Orthogonal design study on factors affecting the degradation of polylactic acid fibers of melt electrospinning
Melt electrospinning is a much simpler and safer method in the production of ultra‐fine fibers compared with solution electrospinning. However, high‐spinning temperature usually leads to serious degradation of polymer materials. In determining factors that affect the relative molecular mass of polyl...
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| Veröffentlicht in: | Journal of applied polymer science 2012-08, Vol.125 (4), p.2652-2658 |
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| creator | Zhao, Fengwen Liu, Yong Yuan, Huilin Yang, Weimin |
| description | Melt electrospinning is a much simpler and safer method in the production of ultra‐fine fibers compared with solution electrospinning. However, high‐spinning temperature usually leads to serious degradation of polymer materials. In determining factors that affect the relative molecular mass of polylactic acid (PLA) fibers during melt electrospinning, an orthogonal design method was used to examine the influence of melting temperature, spinning distance, and species and content of antioxidants. Results showed that antioxidant content at the present three levels (i.e., 0.1%, 0.3%, and 0.5%) has the most considerable effect on the relative molecular mass of PLA fibers. Error analysis showed that changes in temperature, distance, and antioxidant content influence the experiment's results significantly. All interaction effects were larger than those of the single factor in the experimental results. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012 |
| doi_str_mv | 10.1002/app.36426 |
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However, high‐spinning temperature usually leads to serious degradation of polymer materials. In determining factors that affect the relative molecular mass of polylactic acid (PLA) fibers during melt electrospinning, an orthogonal design method was used to examine the influence of melting temperature, spinning distance, and species and content of antioxidants. Results showed that antioxidant content at the present three levels (i.e., 0.1%, 0.3%, and 0.5%) has the most considerable effect on the relative molecular mass of PLA fibers. Error analysis showed that changes in temperature, distance, and antioxidant content influence the experiment's results significantly. All interaction effects were larger than those of the single factor in the experimental results. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012</description><identifier>ISSN: 0021-8995</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.36426</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc., A Wiley Company</publisher><subject>antioxidant ; Antioxidants ; Applied sciences ; Compounding ingredients ; Degradation ; Design engineering ; Design factors ; Electrospinning ; Exact sciences and technology ; Fibers ; Fibers and threads ; Forms of application and semi-finished materials ; Materials science ; melt electrospinning ; Melts ; Polylactic acid ; Polymer industry, paints, wood ; Polymers ; relative molecular mass ; Stabilizers (antioxydants, antiozonants, etc.) ; Technology of polymers</subject><ispartof>Journal of applied polymer science, 2012-08, Vol.125 (4), p.2652-2658</ispartof><rights>Copyright © 2012 Wiley Periodicals, Inc.</rights><rights>2014 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4356-8443524a5e4f24cff94cc1f3a6cb02fc2181c0752d0e9022499c6b2ad98cb4b63</citedby><cites>FETCH-LOGICAL-c4356-8443524a5e4f24cff94cc1f3a6cb02fc2181c0752d0e9022499c6b2ad98cb4b63</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.36426$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.36426$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1417,27924,27925,45574,45575</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=25911500$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhao, Fengwen</creatorcontrib><creatorcontrib>Liu, Yong</creatorcontrib><creatorcontrib>Yuan, Huilin</creatorcontrib><creatorcontrib>Yang, Weimin</creatorcontrib><title>Orthogonal design study on factors affecting the degradation of polylactic acid fibers of melt electrospinning</title><title>Journal of applied polymer science</title><addtitle>J. Appl. Polym. Sci</addtitle><description>Melt electrospinning is a much simpler and safer method in the production of ultra‐fine fibers compared with solution electrospinning. However, high‐spinning temperature usually leads to serious degradation of polymer materials. In determining factors that affect the relative molecular mass of polylactic acid (PLA) fibers during melt electrospinning, an orthogonal design method was used to examine the influence of melting temperature, spinning distance, and species and content of antioxidants. Results showed that antioxidant content at the present three levels (i.e., 0.1%, 0.3%, and 0.5%) has the most considerable effect on the relative molecular mass of PLA fibers. Error analysis showed that changes in temperature, distance, and antioxidant content influence the experiment's results significantly. All interaction effects were larger than those of the single factor in the experimental results. © 2012 Wiley Periodicals, Inc. J Appl Polym Sci, 2012</description><subject>antioxidant</subject><subject>Antioxidants</subject><subject>Applied sciences</subject><subject>Compounding ingredients</subject><subject>Degradation</subject><subject>Design engineering</subject><subject>Design factors</subject><subject>Electrospinning</subject><subject>Exact sciences and technology</subject><subject>Fibers</subject><subject>Fibers and threads</subject><subject>Forms of application and semi-finished materials</subject><subject>Materials science</subject><subject>melt electrospinning</subject><subject>Melts</subject><subject>Polylactic acid</subject><subject>Polymer industry, paints, wood</subject><subject>Polymers</subject><subject>relative molecular mass</subject><subject>Stabilizers (antioxydants, antiozonants, etc.)</subject><subject>Technology of polymers</subject><issn>0021-8995</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNp10E9rFDEYBvAgFlxrD36DgAh6mDb_Z3IsS22FxfawrceQySTb1GwyJll0v31Tt_YgeMrh_T0P5AHgPUanGCFypuf5lApGxCuwwEj2HRNkeA0W7Ya7QUr-Brwt5QEhjDkSCxCvc71PmxR1gJMtfhNhqbtpD1OETpuacoHaOWuqjxtY721Tm6wnXX0TycE5hX1o0BuojZ-g86NtmXbZ2lChDS2aU5l9jK3hHThyOhR78vweg9svF-vlVbe6vvy6PF91hlEuuoG1hzDNLXOEGeckMwY7qoUZEXGG4AEb1HMyISsRIUxKI0aiJzmYkY2CHoNPh945p587W6ra-mJsCDratCsKix4zyrCQjX74hz6kXW57NEU5ZT3vCW3q80GZ9pmSrVNz9lud9woj9bS8asurP8s3-_G5URejg8s6Gl9eAoTLp_FRc2cH98sHu_9_oTq_ufnb3B0SvlT7-yWh8w8letpz9f3bpVqt12u5Wt4pSh8Bjzih0w</recordid><startdate>20120815</startdate><enddate>20120815</enddate><creator>Zhao, Fengwen</creator><creator>Liu, Yong</creator><creator>Yuan, Huilin</creator><creator>Yang, Weimin</creator><general>Wiley Subscription Services, Inc., A Wiley Company</general><general>Wiley</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>FR3</scope><scope>KR7</scope></search><sort><creationdate>20120815</creationdate><title>Orthogonal design study on factors affecting the degradation of polylactic acid fibers of melt electrospinning</title><author>Zhao, Fengwen ; Liu, Yong ; Yuan, Huilin ; Yang, Weimin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4356-8443524a5e4f24cff94cc1f3a6cb02fc2181c0752d0e9022499c6b2ad98cb4b63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>antioxidant</topic><topic>Antioxidants</topic><topic>Applied sciences</topic><topic>Compounding ingredients</topic><topic>Degradation</topic><topic>Design engineering</topic><topic>Design factors</topic><topic>Electrospinning</topic><topic>Exact sciences and technology</topic><topic>Fibers</topic><topic>Fibers and threads</topic><topic>Forms of application and semi-finished materials</topic><topic>Materials science</topic><topic>melt electrospinning</topic><topic>Melts</topic><topic>Polylactic acid</topic><topic>Polymer industry, paints, wood</topic><topic>Polymers</topic><topic>relative molecular mass</topic><topic>Stabilizers (antioxydants, antiozonants, etc.)</topic><topic>Technology of polymers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhao, Fengwen</creatorcontrib><creatorcontrib>Liu, Yong</creatorcontrib><creatorcontrib>Yuan, Huilin</creatorcontrib><creatorcontrib>Yang, Weimin</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Engineering Research Database</collection><collection>Civil Engineering Abstracts</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhao, Fengwen</au><au>Liu, Yong</au><au>Yuan, Huilin</au><au>Yang, Weimin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Orthogonal design study on factors affecting the degradation of polylactic acid fibers of melt electrospinning</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. 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| subjects | antioxidant Antioxidants Applied sciences Compounding ingredients Degradation Design engineering Design factors Electrospinning Exact sciences and technology Fibers Fibers and threads Forms of application and semi-finished materials Materials science melt electrospinning Melts Polylactic acid Polymer industry, paints, wood Polymers relative molecular mass Stabilizers (antioxydants, antiozonants, etc.) Technology of polymers |
| title | Orthogonal design study on factors affecting the degradation of polylactic acid fibers of melt electrospinning |
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