Positron annihilation study of acryl amide/poly (metha acrylic acid) membrane
Gamma irradiation posses a serious role for casting the membranes. Acryl amide /poly (methacrylic acid) membrane was synthesized under γ-radiation effect. The structure of the membrane was characterized by FTIR, thermo-gravimetric analysis and the scanning electron microscope. The properties of the...
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Veröffentlicht in: | Journal of physics. Conference series 2011-01, Vol.262 (1), p.012005-4 |
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creator | Abdel-Hady, E E Abdel-Hamed, M O Eltoony, M M Hammam, A M Elsharkawy, M R M |
description | Gamma irradiation posses a serious role for casting the membranes. Acryl amide /poly (methacrylic acid) membrane was synthesized under γ-radiation effect. The structure of the membrane was characterized by FTIR, thermo-gravimetric analysis and the scanning electron microscope. The properties of the membranes were also investigated in terms of proton conductivity and positron annihilation lifetime (PAL) parameters. On the basis of the values of the long-lived components in the lifetime spectra, the size of the free volume and their intensity were calculated. The positron lifetime study on these irradiated casted membranes shows that the cross-linking and degradation within the membrane matrix affect the free volume content and hence the microstructure. |
doi_str_mv | 10.1088/1742-6596/262/1/012005 |
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Acryl amide /poly (methacrylic acid) membrane was synthesized under γ-radiation effect. The structure of the membrane was characterized by FTIR, thermo-gravimetric analysis and the scanning electron microscope. The properties of the membranes were also investigated in terms of proton conductivity and positron annihilation lifetime (PAL) parameters. On the basis of the values of the long-lived components in the lifetime spectra, the size of the free volume and their intensity were calculated. The positron lifetime study on these irradiated casted membranes shows that the cross-linking and degradation within the membrane matrix affect the free volume content and hence the microstructure.</description><identifier>ISSN: 1742-6596</identifier><identifier>ISSN: 1742-6588</identifier><identifier>EISSN: 1742-6596</identifier><identifier>DOI: 10.1088/1742-6596/262/1/012005</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Acrylic acid ; Amides ; Crosslinking ; Gamma irradiation ; Gravimetric analysis ; Mathematical analysis ; Membranes ; Methacrylic acid ; Physics ; Positron annihilation ; Positrons ; Scanning electron microscopy ; Service life assessment ; Spectra</subject><ispartof>Journal of physics. Conference series, 2011-01, Vol.262 (1), p.012005-4</ispartof><rights>Copyright IOP Publishing Jan 2011</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c444t-44ba10c552ce9368b030d77bcf381f4a52d894dd08c2afd5ee9b3b423947cac13</citedby><cites>FETCH-LOGICAL-c444t-44ba10c552ce9368b030d77bcf381f4a52d894dd08c2afd5ee9b3b423947cac13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://iopscience.iop.org/article/10.1088/1742-6596/262/1/012005/pdf$$EPDF$$P50$$Giop$$H</linktopdf><link.rule.ids>314,780,784,1553,27628,27924,27925,53904,53931</link.rule.ids><linktorsrc>$$Uhttp://iopscience.iop.org/1742-6596/262/1/012005$$EView_record_in_IOP_Publishing$$FView_record_in_$$GIOP_Publishing</linktorsrc></links><search><creatorcontrib>Abdel-Hady, E E</creatorcontrib><creatorcontrib>Abdel-Hamed, M O</creatorcontrib><creatorcontrib>Eltoony, M M</creatorcontrib><creatorcontrib>Hammam, A M</creatorcontrib><creatorcontrib>Elsharkawy, M R M</creatorcontrib><title>Positron annihilation study of acryl amide/poly (metha acrylic acid) membrane</title><title>Journal of physics. Conference series</title><description>Gamma irradiation posses a serious role for casting the membranes. Acryl amide /poly (methacrylic acid) membrane was synthesized under γ-radiation effect. The structure of the membrane was characterized by FTIR, thermo-gravimetric analysis and the scanning electron microscope. The properties of the membranes were also investigated in terms of proton conductivity and positron annihilation lifetime (PAL) parameters. On the basis of the values of the long-lived components in the lifetime spectra, the size of the free volume and their intensity were calculated. The positron lifetime study on these irradiated casted membranes shows that the cross-linking and degradation within the membrane matrix affect the free volume content and hence the microstructure.</description><subject>Acrylic acid</subject><subject>Amides</subject><subject>Crosslinking</subject><subject>Gamma irradiation</subject><subject>Gravimetric analysis</subject><subject>Mathematical analysis</subject><subject>Membranes</subject><subject>Methacrylic acid</subject><subject>Physics</subject><subject>Positron annihilation</subject><subject>Positrons</subject><subject>Scanning electron microscopy</subject><subject>Service life assessment</subject><subject>Spectra</subject><issn>1742-6596</issn><issn>1742-6588</issn><issn>1742-6596</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kMtOxCAUhhujiePoK5gmbsZFLVAosDQTb8kYXeiaUKAZJm2p0C769jKpUWMmsjlcvv9w8iXJJQQ3EDCWQ4pRVhJe5qhEOcwBRACQo2Tx_XD8a3-anIWwA6CIiy6S51cX7OBdl8qus1vbyMHGQxhGPaWuTqXyU5PK1mqT966Z0lVrhq2c762K1errtDVt5WVnzpOTWjbBXHzVZfJ-f_e2fsw2Lw9P69tNpjDGQ4ZxJSFQhCBleFGyChRAU1qpumCwxpIgzTjWGjCFZK2JMbwqKowKjqmSChbLZDX37b37GE0YRGuDMk0TZ3BjELCklJeccRDRqz_ozo2-i9MJRChHCBWMRKqcKeVdCN7Uove2lX4SEIi9ZbEXKPYCRbQsoJgtx2A2B63rfzIHWdHrOvLwAP__H58XHIsu</recordid><startdate>20110101</startdate><enddate>20110101</enddate><creator>Abdel-Hady, E E</creator><creator>Abdel-Hamed, M O</creator><creator>Eltoony, M M</creator><creator>Hammam, A M</creator><creator>Elsharkawy, M R M</creator><general>IOP Publishing</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>H8D</scope><scope>HCIFZ</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>7U5</scope><scope>8BQ</scope><scope>JG9</scope></search><sort><creationdate>20110101</creationdate><title>Positron annihilation study of acryl amide/poly (metha acrylic acid) membrane</title><author>Abdel-Hady, E E ; Abdel-Hamed, M O ; Eltoony, M M ; Hammam, A M ; Elsharkawy, M R M</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c444t-44ba10c552ce9368b030d77bcf381f4a52d894dd08c2afd5ee9b3b423947cac13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Acrylic acid</topic><topic>Amides</topic><topic>Crosslinking</topic><topic>Gamma irradiation</topic><topic>Gravimetric analysis</topic><topic>Mathematical analysis</topic><topic>Membranes</topic><topic>Methacrylic acid</topic><topic>Physics</topic><topic>Positron annihilation</topic><topic>Positrons</topic><topic>Scanning electron microscopy</topic><topic>Service life assessment</topic><topic>Spectra</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Abdel-Hady, E E</creatorcontrib><creatorcontrib>Abdel-Hamed, M O</creatorcontrib><creatorcontrib>Eltoony, M M</creatorcontrib><creatorcontrib>Hammam, A M</creatorcontrib><creatorcontrib>Elsharkawy, M R M</creatorcontrib><collection>CrossRef</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Aerospace Database</collection><collection>SciTech Premium Collection</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Materials Research Database</collection><jtitle>Journal of physics. Conference series</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Abdel-Hady, E E</au><au>Abdel-Hamed, M O</au><au>Eltoony, M M</au><au>Hammam, A M</au><au>Elsharkawy, M R M</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Positron annihilation study of acryl amide/poly (metha acrylic acid) membrane</atitle><jtitle>Journal of physics. Conference series</jtitle><date>2011-01-01</date><risdate>2011</risdate><volume>262</volume><issue>1</issue><spage>012005</spage><epage>4</epage><pages>012005-4</pages><issn>1742-6596</issn><issn>1742-6588</issn><eissn>1742-6596</eissn><abstract>Gamma irradiation posses a serious role for casting the membranes. Acryl amide /poly (methacrylic acid) membrane was synthesized under γ-radiation effect. The structure of the membrane was characterized by FTIR, thermo-gravimetric analysis and the scanning electron microscope. The properties of the membranes were also investigated in terms of proton conductivity and positron annihilation lifetime (PAL) parameters. On the basis of the values of the long-lived components in the lifetime spectra, the size of the free volume and their intensity were calculated. The positron lifetime study on these irradiated casted membranes shows that the cross-linking and degradation within the membrane matrix affect the free volume content and hence the microstructure.</abstract><cop>Bristol</cop><pub>IOP Publishing</pub><doi>10.1088/1742-6596/262/1/012005</doi><tpages>4</tpages><oa>free_for_read</oa></addata></record> |
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subjects | Acrylic acid Amides Crosslinking Gamma irradiation Gravimetric analysis Mathematical analysis Membranes Methacrylic acid Physics Positron annihilation Positrons Scanning electron microscopy Service life assessment Spectra |
title | Positron annihilation study of acryl amide/poly (metha acrylic acid) membrane |
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