New strategy for RDC-assisted diastereotopic proton assignment using a combination of J-scaled BIRD HSQC and J-scaled BIRD HMQC/HSQC

A new strategy to assign diastereotopic protons was developed on the basis of residual dipolar couplings (RDCs) collected in compressed poly(methyl methacrylate) (PMMA) gels. A combination of 2D J‐scaled BIRD HSQC and J‐scaled BIRD HMQC/HSQC NMR experiments was used to collect the RDC data. In the p...

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