Preparation and Thermal Stability Characterization of Copper Tin Selenide Semiconductor Nanoparticles
Copper tin selenide (Cu2SnSe3) nanoparticle powders were successfully synthesized via chemical precipitation method at room temperature. Elemental composition analysis determined byenergy dispersive X-ray confirmed that the Cu2SnSe3 nanoparticles were successfully formed. Field emission scanning ele...
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| Veröffentlicht in: | Materials science forum 2013-05, Vol.756, p.66-73 |
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| creator | Talib, Zainal Abidin Wan Mahmood, Mat Yunus Zainal, Zulkarnain Ying Chyi Liew, Josephine |
| description | Copper tin selenide (Cu2SnSe3) nanoparticle powders were successfully synthesized via chemical precipitation method at room temperature. Elemental composition analysis determined byenergy dispersive X-ray confirmed that the Cu2SnSe3 nanoparticles were successfully formed. Field emission scanning electron and transmission electron micrograph showed the presence of homogeneous distribution of the small spherical nanoparticles in the Cu2SnSe3 powders. The thermal stability of the Cu2SnSe3 structure has been investigated by X-ray diffraction at temperatures ranging from 100 to 523 K. Differential scanning calorimetry and thermogravimetric analysis have been conducted to evaluate the thermal stability and it is found that the maximum temperature of the Cu2SnSe3 nanoparticles can withstand until 600 K. The results show that Cu2SnSe3 nanoparticles exhibited a stable structure at temperature range of 100 – 523 K. |
| doi_str_mv | 10.4028/www.scientific.net/MSF.756.66 |
| format | Article |
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Elemental composition analysis determined byenergy dispersive X-ray confirmed that the Cu2SnSe3 nanoparticles were successfully formed. Field emission scanning electron and transmission electron micrograph showed the presence of homogeneous distribution of the small spherical nanoparticles in the Cu2SnSe3 powders. The thermal stability of the Cu2SnSe3 structure has been investigated by X-ray diffraction at temperatures ranging from 100 to 523 K. Differential scanning calorimetry and thermogravimetric analysis have been conducted to evaluate the thermal stability and it is found that the maximum temperature of the Cu2SnSe3 nanoparticles can withstand until 600 K. 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Elemental composition analysis determined byenergy dispersive X-ray confirmed that the Cu2SnSe3 nanoparticles were successfully formed. Field emission scanning electron and transmission electron micrograph showed the presence of homogeneous distribution of the small spherical nanoparticles in the Cu2SnSe3 powders. The thermal stability of the Cu2SnSe3 structure has been investigated by X-ray diffraction at temperatures ranging from 100 to 523 K. Differential scanning calorimetry and thermogravimetric analysis have been conducted to evaluate the thermal stability and it is found that the maximum temperature of the Cu2SnSe3 nanoparticles can withstand until 600 K. The results show that Cu2SnSe3 nanoparticles exhibited a stable structure at temperature range of 100 – 523 K.</description><subject>Copper</subject><subject>Nanoparticles</subject><subject>PARTICLES</subject><subject>Precipitation</subject><subject>SELENIDES</subject><subject>SEMICONDUCTORS</subject><subject>THERMAL STABILITY</subject><subject>THERMOGRAVIMETRIC ANALYSIS</subject><subject>Tin</subject><subject>X RAYS</subject><issn>0255-5476</issn><issn>1662-9752</issn><issn>1662-9752</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqNkEFr3DAQhUVpoNsk_8GXQi92JFsaKYdSytK0haQt7OYslPGYVfBKrqRlSX99FLbQa07zYN578D7GPgjeSd6bq-Px2GX0FIqfPHaBytXd5qbTCjqAN2wlAPr2Wqv-LVvxXqlWSQ3v2PucHzkfhBGwYvQ70eKSKz6GxoWx2e4o7d3cbIp78LMvT816V_9YKPm_J1ucmnVcFkrN1odmQzMFP1IVe48xjAcsMTU_XYi1uHicKV-ws8nNmS7_3XN2f_N1u_7e3v769mP95bbFQZnSonESuEEcOBDonouxJ9JywoG0oFEiGKjLjTQECoWReiSJvVPu-kH303DOPp56lxT_HCgXu_cZaZ5doHjIVoAWIKRRUK2fTlZMMedEk12S37v0ZAW3L3htxWv_47UVr614bcVr4SX_-ZQvyYVcCHf2MR5SqPNe2fAMxYqOOQ</recordid><startdate>20130501</startdate><enddate>20130501</enddate><creator>Talib, Zainal Abidin</creator><creator>Wan Mahmood, Mat Yunus</creator><creator>Zainal, Zulkarnain</creator><creator>Ying Chyi Liew, Josephine</creator><general>Trans Tech Publications Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>H8G</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20130501</creationdate><title>Preparation and Thermal Stability Characterization of Copper Tin Selenide Semiconductor Nanoparticles</title><author>Talib, Zainal Abidin ; Wan Mahmood, Mat Yunus ; Zainal, Zulkarnain ; Ying Chyi Liew, Josephine</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c358t-c8a4608cc306e67201d2ee74fc3e71ed4c686028848e65c1847de4c2a5a9b72f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Copper</topic><topic>Nanoparticles</topic><topic>PARTICLES</topic><topic>Precipitation</topic><topic>SELENIDES</topic><topic>SEMICONDUCTORS</topic><topic>THERMAL STABILITY</topic><topic>THERMOGRAVIMETRIC ANALYSIS</topic><topic>Tin</topic><topic>X RAYS</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Talib, Zainal Abidin</creatorcontrib><creatorcontrib>Wan Mahmood, Mat Yunus</creatorcontrib><creatorcontrib>Zainal, Zulkarnain</creatorcontrib><creatorcontrib>Ying Chyi Liew, Josephine</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Materials science forum</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Talib, Zainal Abidin</au><au>Wan Mahmood, Mat Yunus</au><au>Zainal, Zulkarnain</au><au>Ying Chyi Liew, Josephine</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and Thermal Stability Characterization of Copper Tin Selenide Semiconductor Nanoparticles</atitle><jtitle>Materials science forum</jtitle><date>2013-05-01</date><risdate>2013</risdate><volume>756</volume><spage>66</spage><epage>73</epage><pages>66-73</pages><issn>0255-5476</issn><issn>1662-9752</issn><eissn>1662-9752</eissn><abstract>Copper tin selenide (Cu2SnSe3) nanoparticle powders were successfully synthesized via chemical precipitation method at room temperature. Elemental composition analysis determined byenergy dispersive X-ray confirmed that the Cu2SnSe3 nanoparticles were successfully formed. Field emission scanning electron and transmission electron micrograph showed the presence of homogeneous distribution of the small spherical nanoparticles in the Cu2SnSe3 powders. The thermal stability of the Cu2SnSe3 structure has been investigated by X-ray diffraction at temperatures ranging from 100 to 523 K. Differential scanning calorimetry and thermogravimetric analysis have been conducted to evaluate the thermal stability and it is found that the maximum temperature of the Cu2SnSe3 nanoparticles can withstand until 600 K. The results show that Cu2SnSe3 nanoparticles exhibited a stable structure at temperature range of 100 – 523 K.</abstract><pub>Trans Tech Publications Ltd</pub><doi>10.4028/www.scientific.net/MSF.756.66</doi><tpages>8</tpages></addata></record> |
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| subjects | Copper Nanoparticles PARTICLES Precipitation SELENIDES SEMICONDUCTORS THERMAL STABILITY THERMOGRAVIMETRIC ANALYSIS Tin X RAYS |
| title | Preparation and Thermal Stability Characterization of Copper Tin Selenide Semiconductor Nanoparticles |
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