Properties of Smart-Scaled PTFE-Tubular Reactors for Continuous Emulsion Polymerization Reactions
Summary This article presents a novel design of smart scale PTFE tubular reactor systems for continuous polymerization reactions. To optimize the flow pattern, CFD calculations and RTD experiments were done. These results led to an unique tube geometry combined with a specialized arrangement of stat...
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| Veröffentlicht in: | Macromolecular symposia. 2013-11, Vol.333 (1), p.69-79 |
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| container_title | Macromolecular symposia. |
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| creator | Lueth, Fabian Gabriel Pauer, Werner Moritz, Hans-Ulrich |
| description | Summary
This article presents a novel design of smart scale PTFE tubular reactor systems for continuous polymerization reactions. To optimize the flow pattern, CFD calculations and RTD experiments were done. These results led to an unique tube geometry combined with a specialized arrangement of static mixers. A comparison of heat transfer properties of two different types of tubular reactors shows the feasibility of using PTFE instead of stainless steel as reactor construction material. The versatility of the operation modes is demonstrated for emulsion copolymerization experiments with the same recipe but at the different modes. |
| doi_str_mv | 10.1002/masy.201300086 |
| format | Article |
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This article presents a novel design of smart scale PTFE tubular reactor systems for continuous polymerization reactions. To optimize the flow pattern, CFD calculations and RTD experiments were done. These results led to an unique tube geometry combined with a specialized arrangement of static mixers. A comparison of heat transfer properties of two different types of tubular reactors shows the feasibility of using PTFE instead of stainless steel as reactor construction material. The versatility of the operation modes is demonstrated for emulsion copolymerization experiments with the same recipe but at the different modes.</description><identifier>ISSN: 1022-1360</identifier><identifier>EISSN: 1521-3900</identifier><identifier>DOI: 10.1002/masy.201300086</identifier><language>eng</language><publisher>Blackwell Publishing Ltd</publisher><subject>CFD ; Computational fluid dynamics ; Copolymerization ; Design engineering ; emulsion polymerization ; Feasibility ; flow pattern ; heat transfer ; Mathematical analysis ; polytetrafluoroethylene (PTFE) ; Polytetrafluoroethylenes ; Reactors ; residence time distribution ; smart scale ; Tubes ; tubular reactor</subject><ispartof>Macromolecular symposia., 2013-11, Vol.333 (1), p.69-79</ispartof><rights>2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fmasy.201300086$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fmasy.201300086$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>315,781,785,1418,27929,27930,45579,45580</link.rule.ids></links><search><creatorcontrib>Lueth, Fabian Gabriel</creatorcontrib><creatorcontrib>Pauer, Werner</creatorcontrib><creatorcontrib>Moritz, Hans-Ulrich</creatorcontrib><title>Properties of Smart-Scaled PTFE-Tubular Reactors for Continuous Emulsion Polymerization Reactions</title><title>Macromolecular symposia.</title><addtitle>Macromol. Symp</addtitle><description>Summary
This article presents a novel design of smart scale PTFE tubular reactor systems for continuous polymerization reactions. To optimize the flow pattern, CFD calculations and RTD experiments were done. These results led to an unique tube geometry combined with a specialized arrangement of static mixers. A comparison of heat transfer properties of two different types of tubular reactors shows the feasibility of using PTFE instead of stainless steel as reactor construction material. The versatility of the operation modes is demonstrated for emulsion copolymerization experiments with the same recipe but at the different modes.</description><subject>CFD</subject><subject>Computational fluid dynamics</subject><subject>Copolymerization</subject><subject>Design engineering</subject><subject>emulsion polymerization</subject><subject>Feasibility</subject><subject>flow pattern</subject><subject>heat transfer</subject><subject>Mathematical analysis</subject><subject>polytetrafluoroethylene (PTFE)</subject><subject>Polytetrafluoroethylenes</subject><subject>Reactors</subject><subject>residence time distribution</subject><subject>smart scale</subject><subject>Tubes</subject><subject>tubular reactor</subject><issn>1022-1360</issn><issn>1521-3900</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNo9kM1Lw0AQxYMoWKtXzzl6Sd2P7keOpbRRiVpsRTwtk81Gokm27iZo_OtNrfQ078HvDTMvCC4xmmCEyHUNvp8QhClCSPKjYIQZwRGNEToeNCIkwpSj0-DM-_cBiWOBRwGsnN0a15bGh7YI1zW4NlprqEwerjbLRbTpsq4CFz4Z0K11PiysC-e2acums50PF3VX-dI24cpWfW1c-QPtzv7xg_DnwUkBlTcX_3McPC8Xm_lNlD4mt_NZGr3R4a4opzpmRExzXSCYao5NJjEDAAaxAM41ZToWBFMphZYFzowspISMZAVBOWV0HFzt926d_eyMb1Vdem2qChozHKowF5gxITka0HiPfpWV6dXWlcPbvcJI7YpUuyLVoUh1P1u_HtyQjfbZ0rfm-5AF96G4oIKpl4dEJQlPKbtLFaa_G-d6FQ</recordid><startdate>201311</startdate><enddate>201311</enddate><creator>Lueth, Fabian Gabriel</creator><creator>Pauer, Werner</creator><creator>Moritz, Hans-Ulrich</creator><general>Blackwell Publishing Ltd</general><scope>BSCLL</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>201311</creationdate><title>Properties of Smart-Scaled PTFE-Tubular Reactors for Continuous Emulsion Polymerization Reactions</title><author>Lueth, Fabian Gabriel ; Pauer, Werner ; Moritz, Hans-Ulrich</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-g3136-d3c95274dcf0a4c61eb815aaa5a97a66c35c97213887c8f1be8f88ab2bf20d353</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>CFD</topic><topic>Computational fluid dynamics</topic><topic>Copolymerization</topic><topic>Design engineering</topic><topic>emulsion polymerization</topic><topic>Feasibility</topic><topic>flow pattern</topic><topic>heat transfer</topic><topic>Mathematical analysis</topic><topic>polytetrafluoroethylene (PTFE)</topic><topic>Polytetrafluoroethylenes</topic><topic>Reactors</topic><topic>residence time distribution</topic><topic>smart scale</topic><topic>Tubes</topic><topic>tubular reactor</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lueth, Fabian Gabriel</creatorcontrib><creatorcontrib>Pauer, Werner</creatorcontrib><creatorcontrib>Moritz, Hans-Ulrich</creatorcontrib><collection>Istex</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Macromolecular symposia.</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lueth, Fabian Gabriel</au><au>Pauer, Werner</au><au>Moritz, Hans-Ulrich</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Properties of Smart-Scaled PTFE-Tubular Reactors for Continuous Emulsion Polymerization Reactions</atitle><jtitle>Macromolecular symposia.</jtitle><addtitle>Macromol. Symp</addtitle><date>2013-11</date><risdate>2013</risdate><volume>333</volume><issue>1</issue><spage>69</spage><epage>79</epage><pages>69-79</pages><issn>1022-1360</issn><eissn>1521-3900</eissn><abstract>Summary
This article presents a novel design of smart scale PTFE tubular reactor systems for continuous polymerization reactions. To optimize the flow pattern, CFD calculations and RTD experiments were done. These results led to an unique tube geometry combined with a specialized arrangement of static mixers. A comparison of heat transfer properties of two different types of tubular reactors shows the feasibility of using PTFE instead of stainless steel as reactor construction material. The versatility of the operation modes is demonstrated for emulsion copolymerization experiments with the same recipe but at the different modes.</abstract><pub>Blackwell Publishing Ltd</pub><doi>10.1002/masy.201300086</doi><tpages>11</tpages></addata></record> |
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| language | eng |
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| source | Wiley Online Library |
| subjects | CFD Computational fluid dynamics Copolymerization Design engineering emulsion polymerization Feasibility flow pattern heat transfer Mathematical analysis polytetrafluoroethylene (PTFE) Polytetrafluoroethylenes Reactors residence time distribution smart scale Tubes tubular reactor |
| title | Properties of Smart-Scaled PTFE-Tubular Reactors for Continuous Emulsion Polymerization Reactions |
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