Fabrication of cemented tungsten carbide components by micro-powder injection moulding
•Manufacturing of a WC–Co component via micro-PIM was investigated.•A WC–10Co–0.8VC (wt.%) powder was mixed with a binder system based on paraffin wax.•The effect of injection, debinding and sintering conditions on process was evaluated.•The WC–Co micro-component was fabricated via micro-PIM success...
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Veröffentlicht in: | Journal of materials processing technology 2014-07, Vol.214 (7), p.1436-1444 |
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creator | Fayyaz, Abdolali Muhamad, Norhamidi Sulong, Abu Bakar Rajabi, Javad Wong, Yee Ning |
description | •Manufacturing of a WC–Co component via micro-PIM was investigated.•A WC–10Co–0.8VC (wt.%) powder was mixed with a binder system based on paraffin wax.•The effect of injection, debinding and sintering conditions on process was evaluated.•The WC–Co micro-component was fabricated via micro-PIM successfully.•The relative density and hardness obtained were 94.5% and 1608HV, respectively.
Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. This research shows that micro-PIM is able to produce small WC–Co components with properties comparable to conventional powder metallurgy. |
doi_str_mv | 10.1016/j.jmatprotec.2014.02.006 |
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Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. This research shows that micro-PIM is able to produce small WC–Co components with properties comparable to conventional powder metallurgy.</description><identifier>ISSN: 0924-0136</identifier><identifier>DOI: 10.1016/j.jmatprotec.2014.02.006</identifier><language>eng</language><publisher>Elsevier B.V</publisher><subject>Binders ; Cemented carbides ; Cemented tungsten carbide ; Cermets ; Cobalt ; Debinding ; Density ; Injection molding ; Micro-powder injection moulding ; Powder metallurgy ; Sintering ; Sintering (powder metallurgy) ; Tungsten carbide</subject><ispartof>Journal of materials processing technology, 2014-07, Vol.214 (7), p.1436-1444</ispartof><rights>2014 Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c421t-858bfd5b5024f2e4985e49186065b5acbf52ac465f0cdc47e505869a7e6e795d3</citedby><cites>FETCH-LOGICAL-c421t-858bfd5b5024f2e4985e49186065b5acbf52ac465f0cdc47e505869a7e6e795d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jmatprotec.2014.02.006$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids></links><search><creatorcontrib>Fayyaz, Abdolali</creatorcontrib><creatorcontrib>Muhamad, Norhamidi</creatorcontrib><creatorcontrib>Sulong, Abu Bakar</creatorcontrib><creatorcontrib>Rajabi, Javad</creatorcontrib><creatorcontrib>Wong, Yee Ning</creatorcontrib><title>Fabrication of cemented tungsten carbide components by micro-powder injection moulding</title><title>Journal of materials processing technology</title><description>•Manufacturing of a WC–Co component via micro-PIM was investigated.•A WC–10Co–0.8VC (wt.%) powder was mixed with a binder system based on paraffin wax.•The effect of injection, debinding and sintering conditions on process was evaluated.•The WC–Co micro-component was fabricated via micro-PIM successfully.•The relative density and hardness obtained were 94.5% and 1608HV, respectively.
Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. This research shows that micro-PIM is able to produce small WC–Co components with properties comparable to conventional powder metallurgy.</description><subject>Binders</subject><subject>Cemented carbides</subject><subject>Cemented tungsten carbide</subject><subject>Cermets</subject><subject>Cobalt</subject><subject>Debinding</subject><subject>Density</subject><subject>Injection molding</subject><subject>Micro-powder injection moulding</subject><subject>Powder metallurgy</subject><subject>Sintering</subject><subject>Sintering (powder metallurgy)</subject><subject>Tungsten carbide</subject><issn>0924-0136</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqFkEtPwzAQhHMAiVL4Dz5ySVi78SNHQLwkJC7A1XLsTeWosYudgvj3uBSJI5ddaXdmpPmqilBoKFBxOTbjZOZtijPahgFtG2ANgDiqFtCxtga6EifVac4jAJWg1KJ6uzN98tbMPgYSB2JxwjCjI_MurPOMgViTeu-Q2DhtYyjPTPovMnmbYr2Nnw4T8WFE-5Mwxd3G-bA-q44Hs8l4_ruX1evd7cvNQ_30fP94c_VU25bRuVZc9YPjPQfWDgzbTvEyqBIgytHYfuDM2FbwAayzrUQOXInOSBQoO-5Wy-rikFtKv-8wz3ry2eJmYwLGXdZUSNlRyRj8L-W8E0IqKotUHaSlY84JB71NfjLpS1PQe9J61H-k9Z60BqYL6WK9PlixtP7wmHS2HoNF51NhpF30_4d8A6lvj7o</recordid><startdate>20140701</startdate><enddate>20140701</enddate><creator>Fayyaz, Abdolali</creator><creator>Muhamad, Norhamidi</creator><creator>Sulong, Abu Bakar</creator><creator>Rajabi, Javad</creator><creator>Wong, Yee Ning</creator><general>Elsevier B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20140701</creationdate><title>Fabrication of cemented tungsten carbide components by micro-powder injection moulding</title><author>Fayyaz, Abdolali ; Muhamad, Norhamidi ; Sulong, Abu Bakar ; Rajabi, Javad ; Wong, Yee Ning</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c421t-858bfd5b5024f2e4985e49186065b5acbf52ac465f0cdc47e505869a7e6e795d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Binders</topic><topic>Cemented carbides</topic><topic>Cemented tungsten carbide</topic><topic>Cermets</topic><topic>Cobalt</topic><topic>Debinding</topic><topic>Density</topic><topic>Injection molding</topic><topic>Micro-powder injection moulding</topic><topic>Powder metallurgy</topic><topic>Sintering</topic><topic>Sintering (powder metallurgy)</topic><topic>Tungsten carbide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Fayyaz, Abdolali</creatorcontrib><creatorcontrib>Muhamad, Norhamidi</creatorcontrib><creatorcontrib>Sulong, Abu Bakar</creatorcontrib><creatorcontrib>Rajabi, Javad</creatorcontrib><creatorcontrib>Wong, Yee Ning</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of materials processing technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Fayyaz, Abdolali</au><au>Muhamad, Norhamidi</au><au>Sulong, Abu Bakar</au><au>Rajabi, Javad</au><au>Wong, Yee Ning</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Fabrication of cemented tungsten carbide components by micro-powder injection moulding</atitle><jtitle>Journal of materials processing technology</jtitle><date>2014-07-01</date><risdate>2014</risdate><volume>214</volume><issue>7</issue><spage>1436</spage><epage>1444</epage><pages>1436-1444</pages><issn>0924-0136</issn><abstract>•Manufacturing of a WC–Co component via micro-PIM was investigated.•A WC–10Co–0.8VC (wt.%) powder was mixed with a binder system based on paraffin wax.•The effect of injection, debinding and sintering conditions on process was evaluated.•The WC–Co micro-component was fabricated via micro-PIM successfully.•The relative density and hardness obtained were 94.5% and 1608HV, respectively.
Micro-powder injection moulding (micro-PIM) is an advanced net-shaping process for the fabrication of metal and ceramic complex micro-components. Cemented tungsten carbide (WC–Co) hardmetal is known for its high hardness and wear resistance in various applications. Micro-PIM is a new alternative manufacturing technique for hardmetal micro-parts. In this work, the fabrication of WC–Co components via a micro-PIM process was studied. A fine WC–10Co–0.8VC (wt.%) powder was mixed with a binder system consisting of paraffin wax, low density polyethylene and stearic acid. A micro-component was injected at low pressure using a semi-automatic injection moulding machine. The injection temperature was determined from the rheological investigation of the feedstock. The binder extraction was carried out in solvent and thermal debinding methods under an argon atmosphere. Thermal gravimetric analysis was used to confirm the removal of the soluble binder from the green part. The sintering process has been performed within a temperature range of 1330–1450°C under vacuum. After sintering, a density of 94.5% theoretical density was obtained, which is a reasonable value. The micro-components showed length shrinkage between 16 and 22% and good surface quality and hardness values when compared with conventional powder metallurgy. This research shows that micro-PIM is able to produce small WC–Co components with properties comparable to conventional powder metallurgy.</abstract><pub>Elsevier B.V</pub><doi>10.1016/j.jmatprotec.2014.02.006</doi><tpages>9</tpages></addata></record> |
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subjects | Binders Cemented carbides Cemented tungsten carbide Cermets Cobalt Debinding Density Injection molding Micro-powder injection moulding Powder metallurgy Sintering Sintering (powder metallurgy) Tungsten carbide |
title | Fabrication of cemented tungsten carbide components by micro-powder injection moulding |
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