Determination of succinate-dehydrogenase-inhibitor fungicide residues in fruits and vegetables by liquid chromatography–tandem mass spectrometry
In recent years, a second generation of succinate-dehydrogenase-inhibitor (SDHI) fungicides has been introduced into the market for effective treatment of fruit and vegetable crops, with fluxapyroxad, boscalid, fluopyram, penflufen, bixafen, penthiopyrad, and isopyrazam being some of the members of...
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| Veröffentlicht in: | Analytical and bioanalytical chemistry 2015-05, Vol.407 (14), p.4207-4211 |
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| creator | Abad-Fuentes, Antonio Ceballos-Alcantarilla, Eric Mercader, Josep V. Agulló, Consuelo Abad-Somovilla, Antonio Esteve-Turrillas, Francesc A. |
| description | In recent years, a second generation of succinate-dehydrogenase-inhibitor (SDHI) fungicides has been introduced into the market for effective treatment of fruit and vegetable crops, with fluxapyroxad, boscalid, fluopyram, penflufen, bixafen, penthiopyrad, and isopyrazam being some of the members of this new class of agrochemical. We herein report the development of an analytical procedure for the determination of residues of these SDHI fungicides in food samples, based on a modification of the QuEChERS extraction method followed by ultra-performance liquid chromatography coupled to tandem-mass-spectrometry determination. The proposed method reached limits of detection from 0.8 to 2.0 μg L
−1
. Apple, strawberry, tomato, and spinach samples were used as model samples. Spiked samples, from 10 to 1000 μg kg
−1
, were analysed by the proposed method and quantitative recoveries were obtained (from 81 to 115 % for apples, from 84 to 136 % for strawberries, from 84 to 135 % for tomatoes, and from 80 to 136 % for spinach), with precision better than 20 % in all cases. Thus, the proposed method can be used for the analysis of SDHI fungicide residues to efficiently ensure that marketed fruits and vegetables comply with the maximum residue levels established by competent authorities.
Graphical Abstract
Schematic representation of the proposed QuEChERS method using different dSPE supports |
| doi_str_mv | 10.1007/s00216-015-8608-3 |
| format | Article |
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−1
. Apple, strawberry, tomato, and spinach samples were used as model samples. Spiked samples, from 10 to 1000 μg kg
−1
, were analysed by the proposed method and quantitative recoveries were obtained (from 81 to 115 % for apples, from 84 to 136 % for strawberries, from 84 to 135 % for tomatoes, and from 80 to 136 % for spinach), with precision better than 20 % in all cases. Thus, the proposed method can be used for the analysis of SDHI fungicide residues to efficiently ensure that marketed fruits and vegetables comply with the maximum residue levels established by competent authorities.
Graphical Abstract
Schematic representation of the proposed QuEChERS method using different dSPE supports</description><identifier>ISSN: 1618-2642</identifier><identifier>EISSN: 1618-2650</identifier><identifier>DOI: 10.1007/s00216-015-8608-3</identifier><identifier>PMID: 25796526</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer Berlin Heidelberg</publisher><subject>Agrochemicals ; Analysis ; Analytical Chemistry ; Biochemistry ; Cereals ; Characterization and Evaluation of Materials ; Chemistry ; Chemistry and Materials Science ; Chromatography ; Chromatography, Liquid - methods ; Dehydrogenase ; Dehydrogenases ; Food ; Food Science ; Fruit ; Fruits ; Fungicides ; Fungicides, Industrial - chemistry ; Laboratory Medicine ; Liquid chromatography ; Mass spectrometry ; Monitoring/Environmental Analysis ; Pesticide Residues - chemistry ; Pesticides ; Residues ; Scientific imaging ; Spinach ; Strawberries ; Succinate Dehydrogenase - antagonists & inhibitors ; Tandem Mass Spectrometry - methods ; Tomatoes ; Vegetables</subject><ispartof>Analytical and bioanalytical chemistry, 2015-05, Vol.407 (14), p.4207-4211</ispartof><rights>Springer-Verlag Berlin Heidelberg 2015</rights><rights>COPYRIGHT 2015 Springer</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c654t-bddbeccf866bff9ee3014ffa0b8c929bc1d5387694cbb0eea288bfab68cf14a3</citedby><cites>FETCH-LOGICAL-c654t-bddbeccf866bff9ee3014ffa0b8c929bc1d5387694cbb0eea288bfab68cf14a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00216-015-8608-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00216-015-8608-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25796526$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Abad-Fuentes, Antonio</creatorcontrib><creatorcontrib>Ceballos-Alcantarilla, Eric</creatorcontrib><creatorcontrib>Mercader, Josep V.</creatorcontrib><creatorcontrib>Agulló, Consuelo</creatorcontrib><creatorcontrib>Abad-Somovilla, Antonio</creatorcontrib><creatorcontrib>Esteve-Turrillas, Francesc A.</creatorcontrib><title>Determination of succinate-dehydrogenase-inhibitor fungicide residues in fruits and vegetables by liquid chromatography–tandem mass spectrometry</title><title>Analytical and bioanalytical chemistry</title><addtitle>Anal Bioanal Chem</addtitle><addtitle>Anal Bioanal Chem</addtitle><description>In recent years, a second generation of succinate-dehydrogenase-inhibitor (SDHI) fungicides has been introduced into the market for effective treatment of fruit and vegetable crops, with fluxapyroxad, boscalid, fluopyram, penflufen, bixafen, penthiopyrad, and isopyrazam being some of the members of this new class of agrochemical. We herein report the development of an analytical procedure for the determination of residues of these SDHI fungicides in food samples, based on a modification of the QuEChERS extraction method followed by ultra-performance liquid chromatography coupled to tandem-mass-spectrometry determination. The proposed method reached limits of detection from 0.8 to 2.0 μg L
−1
. Apple, strawberry, tomato, and spinach samples were used as model samples. Spiked samples, from 10 to 1000 μg kg
−1
, were analysed by the proposed method and quantitative recoveries were obtained (from 81 to 115 % for apples, from 84 to 136 % for strawberries, from 84 to 135 % for tomatoes, and from 80 to 136 % for spinach), with precision better than 20 % in all cases. Thus, the proposed method can be used for the analysis of SDHI fungicide residues to efficiently ensure that marketed fruits and vegetables comply with the maximum residue levels established by competent authorities.
Graphical Abstract
Schematic representation of the proposed QuEChERS method using different dSPE supports</description><subject>Agrochemicals</subject><subject>Analysis</subject><subject>Analytical Chemistry</subject><subject>Biochemistry</subject><subject>Cereals</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Chromatography, Liquid - methods</subject><subject>Dehydrogenase</subject><subject>Dehydrogenases</subject><subject>Food</subject><subject>Food Science</subject><subject>Fruit</subject><subject>Fruits</subject><subject>Fungicides</subject><subject>Fungicides, Industrial - chemistry</subject><subject>Laboratory Medicine</subject><subject>Liquid chromatography</subject><subject>Mass spectrometry</subject><subject>Monitoring/Environmental Analysis</subject><subject>Pesticide Residues - chemistry</subject><subject>Pesticides</subject><subject>Residues</subject><subject>Scientific imaging</subject><subject>Spinach</subject><subject>Strawberries</subject><subject>Succinate Dehydrogenase - 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Academic</collection><jtitle>Analytical and bioanalytical chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Abad-Fuentes, Antonio</au><au>Ceballos-Alcantarilla, Eric</au><au>Mercader, Josep V.</au><au>Agulló, Consuelo</au><au>Abad-Somovilla, Antonio</au><au>Esteve-Turrillas, Francesc A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of succinate-dehydrogenase-inhibitor fungicide residues in fruits and vegetables by liquid chromatography–tandem mass spectrometry</atitle><jtitle>Analytical and bioanalytical chemistry</jtitle><stitle>Anal Bioanal Chem</stitle><addtitle>Anal Bioanal Chem</addtitle><date>2015-05-01</date><risdate>2015</risdate><volume>407</volume><issue>14</issue><spage>4207</spage><epage>4211</epage><pages>4207-4211</pages><issn>1618-2642</issn><eissn>1618-2650</eissn><abstract>In recent years, a second generation of succinate-dehydrogenase-inhibitor (SDHI) fungicides has been introduced into the market for effective treatment of fruit and vegetable crops, with fluxapyroxad, boscalid, fluopyram, penflufen, bixafen, penthiopyrad, and isopyrazam being some of the members of this new class of agrochemical. We herein report the development of an analytical procedure for the determination of residues of these SDHI fungicides in food samples, based on a modification of the QuEChERS extraction method followed by ultra-performance liquid chromatography coupled to tandem-mass-spectrometry determination. The proposed method reached limits of detection from 0.8 to 2.0 μg L
−1
. Apple, strawberry, tomato, and spinach samples were used as model samples. Spiked samples, from 10 to 1000 μg kg
−1
, were analysed by the proposed method and quantitative recoveries were obtained (from 81 to 115 % for apples, from 84 to 136 % for strawberries, from 84 to 135 % for tomatoes, and from 80 to 136 % for spinach), with precision better than 20 % in all cases. Thus, the proposed method can be used for the analysis of SDHI fungicide residues to efficiently ensure that marketed fruits and vegetables comply with the maximum residue levels established by competent authorities.
Graphical Abstract
Schematic representation of the proposed QuEChERS method using different dSPE supports</abstract><cop>Berlin/Heidelberg</cop><pub>Springer Berlin Heidelberg</pub><pmid>25796526</pmid><doi>10.1007/s00216-015-8608-3</doi><tpages>5</tpages></addata></record> |
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| ispartof | Analytical and bioanalytical chemistry, 2015-05, Vol.407 (14), p.4207-4211 |
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| subjects | Agrochemicals Analysis Analytical Chemistry Biochemistry Cereals Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Chromatography Chromatography, Liquid - methods Dehydrogenase Dehydrogenases Food Food Science Fruit Fruits Fungicides Fungicides, Industrial - chemistry Laboratory Medicine Liquid chromatography Mass spectrometry Monitoring/Environmental Analysis Pesticide Residues - chemistry Pesticides Residues Scientific imaging Spinach Strawberries Succinate Dehydrogenase - antagonists & inhibitors Tandem Mass Spectrometry - methods Tomatoes Vegetables |
| title | Determination of succinate-dehydrogenase-inhibitor fungicide residues in fruits and vegetables by liquid chromatography–tandem mass spectrometry |
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