Synthesis of Nano Calcium Phosphate via Biomimetic Method for Bone Tissue Engineering Scaffolds and Investigation of its Phase Transformation in Simulated Body Fluid
In this study the formation of calcium phosphate phase via double diffusion method into a hydrogel matrix was investigated and its phase transformation in simulated body fluid was studied. White precipitate was formed within the hydrogel, due to the diffusion of calcium and phosphate ions through th...
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| Veröffentlicht in: | Key engineering materials 2014-01, Vol.587, p.86-92 |
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| creator | Moztarzadeh, F. Shokrgozar, Mohammad A. Raz, Majid Tahriri, M. |
| description | In this study the formation of calcium phosphate phase via double diffusion method into a hydrogel matrix was investigated and its phase transformation in simulated body fluid was studied. White precipitate was formed within the hydrogel, due to the diffusion of calcium and phosphate ions through the hydrogel matrix in similar pH to human body. Phase composition, microstructure and structural groups in the composite samples were also characterized by X-Ray Diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infra-red (FTIR) analyses. Microstructure of precipitates formed within middle hydrogel, showed that detected materials are composed of carbonated hydroxyapatite and dicalcium phosphate dihydrate (DCPD, brushite). The particle size was about 10 nm .Analysis results showed that after incubation in simulated body fluid, dicalcium phosphate dehydrate phase transformed into crystalline hydroxy apatite. |
| doi_str_mv | 10.4028/www.scientific.net/KEM.587.86 |
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White precipitate was formed within the hydrogel, due to the diffusion of calcium and phosphate ions through the hydrogel matrix in similar pH to human body. Phase composition, microstructure and structural groups in the composite samples were also characterized by X-Ray Diffraction (XRD), scanning electron microscopy (SEM) and Fourier transform infra-red (FTIR) analyses. Microstructure of precipitates formed within middle hydrogel, showed that detected materials are composed of carbonated hydroxyapatite and dicalcium phosphate dihydrate (DCPD, brushite). 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The particle size was about 10 nm .Analysis results showed that after incubation in simulated body fluid, dicalcium phosphate dehydrate phase transformed into crystalline hydroxy apatite.</description><subject>Calcium phosphate</subject><subject>Diffusion</subject><subject>Fourier transforms</subject><subject>Hydrogels</subject><subject>Phase transformations</subject><subject>Precipitates</subject><subject>Precipitation</subject><subject>Scanning electron microscopy</subject><issn>1013-9826</issn><issn>1662-9795</issn><issn>1662-9795</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqNkcFu1DAQhiMEEqXwDr4gcdnUdhLHOSBEV1uoaAFpy9ly7PFmqsReYqerfSDeE68WiWtPM9L8_z-j-YriPaNlTbm8OhwOZTQIPqFDU3pIV98292Uj21KKF8UFE4KvurZrXuaesmrVSS5eF29ifKS0YpI1F8Wf7dGnASJGEhz5rn0gaz0aXCbycwhxP-gE5Ak1ucYw4QQJDbmHNARLXJjJdfBAHjDGBcjG79ADzOh3ZGu0c2G0kWhvya1_gphwpxMGf9qDKeZ4HbN31j7mpOk8Q0-2OC1j3mpzuD2Sm3FB-7Z45fQY4d2_eln8utk8rL-u7n58uV1_vluZSsi0klZ2IOre8L5lvYHaSdn2nWB9RaHtW224cX3TdayxjvKairqrLOc2T6mseHVZfDjn7ufwe8k3qwmjgXHUHsISFROtpKxtu_oZUk5pTRtZZenHs9TMIcYZnNrPOOn5qBhVJ5Iqk1T_SapMUmWSKpNUUmT_p7M_nZ6VwAzqMSyzz594ZsJfrrSymA</recordid><startdate>20140101</startdate><enddate>20140101</enddate><creator>Moztarzadeh, F.</creator><creator>Shokrgozar, Mohammad A.</creator><creator>Raz, Majid</creator><creator>Tahriri, M.</creator><general>Trans Tech Publications Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20140101</creationdate><title>Synthesis of Nano Calcium Phosphate via Biomimetic Method for Bone Tissue Engineering Scaffolds and Investigation of its Phase Transformation in Simulated Body Fluid</title><author>Moztarzadeh, F. ; Shokrgozar, Mohammad A. ; Raz, Majid ; Tahriri, M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c368t-8d89e64bc2b71bce4f887b961b30e7b7ac2cfb59915df02406493d22d0e708323</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Calcium phosphate</topic><topic>Diffusion</topic><topic>Fourier transforms</topic><topic>Hydrogels</topic><topic>Phase transformations</topic><topic>Precipitates</topic><topic>Precipitation</topic><topic>Scanning electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Moztarzadeh, F.</creatorcontrib><creatorcontrib>Shokrgozar, Mohammad A.</creatorcontrib><creatorcontrib>Raz, Majid</creatorcontrib><creatorcontrib>Tahriri, M.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Key engineering materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Moztarzadeh, F.</au><au>Shokrgozar, Mohammad A.</au><au>Raz, Majid</au><au>Tahriri, M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Nano Calcium Phosphate via Biomimetic Method for Bone Tissue Engineering Scaffolds and Investigation of its Phase Transformation in Simulated Body Fluid</atitle><jtitle>Key engineering materials</jtitle><date>2014-01-01</date><risdate>2014</risdate><volume>587</volume><spage>86</spage><epage>92</epage><pages>86-92</pages><issn>1013-9826</issn><issn>1662-9795</issn><eissn>1662-9795</eissn><abstract>In this study the formation of calcium phosphate phase via double diffusion method into a hydrogel matrix was investigated and its phase transformation in simulated body fluid was studied. 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| subjects | Calcium phosphate Diffusion Fourier transforms Hydrogels Phase transformations Precipitates Precipitation Scanning electron microscopy |
| title | Synthesis of Nano Calcium Phosphate via Biomimetic Method for Bone Tissue Engineering Scaffolds and Investigation of its Phase Transformation in Simulated Body Fluid |
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