ORGANIC SOL-GEL METHOD IN THE SYNTHESIS AND CHARACTERIZATION OF ZINC OXIDE NANOPARTICLES
Nanosized Zinc Oxide (ZnO) was synthesized, using sol-gel method. The nanomaterials with structure were annealed at different temperatures ranging from 500 to 700 degree Celsius which were chosen based on the Thermogravimetric Analysis. The structure and morphology were characterized by Powder XRay...
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| Veröffentlicht in: | American journal of applied sciences 2014-06, Vol.11 (6), p.959-962 |
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| container_title | American journal of applied sciences |
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| creator | Lee, Keanchuan Saipolbahri, Zulhilmi Akmal Guan, Beh Hoe Soleimani, Hassan |
| description | Nanosized Zinc Oxide (ZnO) was synthesized, using sol-gel method. The nanomaterials with structure were annealed at different temperatures ranging from 500 to 700 degree Celsius which were chosen based on the Thermogravimetric Analysis. The structure and morphology were characterized by Powder XRay Diffraction (PXRD) and Transmission Electron Microscope (TEM), respectively. The PXRD shows the increasing tendency in crystallite size when the annealing temperature increases and the hexagonal structure of ZnO. TEM further revealed the same tendency which the Zn NPs size increased with the annealing temperature. |
| doi_str_mv | 10.3844/ajassp.2014.959.962 |
| format | Article |
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The nanomaterials with structure were annealed at different temperatures ranging from 500 to 700 degree Celsius which were chosen based on the Thermogravimetric Analysis. The structure and morphology were characterized by Powder XRay Diffraction (PXRD) and Transmission Electron Microscope (TEM), respectively. The PXRD shows the increasing tendency in crystallite size when the annealing temperature increases and the hexagonal structure of ZnO. TEM further revealed the same tendency which the Zn NPs size increased with the annealing temperature.</description><identifier>ISSN: 1546-9239</identifier><identifier>EISSN: 1554-3641</identifier><identifier>DOI: 10.3844/ajassp.2014.959.962</identifier><language>eng</language><subject>Annealing ; Crystallites ; Diffraction ; Nanomaterials ; Nanoparticles ; Sol gel process ; Transmission electron microscopy ; Zinc oxide</subject><ispartof>American journal of applied sciences, 2014-06, Vol.11 (6), p.959-962</ispartof><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2422-23c95a98414eaf78aab2082dfb262a60caf4c4c49a5c978fdf313c31022cec6f3</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Lee, Keanchuan</creatorcontrib><creatorcontrib>Saipolbahri, Zulhilmi Akmal</creatorcontrib><creatorcontrib>Guan, Beh Hoe</creatorcontrib><creatorcontrib>Soleimani, Hassan</creatorcontrib><title>ORGANIC SOL-GEL METHOD IN THE SYNTHESIS AND CHARACTERIZATION OF ZINC OXIDE NANOPARTICLES</title><title>American journal of applied sciences</title><description>Nanosized Zinc Oxide (ZnO) was synthesized, using sol-gel method. The nanomaterials with structure were annealed at different temperatures ranging from 500 to 700 degree Celsius which were chosen based on the Thermogravimetric Analysis. The structure and morphology were characterized by Powder XRay Diffraction (PXRD) and Transmission Electron Microscope (TEM), respectively. The PXRD shows the increasing tendency in crystallite size when the annealing temperature increases and the hexagonal structure of ZnO. TEM further revealed the same tendency which the Zn NPs size increased with the annealing temperature.</description><subject>Annealing</subject><subject>Crystallites</subject><subject>Diffraction</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Sol gel process</subject><subject>Transmission electron microscopy</subject><subject>Zinc oxide</subject><issn>1546-9239</issn><issn>1554-3641</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNot0L1OwzAUBWALgUQpPAGLR5YE_8WJxyhNG0vBRkmQShfLdWOpVUtLTAfenlRFdzh3ODrDB8AzRjHNGHu1OxvCKSYIs1gkIhac3IAJThIWUc7w7eVnPBKEinvwEMIOIcpJiidgqZtFrmQBW11Hi7KGb2VX6RmUCnZVCdtPNUYrW5irGSyqvMmLrmzkKu-kVlDP4UqqAuqlnJVQ5Uq_500ni7psH8Gdt_vQP_3nFHzMy66oolovZJHXkSOMkIhQJxIrMoZZb32aWbsmKCMbvyacWI6c9cyNJ2ziRJr5jaeYOooRIa533NMpeLnunobj97kPP-awDa7f7-1XfzwHg3mKE84TRscqvVbdcAxh6L05DduDHX4NRubiaK6O5uJoRkczOtI_UWFgDA</recordid><startdate>20140611</startdate><enddate>20140611</enddate><creator>Lee, Keanchuan</creator><creator>Saipolbahri, Zulhilmi Akmal</creator><creator>Guan, Beh Hoe</creator><creator>Soleimani, Hassan</creator><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20140611</creationdate><title>ORGANIC SOL-GEL METHOD IN THE SYNTHESIS AND CHARACTERIZATION OF ZINC OXIDE NANOPARTICLES</title><author>Lee, Keanchuan ; Saipolbahri, Zulhilmi Akmal ; Guan, Beh Hoe ; Soleimani, Hassan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c2422-23c95a98414eaf78aab2082dfb262a60caf4c4c49a5c978fdf313c31022cec6f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Annealing</topic><topic>Crystallites</topic><topic>Diffraction</topic><topic>Nanomaterials</topic><topic>Nanoparticles</topic><topic>Sol gel process</topic><topic>Transmission electron microscopy</topic><topic>Zinc oxide</topic><toplevel>online_resources</toplevel><creatorcontrib>Lee, Keanchuan</creatorcontrib><creatorcontrib>Saipolbahri, Zulhilmi Akmal</creatorcontrib><creatorcontrib>Guan, Beh Hoe</creatorcontrib><creatorcontrib>Soleimani, Hassan</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>American journal of applied sciences</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lee, Keanchuan</au><au>Saipolbahri, Zulhilmi Akmal</au><au>Guan, Beh Hoe</au><au>Soleimani, Hassan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>ORGANIC SOL-GEL METHOD IN THE SYNTHESIS AND CHARACTERIZATION OF ZINC OXIDE NANOPARTICLES</atitle><jtitle>American journal of applied sciences</jtitle><date>2014-06-11</date><risdate>2014</risdate><volume>11</volume><issue>6</issue><spage>959</spage><epage>962</epage><pages>959-962</pages><issn>1546-9239</issn><eissn>1554-3641</eissn><abstract>Nanosized Zinc Oxide (ZnO) was synthesized, using sol-gel method. 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| subjects | Annealing Crystallites Diffraction Nanomaterials Nanoparticles Sol gel process Transmission electron microscopy Zinc oxide |
| title | ORGANIC SOL-GEL METHOD IN THE SYNTHESIS AND CHARACTERIZATION OF ZINC OXIDE NANOPARTICLES |
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