Fabrication of cemented tungsten carbide components by micro-powder injection moulding

•Manufacturing of a WC–Co component via micro-PIM was investigated.•A WC–10Co–0.8VC (wt.%) powder was mixed with a binder system based on paraffin wax.•The effect of injection, debinding and sintering conditions on process was evaluated.•The WC–Co micro-component was fabricated via micro-PIM success...

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Veröffentlicht in:Journal of materials processing technology 2014-07, Vol.214 (7), p.1436-1444
Hauptverfasser: Fayyaz, Abdolali, Muhamad, Norhamidi, Sulong, Abu Bakar, Rajabi, Javad, Wong, Yee Ning
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container_end_page 1444
container_issue 7
container_start_page 1436
container_title Journal of materials processing technology
container_volume 214
creator Fayyaz, Abdolali
Muhamad, Norhamidi
Sulong, Abu Bakar
Rajabi, Javad
Wong, Yee Ning
description •Manufacturing of a WC–Co component via micro-PIM was investigated.•A WC–10Co–0.8VC (wt.%) powder was mixed with a binder system based on paraffin wax.•The effect of injection, debinding and sintering conditions on process was evaluated.•The WC–Co micro-component was fabricated via micro-PIM successfully.•The relative density and hardness obtained were 94.5% and 1608HV, respectively. Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. This research shows that micro-PIM is able to produce small WC–Co components with properties comparable to conventional powder metallurgy.
doi_str_mv 10.1016/j.jmatprotec.2014.02.006
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Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. 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Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. 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Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. 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subjects Binders
Cemented carbides
Cemented tungsten carbide
Cermets
Cobalt
Debinding
Density
Injection molding
Micro-powder injection moulding
Powder metallurgy
Sintering
Sintering (powder metallurgy)
Tungsten carbide
title Fabrication of cemented tungsten carbide components by micro-powder injection moulding
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