Plasma-Chemical Synthesis of Oxide Powders Using Transformer-Coupled Discharge
An experimental investigation of transformer-coupled discharge in an Ar-O2 mixture with the addition of SICl4, TiCl4 and ZrCl4 has been carried out under the atmospheric pressure of plasma-forming gases. Discharge power and discharge heat losses have been determined, and the dispersion and phase com...
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| Veröffentlicht in: | Plasma science & technology 2013-04, Vol.15 (4), p.386-390, Article 386 |
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| creator | Ulanov, I. M. Isupov, M. V. Litvinsev, A. Yu Mischenko, P. A. |
| description | An experimental investigation of transformer-coupled discharge in an Ar-O2 mixture with the addition of SICl4, TiCl4 and ZrCl4 has been carried out under the atmospheric pressure of plasma-forming gases. Discharge power and discharge heat losses have been determined, and the dispersion and phase composition of reaction products （oxide powders） has been analyzed with SEM and X-ray diffraction analysis. Investigations reveal the formation of ultrafine oxide powders in the case of vaporized chloride （SiCl4 and TiCl4） injecting into the transformer coupled discharge. In the case of fine powder （ZrCl4） injection, full oxidation was not observed and reaction products consisted of a mixture of ZrO2 and ZrOCl2. A conclusion has been made regarding the perspectives of using transformer-coupled discharge to produce ultrafine oxide powders. |
| doi_str_mv | 10.1088/1009-0630/15/4/14 |
| format | Article |
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M. ; Isupov, M. V. ; Litvinsev, A. Yu ; Mischenko, P. A.</creator><creatorcontrib>Ulanov, I. M. ; Isupov, M. V. ; Litvinsev, A. Yu ; Mischenko, P. A.</creatorcontrib><description>An experimental investigation of transformer-coupled discharge in an Ar-O2 mixture with the addition of SICl4, TiCl4 and ZrCl4 has been carried out under the atmospheric pressure of plasma-forming gases. Discharge power and discharge heat losses have been determined, and the dispersion and phase composition of reaction products （oxide powders） has been analyzed with SEM and X-ray diffraction analysis. Investigations reveal the formation of ultrafine oxide powders in the case of vaporized chloride （SiCl4 and TiCl4） injecting into the transformer coupled discharge. In the case of fine powder （ZrCl4） injection, full oxidation was not observed and reaction products consisted of a mixture of ZrO2 and ZrOCl2. 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M.</creatorcontrib><creatorcontrib>Isupov, M. V.</creatorcontrib><creatorcontrib>Litvinsev, A. Yu</creatorcontrib><creatorcontrib>Mischenko, P. A.</creatorcontrib><title>Plasma-Chemical Synthesis of Oxide Powders Using Transformer-Coupled Discharge</title><title>Plasma science & technology</title><addtitle>Plasma Science ＆ Technology</addtitle><description>An experimental investigation of transformer-coupled discharge in an Ar-O2 mixture with the addition of SICl4, TiCl4 and ZrCl4 has been carried out under the atmospheric pressure of plasma-forming gases. Discharge power and discharge heat losses have been determined, and the dispersion and phase composition of reaction products （oxide powders） has been analyzed with SEM and X-ray diffraction analysis. Investigations reveal the formation of ultrafine oxide powders in the case of vaporized chloride （SiCl4 and TiCl4） injecting into the transformer coupled discharge. In the case of fine powder （ZrCl4） injection, full oxidation was not observed and reaction products consisted of a mixture of ZrO2 and ZrOCl2. A conclusion has been made regarding the perspectives of using transformer-coupled discharge to produce ultrafine oxide powders.</description><subject>Atmospheric pressure</subject><subject>Chlorides</subject><subject>Diffraction</subject><subject>Discharge</subject><subject>Dispersions</subject><subject>Oxides</subject><subject>Reaction products</subject><subject>Transformers</subject><subject>X-射线衍射分析</subject><subject>Zirconium dioxide</subject><subject>化学合成</subject><subject>变压器耦合</subject><subject>四氯化硅</subject><subject>四氯化钛</subject><subject>放电等离子体</subject><subject>粉末</subject><subject>超细氧化物</subject><issn>1009-0630</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNp9kD1PwzAQhj2ARCn8ALawsYTYxI7tEYVPqaKVaGfLcS6NURK3dirovydRqw4MTHc6vc_d6UHohuB7goVICMYyxlmKE8ISmhB6hian2QW6DOELY0alSCfoY9Ho0Oo4r6G1RjfR577rawg2RK6K5j-2hGjhvkvwIVoF262jpdddqJxvwce5220aKKMnG0yt_Rqu0HmlmwDXxzpFq5fnZf4Wz-av7_njLDYppn0sOZcVAWp0kZlSc0MehJRgBAdJS14VmDBGizTjGS1BQ0bxODVs6AEzSKfo7rB34912B6FX7fACNI3uwO2CIplgXFIm-BAlh6jxLgQPldp422q_VwSr0Zca3ajRjSJMUUXowPA_jLG97q3req9t8y95eyRr1623g7DTOcqylDPG01-8pX14</recordid><startdate>20130401</startdate><enddate>20130401</enddate><creator>Ulanov, I. 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Investigations reveal the formation of ultrafine oxide powders in the case of vaporized chloride （SiCl4 and TiCl4） injecting into the transformer coupled discharge. In the case of fine powder （ZrCl4） injection, full oxidation was not observed and reaction products consisted of a mixture of ZrO2 and ZrOCl2. A conclusion has been made regarding the perspectives of using transformer-coupled discharge to produce ultrafine oxide powders.</abstract><doi>10.1088/1009-0630/15/4/14</doi><tpages>5</tpages></addata></record> |
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| source | Institute of Physics Journals |
| subjects | Atmospheric pressure Chlorides Diffraction Discharge Dispersions Oxides Reaction products Transformers X-射线衍射分析 Zirconium dioxide 化学合成 变压器耦合 四氯化硅 四氯化钛 放电等离子体 粉末 超细氧化物 |
| title | Plasma-Chemical Synthesis of Oxide Powders Using Transformer-Coupled Discharge |
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