Vitrification of Liquid Inclusions in hcp 3He-4He Crystal: the Role of an Intermediate bcc Phase
The phase structure of the rapidly quenched solid helium samples is studied by the NMR technique in dilute 3 He- 4 He mixtures at 1.35–1.8 K. The pulse NMR method is used to measure the spin-lattice and spin-spin relaxation times for all coexisting phases. An additional spin-lattice relaxation proce...
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| Veröffentlicht in: | Journal of low temperature physics 2014-04, Vol.175 (1-2), p.154-159 |
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| container_title | Journal of low temperature physics |
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| creator | Mikhin, N. P. Birchenko, A. P. Neoneta, A. S. Rudavskii, E. Y. Baidakov, V. G. |
| description | The phase structure of the rapidly quenched solid helium samples is studied by the NMR technique in dilute
3
He-
4
He mixtures at 1.35–1.8 K. The pulse NMR method is used to measure the spin-lattice and spin-spin relaxation times for all coexisting phases. An additional spin-lattice relaxation process is found just before vitrification of the liquid inclusions in hcp matrix. The relaxation rate of the new process coincides with that of bcc solid. It has been found that the new relaxation process is observed only in the temperature region of the phase diagram where an equilibrium bcc phase exists. After the liquid inclusions vitrification has been completed, the contribution from the bcc phase is not detected. The spin-lattice relaxation times in all of coexisting phases are discussed. |
| doi_str_mv | 10.1007/s10909-013-0941-3 |
| format | Article |
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3
He-
4
He mixtures at 1.35–1.8 K. The pulse NMR method is used to measure the spin-lattice and spin-spin relaxation times for all coexisting phases. An additional spin-lattice relaxation process is found just before vitrification of the liquid inclusions in hcp matrix. The relaxation rate of the new process coincides with that of bcc solid. It has been found that the new relaxation process is observed only in the temperature region of the phase diagram where an equilibrium bcc phase exists. After the liquid inclusions vitrification has been completed, the contribution from the bcc phase is not detected. The spin-lattice relaxation times in all of coexisting phases are discussed.</description><identifier>ISSN: 0022-2291</identifier><identifier>EISSN: 1573-7357</identifier><identifier>DOI: 10.1007/s10909-013-0941-3</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Body centered cubic lattice ; Characterization and Evaluation of Materials ; Close packed lattices ; Condensed Matter Physics ; Hexagonal cells ; Inclusions ; Liquids ; Magnetic Materials ; Magnetism ; Nuclear magnetic resonance ; Physics ; Physics and Astronomy ; Spin-lattice relaxation ; Vitrification</subject><ispartof>Journal of low temperature physics, 2014-04, Vol.175 (1-2), p.154-159</ispartof><rights>Springer Science+Business Media New York 2013</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c1663-9a93d59f648782530eb673831acf6a1103fb1dd78660c9970e913b4269dc5963</citedby><cites>FETCH-LOGICAL-c1663-9a93d59f648782530eb673831acf6a1103fb1dd78660c9970e913b4269dc5963</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10909-013-0941-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10909-013-0941-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Mikhin, N. P.</creatorcontrib><creatorcontrib>Birchenko, A. P.</creatorcontrib><creatorcontrib>Neoneta, A. S.</creatorcontrib><creatorcontrib>Rudavskii, E. Y.</creatorcontrib><creatorcontrib>Baidakov, V. G.</creatorcontrib><title>Vitrification of Liquid Inclusions in hcp 3He-4He Crystal: the Role of an Intermediate bcc Phase</title><title>Journal of low temperature physics</title><addtitle>J Low Temp Phys</addtitle><description>The phase structure of the rapidly quenched solid helium samples is studied by the NMR technique in dilute
3
He-
4
He mixtures at 1.35–1.8 K. The pulse NMR method is used to measure the spin-lattice and spin-spin relaxation times for all coexisting phases. An additional spin-lattice relaxation process is found just before vitrification of the liquid inclusions in hcp matrix. The relaxation rate of the new process coincides with that of bcc solid. It has been found that the new relaxation process is observed only in the temperature region of the phase diagram where an equilibrium bcc phase exists. After the liquid inclusions vitrification has been completed, the contribution from the bcc phase is not detected. The spin-lattice relaxation times in all of coexisting phases are discussed.</description><subject>Body centered cubic lattice</subject><subject>Characterization and Evaluation of Materials</subject><subject>Close packed lattices</subject><subject>Condensed Matter Physics</subject><subject>Hexagonal cells</subject><subject>Inclusions</subject><subject>Liquids</subject><subject>Magnetic Materials</subject><subject>Magnetism</subject><subject>Nuclear magnetic resonance</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Spin-lattice relaxation</subject><subject>Vitrification</subject><issn>0022-2291</issn><issn>1573-7357</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNp9kEFLwzAUgIMoOKc_wFuOXqLvNU3SeJOhbjBQZHiNaZq6jK7dkvbgv7ejnj09eHzfg_cRcotwjwDqISFo0AyQM9A5Mn5GZigUZ4oLdU5mAFnGskzjJblKaQcAupB8Rr4-Qx9DHZztQ9fSrqbrcBxCRVeta4Y07hINLd26A-VLz_Klp4v4k3rbPNJ-6-lH1_iTZdvR6H3c-yrY3tPSOfq-tclfk4vaNsnf_M052bw8bxZLtn57XS2e1syhlJxpq3kldC3zQhWZ4OBLqXjB0bpaWkTgdYlVpQopwWmtwGvkZZ5JXTmhJZ-Tu-nsIXbHwafe7ENyvmls67shGZQKc50LIUYUJ9TFLqXoa3OIYW_jj0Ewp5hmimnGmOYU0_DRySYnjWz77aPZdUNsx4f-kX4BqO50-g</recordid><startdate>20140401</startdate><enddate>20140401</enddate><creator>Mikhin, N. P.</creator><creator>Birchenko, A. P.</creator><creator>Neoneta, A. S.</creator><creator>Rudavskii, E. Y.</creator><creator>Baidakov, V. G.</creator><general>Springer US</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20140401</creationdate><title>Vitrification of Liquid Inclusions in hcp 3He-4He Crystal: the Role of an Intermediate bcc Phase</title><author>Mikhin, N. P. ; Birchenko, A. P. ; Neoneta, A. S. ; Rudavskii, E. Y. ; Baidakov, V. G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c1663-9a93d59f648782530eb673831acf6a1103fb1dd78660c9970e913b4269dc5963</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Body centered cubic lattice</topic><topic>Characterization and Evaluation of Materials</topic><topic>Close packed lattices</topic><topic>Condensed Matter Physics</topic><topic>Hexagonal cells</topic><topic>Inclusions</topic><topic>Liquids</topic><topic>Magnetic Materials</topic><topic>Magnetism</topic><topic>Nuclear magnetic resonance</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Spin-lattice relaxation</topic><topic>Vitrification</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Mikhin, N. P.</creatorcontrib><creatorcontrib>Birchenko, A. P.</creatorcontrib><creatorcontrib>Neoneta, A. S.</creatorcontrib><creatorcontrib>Rudavskii, E. Y.</creatorcontrib><creatorcontrib>Baidakov, V. G.</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of low temperature physics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Mikhin, N. P.</au><au>Birchenko, A. P.</au><au>Neoneta, A. S.</au><au>Rudavskii, E. Y.</au><au>Baidakov, V. G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Vitrification of Liquid Inclusions in hcp 3He-4He Crystal: the Role of an Intermediate bcc Phase</atitle><jtitle>Journal of low temperature physics</jtitle><stitle>J Low Temp Phys</stitle><date>2014-04-01</date><risdate>2014</risdate><volume>175</volume><issue>1-2</issue><spage>154</spage><epage>159</epage><pages>154-159</pages><issn>0022-2291</issn><eissn>1573-7357</eissn><abstract>The phase structure of the rapidly quenched solid helium samples is studied by the NMR technique in dilute
3
He-
4
He mixtures at 1.35–1.8 K. The pulse NMR method is used to measure the spin-lattice and spin-spin relaxation times for all coexisting phases. An additional spin-lattice relaxation process is found just before vitrification of the liquid inclusions in hcp matrix. The relaxation rate of the new process coincides with that of bcc solid. It has been found that the new relaxation process is observed only in the temperature region of the phase diagram where an equilibrium bcc phase exists. After the liquid inclusions vitrification has been completed, the contribution from the bcc phase is not detected. The spin-lattice relaxation times in all of coexisting phases are discussed.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10909-013-0941-3</doi><tpages>6</tpages></addata></record> |
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| language | eng |
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| subjects | Body centered cubic lattice Characterization and Evaluation of Materials Close packed lattices Condensed Matter Physics Hexagonal cells Inclusions Liquids Magnetic Materials Magnetism Nuclear magnetic resonance Physics Physics and Astronomy Spin-lattice relaxation Vitrification |
| title | Vitrification of Liquid Inclusions in hcp 3He-4He Crystal: the Role of an Intermediate bcc Phase |
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