Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition

Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition....

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Veröffentlicht in:Ceramics international 2013-12, Vol.39 (8), p.8797-8803
Hauptverfasser: Yaacob, Khatijah A., Riley, D. Jason
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description Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition. A colloidal suspension of TOPO-capped CdSe nanoparticles was prepared by the hot injection method, followed by ligand exchange to produce MUA-capped CdSe nanoparticles. As-prepared MUA-capped CdSe nanoparticles were washed using ethyl acetate and ethyl ether. Then, the washed nanoparticles were resuspended in ethanol and immediately used for EPD. A CdSe nanoparticle film measuring 2.75µm in thickness was deposited at an applied voltage of 5V and deposition time of 5min.
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subjects Cadmium selenides
Deposition
Electrophoretic deposition
Ethyl alcohol
Intermetallics
Ligand exchange
Mercaptoundeconic acid (MUA)-capped CdSe
Nanocomposites
Nanomaterials
Nanoparticles
Nanostructure
Trioctylphosphine oxide (TOPO)-capped CdSe
title Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition
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