Annealing and recrystallization of amorphous ZnO thin films deposited under cryogenic conditions by pulsed laser deposition

This article deals with the annealing of amorphous ZnO thin films prepared by pulsed laser deposition (PLD) under cryogenic conditions. The substrate holder was cooled by liquid nitrogen. X-ray diffraction analysis evidenced that as-deposited films had amorphous structures: analysis by scanning elec...

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Veröffentlicht in:Thin solid films 2011-11, Vol.520 (2), p.866-870
Hauptverfasser: Bruncko, J., Vincze, A., Netrvalova, M., Šutta, P., Hasko, D., Michalka, M.
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container_end_page 870
container_issue 2
container_start_page 866
container_title Thin solid films
container_volume 520
creator Bruncko, J.
Vincze, A.
Netrvalova, M.
Šutta, P.
Hasko, D.
Michalka, M.
description This article deals with the annealing of amorphous ZnO thin films prepared by pulsed laser deposition (PLD) under cryogenic conditions. The substrate holder was cooled by liquid nitrogen. X-ray diffraction analysis evidenced that as-deposited films had amorphous structures: analysis by scanning electron microscopy (SEM) revealed their fine grained surface and inner structure. Annealing at temperatures in the range of 200–800 °C resulted in a transition in the thin film crystal structure from amorphous to polycrystalline. Various properties of the ZnO films were found depending on the recrystallization temperature. In depth investigations employing SEM, X-ray diffraction, atomic force microscopy and secondary ion mass spectroscopy provided comparisons of the recrystallizations of undoped ZnO thin films during the phase transition processes from amorphous to hexagonal wurtzite structures.
doi_str_mv 10.1016/j.tsf.2011.04.202
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subjects Amorphous structure
Annealing
Condensed matter: structure, mechanical and thermal properties
Cross-disciplinary physics: materials science
rheology
Cryogenic temperature
Diffraction
Electron, ion, and scanning probe microscopy
Exact sciences and technology
Laser deposition
Materials science
Methods of deposition of films and coatings
film growth and epitaxy
Physics
Pulsed laser deposition
Recrystallization
Scanning electron microscopy
Structure and morphology
thickness
Structure of solids and liquids
crystallography
Surfaces and interfaces
thin films and whiskers (structure and nonelectronic properties)
Thin film structure and morphology
Thin films
X-rays
Zinc oxide
title Annealing and recrystallization of amorphous ZnO thin films deposited under cryogenic conditions by pulsed laser deposition
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