Investigations on crystal growth, structural, optical, dielectric, mechanical and thermal properties of a novel optical crystal: Nicotinium nitrate monohydrate
Nicotinium nitrate monohydrate (NNM), a novel optical material, was synthesized and its crystals were grown from an aqueous solution. The solubility and metastable zone-width of NNM were found. Single-crystal X-ray diffraction analysis was used to estimate the cell parameters of the grown crystal. T...
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| Veröffentlicht in: | Journal of crystal growth 2011-03, Vol.318 (1), p.974-978 |
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| container_title | Journal of crystal growth |
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| creator | Dhanaraj, P.V. Rajesh, N.P. |
| description | Nicotinium nitrate monohydrate (NNM), a novel optical material, was synthesized and its crystals were grown from an aqueous solution. The solubility and metastable zone-width of NNM were found. Single-crystal X-ray diffraction analysis was used to estimate the cell parameters of the grown crystal. The structural perfection of crystals has been analyzed using high-resolution X-ray diffraction rocking curve measurements. Functional groups in NNM were identified by Fourier transform infrared spectral analysis. Thermal behavior and stability of NNM were studied by thermogravimetric and differential thermal analyses and differential scanning calorimetry. Mechanical and dielectric properties of NNM crystals were analyzed. Optical studies reveal that NNM crystals are transparent in the wavelength range 308–1100nm. The third order nonlinear optical parameters of NNM were derived by the Z-scan technique. |
| doi_str_mv | 10.1016/j.jcrysgro.2010.10.178 |
| format | Article |
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The solubility and metastable zone-width of NNM were found. Single-crystal X-ray diffraction analysis was used to estimate the cell parameters of the grown crystal. The structural perfection of crystals has been analyzed using high-resolution X-ray diffraction rocking curve measurements. Functional groups in NNM were identified by Fourier transform infrared spectral analysis. Thermal behavior and stability of NNM were studied by thermogravimetric and differential thermal analyses and differential scanning calorimetry. Mechanical and dielectric properties of NNM crystals were analyzed. Optical studies reveal that NNM crystals are transparent in the wavelength range 308–1100nm. 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The solubility and metastable zone-width of NNM were found. Single-crystal X-ray diffraction analysis was used to estimate the cell parameters of the grown crystal. The structural perfection of crystals has been analyzed using high-resolution X-ray diffraction rocking curve measurements. Functional groups in NNM were identified by Fourier transform infrared spectral analysis. Thermal behavior and stability of NNM were studied by thermogravimetric and differential thermal analyses and differential scanning calorimetry. Mechanical and dielectric properties of NNM crystals were analyzed. Optical studies reveal that NNM crystals are transparent in the wavelength range 308–1100nm. The third order nonlinear optical parameters of NNM were derived by the Z-scan technique.</description><subject>A1. High-resolution X-ray diffraction</subject><subject>A1. Solubility</subject><subject>A2. Growth from solutions</subject><subject>A2. Single crystal growth</subject><subject>B2. Dielectric materials</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Crystal growth</subject><subject>Crystal structure</subject><subject>Crystals</subject><subject>Dielectric properties</subject><subject>Diffraction</subject><subject>Equations of state, phase equilibria, and phase transitions</subject><subject>Exact sciences and technology</subject><subject>Growth from solutions</subject><subject>Materials science</subject><subject>Methods of crystal growth; physics of crystal growth</subject><subject>Nitrates</subject><subject>Optical properties</subject><subject>Physics</subject><subject>Solubility, segregation, and mixing; phase separation</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><subject>Thermal expansion; thermomechanical effects and density</subject><subject>Thermal properties of condensed matter</subject><subject>Thermal properties of crystalline solids</subject><subject>X-rays</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNqFUcGOFCEQJUYTx9VfMFxMPEyPQNNAe9JsdHeTjV72Thi62GHSDSPQY-Zr_FXpnR2vXqBSqfde1XsIvadkQwkVn_abvU2n_JjihpGn5oZK9QKtqJJt0xHCXqJVfVlDGFev0Zuc94RUJCUr9OcuHCEX_2iKjyHjGPBCVsyIK-HvslvjXNJsy5zMuMbxULxdisHDCLYkb9d4ArszYeljEwZcdpCmWh9SPEAqHiqrwwaHeITxwnBR-Yx_eBuLD36ecPAlmQJ4iiHuTsNSv0WvnBkzvHv-r9DD928P17fN_c-bu-uv941tZVcaaYehFT1slePEGMGccIwzQ1vlui0hW6d6xzlnijkyqF52WyF7TvpqhJGivUIfz7R16V9zNURPPlsYRxMgzllTISlXXLW0jorzqE0x5wROH5KfTDppSvQSiN7rSyB6CeSpL1UFfnjWMLk64JIJ1ud_aMYJ6wRZdvlynoN679FD0tl6CBYGn6rleoj-f1J_Acm5qOM</recordid><startdate>20110301</startdate><enddate>20110301</enddate><creator>Dhanaraj, P.V.</creator><creator>Rajesh, N.P.</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20110301</creationdate><title>Investigations on crystal growth, structural, optical, dielectric, mechanical and thermal properties of a novel optical crystal: Nicotinium nitrate monohydrate</title><author>Dhanaraj, P.V. ; Rajesh, N.P.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c375t-7cdd369eb8f40aa62f6f242a138f5b00bf89f444282f0d8975b679409000a763</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>A1. High-resolution X-ray diffraction</topic><topic>A1. Solubility</topic><topic>A2. Growth from solutions</topic><topic>A2. Single crystal growth</topic><topic>B2. 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| source | Elsevier ScienceDirect Journals |
| subjects | A1. High-resolution X-ray diffraction A1. Solubility A2. Growth from solutions A2. Single crystal growth B2. Dielectric materials Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Crystal growth Crystal structure Crystals Dielectric properties Diffraction Equations of state, phase equilibria, and phase transitions Exact sciences and technology Growth from solutions Materials science Methods of crystal growth physics of crystal growth Nitrates Optical properties Physics Solubility, segregation, and mixing phase separation Structure of solids and liquids crystallography Structure of specific crystalline solids Thermal expansion thermomechanical effects and density Thermal properties of condensed matter Thermal properties of crystalline solids X-rays |
| title | Investigations on crystal growth, structural, optical, dielectric, mechanical and thermal properties of a novel optical crystal: Nicotinium nitrate monohydrate |
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