Imaging interfacial micro- and nano-bubbles by scanning transmission soft X-ray microscopy
Synchrotron‐based scanning transmission soft X‐ray microscopy (STXM) with nanometer resolution was used to investigate the existence and behavior of interfacial gas nanobubbles confined between two silicon nitride windows. The observed nanobubbles of SF6 and Ne with diameters smaller than 2.5 µm wer...
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| Veröffentlicht in: | Journal of synchrotron radiation 2013-05, Vol.20 (3), p.413-418 |
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| creator | Zhang, Lijuan Zhao, Binyu Xue, Lian Guo, Zhi Dong, Yaming Fang, Haiping Tai, Renzhong Hu, Jun |
| description | Synchrotron‐based scanning transmission soft X‐ray microscopy (STXM) with nanometer resolution was used to investigate the existence and behavior of interfacial gas nanobubbles confined between two silicon nitride windows. The observed nanobubbles of SF6 and Ne with diameters smaller than 2.5 µm were quite stable. However, larger bubbles became unstable and grew during the soft X‐ray imaging, indicating that stable nanobubbles may have a length scale, which is consistent with a previous report using atomic force microscopy [Zhang et al. (2010), Soft Matter, 6, 4515–4519]. Here, it is shown that STXM is a promising technique for studying the aggregation of gases near the solid/water interfaces at the nanometer scale. |
| doi_str_mv | 10.1107/S0909049513003671 |
| format | Article |
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The observed nanobubbles of SF6 and Ne with diameters smaller than 2.5 µm were quite stable. However, larger bubbles became unstable and grew during the soft X‐ray imaging, indicating that stable nanobubbles may have a length scale, which is consistent with a previous report using atomic force microscopy [Zhang et al. (2010), Soft Matter, 6, 4515–4519]. 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Synchrotron Rad</addtitle><description>Synchrotron‐based scanning transmission soft X‐ray microscopy (STXM) with nanometer resolution was used to investigate the existence and behavior of interfacial gas nanobubbles confined between two silicon nitride windows. The observed nanobubbles of SF6 and Ne with diameters smaller than 2.5 µm were quite stable. However, larger bubbles became unstable and grew during the soft X‐ray imaging, indicating that stable nanobubbles may have a length scale, which is consistent with a previous report using atomic force microscopy [Zhang et al. (2010), Soft Matter, 6, 4515–4519]. Here, it is shown that STXM is a promising technique for studying the aggregation of gases near the solid/water interfaces at the nanometer scale.</description><subject>Equipment Design</subject><subject>Equipment Failure Analysis</subject><subject>Gases - analysis</subject><subject>Image Enhancement - instrumentation</subject><subject>Imaging</subject><subject>interfacial science</subject><subject>Microscopy</subject><subject>Microscopy, Electron, Scanning Transmission - instrumentation</subject><subject>nanobubbles</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nanostructure</subject><subject>Nanostructures - analysis</subject><subject>Nanostructures - ultrastructure</subject><subject>Scanning</subject><subject>scanning transmission soft X-ray microscopy</subject><subject>Soft x-rays</subject><subject>Synchrotron radiation</subject><subject>Synchrotrons - instrumentation</subject><issn>1600-5775</issn><issn>0909-0495</issn><issn>1600-5775</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkUtP3DAUha2qqMCUH9ANitQNmxQ_xna8rIbXVIguAPHYWI4fyDRxBjtRm3-PhwCqYIG8sC1959x7dAD4huAPhCDfP4cin7mgiEBIGEefwBZiEJaUc_r5v_cm2E7pHkLEOCZfwCYmVGCGxBa4Xbbqzoe7wofeRqe0V03Reh27slDBFEGFrqyHum5sKuqxSFqFsOb7qEJqfUq-C0XqXF9cl1GNkzbpbjV-BRtONcnuPN8zcHl0eLE4KU9_Hy8XP09LTWlFSscqg5ERnBlMrXWYwEpbjCwzpFJMC2Kh0ih_jDEO8ZoIqOcVYsI5rYwhM7A3-a5i9zDY1Mu8lrZNo4LthiRzaERxJQT8GCW4ovM8gGT0-xv0vhtiyEGeKIg5g_NMoYlah07ROrmKvlVxlAjKdUfyXUdZs_vsPNStNa-Kl1IyUE3AX9_Y8WNH-ev85uSIYrzeupykPvX236tUxT-SccKpvDo7luSAXy8IvpUX5BGNMqq7</recordid><startdate>201305</startdate><enddate>201305</enddate><creator>Zhang, Lijuan</creator><creator>Zhao, Binyu</creator><creator>Xue, Lian</creator><creator>Guo, Zhi</creator><creator>Dong, Yaming</creator><creator>Fang, Haiping</creator><creator>Tai, Renzhong</creator><creator>Hu, Jun</creator><general>International Union of Crystallography</general><general>John Wiley & Sons, Inc</general><scope>BSCLL</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>JQ2</scope><scope>L7M</scope><scope>7X8</scope></search><sort><creationdate>201305</creationdate><title>Imaging interfacial micro- and nano-bubbles by scanning transmission soft X-ray microscopy</title><author>Zhang, Lijuan ; Zhao, Binyu ; Xue, Lian ; Guo, Zhi ; Dong, Yaming ; Fang, Haiping ; Tai, Renzhong ; Hu, Jun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c5583-f68d21d976d25eef2308ce21e6d38a6c93e0ac1d38dddf17b390c48169ffcadd3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Equipment Design</topic><topic>Equipment Failure Analysis</topic><topic>Gases - analysis</topic><topic>Image Enhancement - instrumentation</topic><topic>Imaging</topic><topic>interfacial science</topic><topic>Microscopy</topic><topic>Microscopy, Electron, Scanning Transmission - instrumentation</topic><topic>nanobubbles</topic><topic>Nanocomposites</topic><topic>Nanomaterials</topic><topic>Nanostructure</topic><topic>Nanostructures - analysis</topic><topic>Nanostructures - ultrastructure</topic><topic>Scanning</topic><topic>scanning transmission soft X-ray microscopy</topic><topic>Soft x-rays</topic><topic>Synchrotron radiation</topic><topic>Synchrotrons - instrumentation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhang, Lijuan</creatorcontrib><creatorcontrib>Zhao, Binyu</creatorcontrib><creatorcontrib>Xue, Lian</creatorcontrib><creatorcontrib>Guo, Zhi</creatorcontrib><creatorcontrib>Dong, Yaming</creatorcontrib><creatorcontrib>Fang, Haiping</creatorcontrib><creatorcontrib>Tai, Renzhong</creatorcontrib><creatorcontrib>Hu, Jun</creatorcontrib><collection>Istex</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest Computer Science Collection</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of synchrotron radiation</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext_linktorsrc</fulltext></delivery><addata><au>Zhang, Lijuan</au><au>Zhao, Binyu</au><au>Xue, Lian</au><au>Guo, Zhi</au><au>Dong, Yaming</au><au>Fang, Haiping</au><au>Tai, Renzhong</au><au>Hu, Jun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Imaging interfacial micro- and nano-bubbles by scanning transmission soft X-ray microscopy</atitle><jtitle>Journal of synchrotron radiation</jtitle><addtitle>J. Synchrotron Rad</addtitle><date>2013-05</date><risdate>2013</risdate><volume>20</volume><issue>3</issue><spage>413</spage><epage>418</epage><pages>413-418</pages><issn>1600-5775</issn><issn>0909-0495</issn><eissn>1600-5775</eissn><abstract>Synchrotron‐based scanning transmission soft X‐ray microscopy (STXM) with nanometer resolution was used to investigate the existence and behavior of interfacial gas nanobubbles confined between two silicon nitride windows. The observed nanobubbles of SF6 and Ne with diameters smaller than 2.5 µm were quite stable. However, larger bubbles became unstable and grew during the soft X‐ray imaging, indicating that stable nanobubbles may have a length scale, which is consistent with a previous report using atomic force microscopy [Zhang et al. (2010), Soft Matter, 6, 4515–4519]. 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| subjects | Equipment Design Equipment Failure Analysis Gases - analysis Image Enhancement - instrumentation Imaging interfacial science Microscopy Microscopy, Electron, Scanning Transmission - instrumentation nanobubbles Nanocomposites Nanomaterials Nanostructure Nanostructures - analysis Nanostructures - ultrastructure Scanning scanning transmission soft X-ray microscopy Soft x-rays Synchrotron radiation Synchrotrons - instrumentation |
| title | Imaging interfacial micro- and nano-bubbles by scanning transmission soft X-ray microscopy |
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