Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition
Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition....
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Veröffentlicht in: | Ceramics international 2013-12, Vol.39 (8), p.8797-8803 |
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description | Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition. A colloidal suspension of TOPO-capped CdSe nanoparticles was prepared by the hot injection method, followed by ligand exchange to produce MUA-capped CdSe nanoparticles. As-prepared MUA-capped CdSe nanoparticles were washed using ethyl acetate and ethyl ether. Then, the washed nanoparticles were resuspended in ethanol and immediately used for EPD. A CdSe nanoparticle film measuring 2.75µm in thickness was deposited at an applied voltage of 5V and deposition time of 5min. |
doi_str_mv | 10.1016/j.ceramint.2013.04.067 |
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Jason</creator><creatorcontrib>Yaacob, Khatijah A. ; Riley, D. Jason</creatorcontrib><description>Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition. A colloidal suspension of TOPO-capped CdSe nanoparticles was prepared by the hot injection method, followed by ligand exchange to produce MUA-capped CdSe nanoparticles. As-prepared MUA-capped CdSe nanoparticles were washed using ethyl acetate and ethyl ether. Then, the washed nanoparticles were resuspended in ethanol and immediately used for EPD. A CdSe nanoparticle film measuring 2.75µm in thickness was deposited at an applied voltage of 5V and deposition time of 5min.</description><identifier>ISSN: 0272-8842</identifier><identifier>EISSN: 1873-3956</identifier><identifier>DOI: 10.1016/j.ceramint.2013.04.067</identifier><language>eng</language><publisher>Elsevier Ltd</publisher><subject>Cadmium selenides ; Deposition ; Electrophoretic deposition ; Ethyl alcohol ; Intermetallics ; Ligand exchange ; Mercaptoundeconic acid (MUA)-capped CdSe ; Nanocomposites ; Nanomaterials ; Nanoparticles ; Nanostructure ; Trioctylphosphine oxide (TOPO)-capped CdSe</subject><ispartof>Ceramics international, 2013-12, Vol.39 (8), p.8797-8803</ispartof><rights>2013 Elsevier Ltd and Techna Group S.r.l.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c378t-5b92835fcb6b43170d9edda8a63cf1f17279af3eeb5abec42671d1c925ff6ab13</citedby><cites>FETCH-LOGICAL-c378t-5b92835fcb6b43170d9edda8a63cf1f17279af3eeb5abec42671d1c925ff6ab13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.ceramint.2013.04.067$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Yaacob, Khatijah A.</creatorcontrib><creatorcontrib>Riley, D. Jason</creatorcontrib><title>Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition</title><title>Ceramics international</title><description>Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition. A colloidal suspension of TOPO-capped CdSe nanoparticles was prepared by the hot injection method, followed by ligand exchange to produce MUA-capped CdSe nanoparticles. As-prepared MUA-capped CdSe nanoparticles were washed using ethyl acetate and ethyl ether. Then, the washed nanoparticles were resuspended in ethanol and immediately used for EPD. A CdSe nanoparticle film measuring 2.75µm in thickness was deposited at an applied voltage of 5V and deposition time of 5min.</description><subject>Cadmium selenides</subject><subject>Deposition</subject><subject>Electrophoretic deposition</subject><subject>Ethyl alcohol</subject><subject>Intermetallics</subject><subject>Ligand exchange</subject><subject>Mercaptoundeconic acid (MUA)-capped CdSe</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Nanostructure</subject><subject>Trioctylphosphine oxide (TOPO)-capped CdSe</subject><issn>0272-8842</issn><issn>1873-3956</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqFkUlLBDEQhYMoOC5_QXLUQ7fZeslNGVdQPOicQzqpYIbuTpv0CPPvzTB69lRQ9d6DVx9CF5SUlND6el0aiHrw41wyQnlJREnq5gAtaNvwgsuqPkQLwhpWtK1gx-gkpTXJRinIArmHEAc9-zDi4PDr6hZfDhCNnuawGS2YMHqDtfH2qsjLCSxe3r0DHvUYJh1nb3rAzvdDwt0WQw9mjmH6DBHyCVuYQvK78DN05HSf4Px3nqLVw_3H8ql4eXt8Xt6-FIY37VxUnWQtr5zp6k5w2hArwVrd6pobRx1tWCO14wBdpTswgtUNtdRIVjlX647yU3S5z51i-NpAmtXgk4G-1yOETVK5NeOCSi7-lwopeCWFkFla76UmhpQiODVFP-i4VZSoHQO1Vn8M1I6BIkJlBtl4szdC7vztIapkPIwGrI_5VcoG_1_ED1qflRI</recordid><startdate>20131201</startdate><enddate>20131201</enddate><creator>Yaacob, Khatijah A.</creator><creator>Riley, D. Jason</creator><general>Elsevier Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20131201</creationdate><title>Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition</title><author>Yaacob, Khatijah A. ; Riley, D. Jason</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c378t-5b92835fcb6b43170d9edda8a63cf1f17279af3eeb5abec42671d1c925ff6ab13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Cadmium selenides</topic><topic>Deposition</topic><topic>Electrophoretic deposition</topic><topic>Ethyl alcohol</topic><topic>Intermetallics</topic><topic>Ligand exchange</topic><topic>Mercaptoundeconic acid (MUA)-capped CdSe</topic><topic>Nanocomposites</topic><topic>Nanomaterials</topic><topic>Nanoparticles</topic><topic>Nanostructure</topic><topic>Trioctylphosphine oxide (TOPO)-capped CdSe</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yaacob, Khatijah A.</creatorcontrib><creatorcontrib>Riley, D. Jason</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Ceramics international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yaacob, Khatijah A.</au><au>Riley, D. Jason</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition</atitle><jtitle>Ceramics international</jtitle><date>2013-12-01</date><risdate>2013</risdate><volume>39</volume><issue>8</issue><spage>8797</spage><epage>8803</epage><pages>8797-8803</pages><issn>0272-8842</issn><eissn>1873-3956</eissn><abstract>Electrophoretic deposition (EPD) has gained increasing interest for the deposition of materials such as TiO2, carbon nanotubes and trioctylphosphine oxide (TOPO)-capped CdSe nanoparticles. In this study, a mercaptoundecanoic acid (MUA) CdSe nanoparticle film was formed by electrophoretic deposition. A colloidal suspension of TOPO-capped CdSe nanoparticles was prepared by the hot injection method, followed by ligand exchange to produce MUA-capped CdSe nanoparticles. As-prepared MUA-capped CdSe nanoparticles were washed using ethyl acetate and ethyl ether. Then, the washed nanoparticles were resuspended in ethanol and immediately used for EPD. A CdSe nanoparticle film measuring 2.75µm in thickness was deposited at an applied voltage of 5V and deposition time of 5min.</abstract><pub>Elsevier Ltd</pub><doi>10.1016/j.ceramint.2013.04.067</doi><tpages>7</tpages></addata></record> |
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subjects | Cadmium selenides Deposition Electrophoretic deposition Ethyl alcohol Intermetallics Ligand exchange Mercaptoundeconic acid (MUA)-capped CdSe Nanocomposites Nanomaterials Nanoparticles Nanostructure Trioctylphosphine oxide (TOPO)-capped CdSe |
title | Formation of MUA (mercaptoundeconic acid)-capped CDSe nanoparticle films by electrophoretic deposition |
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