366</pages><issn>0272-8842</issn><eissn>1873-3956</eissn><abstract>In this work, boron carbide ceramics were sintered in the temperature range of 1400–1600°C by spark plasma sintering (SPS). The influence of sintering temperature, heating rate, and holding time on the microstructure, densification process and physical property was studied. The heating rate was found to have greater influence than that of the holding time on the microstructure and the densification of boron carbide. The optimal sintering temperature was 1600°C under the heating rate higher than 100°C/min. The relative density, flexural strength, Vickers hardness and fracture toughness of the sample synthesized at 1600°C were 98.33%, 828MPa, 31GPa and 2.66±0.29MPam1/2, respectively. The densification mechanism was also investigated.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.ceramint.2013.08.106</doi><tpages>8</tpages></addata></record> |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Boron carbide Ceramics Densification Density Flexural strength Heating rate Microstructure Sintering Sintering behavior Spark plasma sintering TEM XRD |
| title | Densification behavior and related phenomena of spark plasma sintered boron carbide |
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