Rapid Hydrothermal Synthesis of Zinc Oxide Nanowires by Annealing Methods on Seed Layers
Well-aligned zinc oxide (ZnO) nanowire arrays were successfully synthesized on a glass substrate using the rapid microwave heating process. The ZnO seed layers were produced by spinning the precursor solutions onto the substrate. Among coatings, the ZnO seed layers were annealed at 100°C for 5 minut...
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| Veröffentlicht in: | Journal of nanomaterials 2011-01, Vol.2011 (2011), p.1-6 |
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| creator | Shim, Jang Bo Chang, Hyuk Kim, Sung-O |
| description | Well-aligned zinc oxide (ZnO) nanowire arrays were successfully synthesized on a glass substrate using the rapid microwave heating process. The ZnO seed layers were produced by spinning the precursor solutions onto the substrate. Among coatings, the ZnO seed layers were annealed at 100°C for 5 minutes to ensure particle adhesion to the glass surface in air, nitrogen, and vacuum atmospheres. The annealing treatment of the ZnO seed layer was most important for achieving the high quality of ZnO nanowire arrays as ZnO seed nanoparticles of larger than 30 nm in diameter evolve into ZnO nanowire arrays. Transmission electron microscopy analysis revealed a single-crystalline lattice of the ZnO nanowires. Because of their low power (140 W), low operating temperatures (90°C), easy fabrication (variable microwave sintering system), and low cost (90% cost reduction compared with gas condensation methods), high quality ZnO nanowires created with the rapid microwave heating process show great promise for use in flexible solar cells and flexible display devices. |
| doi_str_mv | 10.1155/2011/582764 |
| format | Article |
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The ZnO seed layers were produced by spinning the precursor solutions onto the substrate. Among coatings, the ZnO seed layers were annealed at 100°C for 5 minutes to ensure particle adhesion to the glass surface in air, nitrogen, and vacuum atmospheres. The annealing treatment of the ZnO seed layer was most important for achieving the high quality of ZnO nanowire arrays as ZnO seed nanoparticles of larger than 30 nm in diameter evolve into ZnO nanowire arrays. Transmission electron microscopy analysis revealed a single-crystalline lattice of the ZnO nanowires. Because of their low power (140 W), low operating temperatures (90°C), easy fabrication (variable microwave sintering system), and low cost (90% cost reduction compared with gas condensation methods), high quality ZnO nanowires created with the rapid microwave heating process show great promise for use in flexible solar cells and flexible display devices.</description><identifier>ISSN: 1687-4110</identifier><identifier>EISSN: 1687-4129</identifier><identifier>DOI: 10.1155/2011/582764</identifier><language>eng</language><publisher>Cairo, Egypt: Hindawi Puplishing Corporation</publisher><subject>Annealing ; Arrays ; Atmospheric pressure ; Crystal structure ; Heating ; Investigations ; Methods ; Microwave heating ; Microwaves ; Nanomaterials ; Nanoparticles ; Nanowires ; Operating temperature ; Optics ; Scanning electron microscopy ; Seeds ; Solution chemistry ; Temperature ; Vacancies ; Zinc oxide</subject><ispartof>Journal of nanomaterials, 2011-01, Vol.2011 (2011), p.1-6</ispartof><rights>Copyright © 2011 Jang Bo Shim et al.</rights><rights>Copyright © 2011 Jang Bo Shim et al. Jang Bo Shim et al. This is an open access article distributed under the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a460t-c895bb33cf0359086235295fc0adf26a24dbb0bb05a53bdad0d6d0ac05779df93</citedby><cites>FETCH-LOGICAL-a460t-c895bb33cf0359086235295fc0adf26a24dbb0bb05a53bdad0d6d0ac05779df93</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><contributor>ChunXiang, Cui</contributor><creatorcontrib>Shim, Jang Bo</creatorcontrib><creatorcontrib>Chang, Hyuk</creatorcontrib><creatorcontrib>Kim, Sung-O</creatorcontrib><title>Rapid Hydrothermal Synthesis of Zinc Oxide Nanowires by Annealing Methods on Seed Layers</title><title>Journal of nanomaterials</title><description>Well-aligned zinc oxide (ZnO) nanowire arrays were successfully synthesized on a glass substrate using the rapid microwave heating process. The ZnO seed layers were produced by spinning the precursor solutions onto the substrate. Among coatings, the ZnO seed layers were annealed at 100°C for 5 minutes to ensure particle adhesion to the glass surface in air, nitrogen, and vacuum atmospheres. The annealing treatment of the ZnO seed layer was most important for achieving the high quality of ZnO nanowire arrays as ZnO seed nanoparticles of larger than 30 nm in diameter evolve into ZnO nanowire arrays. Transmission electron microscopy analysis revealed a single-crystalline lattice of the ZnO nanowires. Because of their low power (140 W), low operating temperatures (90°C), easy fabrication (variable microwave sintering system), and low cost (90% cost reduction compared with gas condensation methods), high quality ZnO nanowires created with the rapid microwave heating process show great promise for use in flexible solar cells and flexible display devices.</description><subject>Annealing</subject><subject>Arrays</subject><subject>Atmospheric pressure</subject><subject>Crystal structure</subject><subject>Heating</subject><subject>Investigations</subject><subject>Methods</subject><subject>Microwave heating</subject><subject>Microwaves</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Nanowires</subject><subject>Operating temperature</subject><subject>Optics</subject><subject>Scanning electron microscopy</subject><subject>Seeds</subject><subject>Solution chemistry</subject><subject>Temperature</subject><subject>Vacancies</subject><subject>Zinc oxide</subject><issn>1687-4110</issn><issn>1687-4129</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>RHX</sourceid><sourceid>BENPR</sourceid><recordid>eNqF0M9LwzAUB_AgCs7pybMQPIkylx9N2h7HUCdMB05BvIS0SVxGl86kY_a_N6OygxfhwfsePjweXwDOMbrFmLEhQRgPWUZSnhyAHuZZOkgwyQ_3GaNjcBLCEqGE5Yz0wPuLXFsFJ63ydbPQfiUrOG9djMEGWBv4YV0JZ99WafgsXb21XgdYtHDknJaVdZ_wSTeLWkXs4FxrBaey1T6cgiMjq6DPfncfvN3fvY4ng-ns4XE8mg5kwlEzKLOcFQWlpUGU5SjjhDKSM1MiqQzhkiSqKFAcJhktlFRIcYVkiVia5srktA-uurtrX39tdGjEyoZSV5V0ut4EgXmKSUJZsqOXf-iy3ngXvxNZSlPGGaMR3XSo9HUIXhux9nYlfSswEruSxa5k0ZUc9XWnF9YpubX_4IsO60i0kXucZITHH38ABBWEkQ</recordid><startdate>20110101</startdate><enddate>20110101</enddate><creator>Shim, Jang Bo</creator><creator>Chang, Hyuk</creator><creator>Kim, Sung-O</creator><general>Hindawi Puplishing Corporation</general><general>Hindawi Publishing Corporation</general><general>Hindawi Limited</general><scope>ADJCN</scope><scope>AHFXO</scope><scope>RHU</scope><scope>RHW</scope><scope>RHX</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>CWDGH</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>F28</scope><scope>FR3</scope></search><sort><creationdate>20110101</creationdate><title>Rapid Hydrothermal Synthesis of Zinc Oxide Nanowires by Annealing Methods on Seed Layers</title><author>Shim, Jang Bo ; 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| source | Wiley Online Library Open Access; EZB-FREE-00999 freely available EZB journals; Alma/SFX Local Collection; Free Full-Text Journals in Chemistry |
| subjects | Annealing Arrays Atmospheric pressure Crystal structure Heating Investigations Methods Microwave heating Microwaves Nanomaterials Nanoparticles Nanowires Operating temperature Optics Scanning electron microscopy Seeds Solution chemistry Temperature Vacancies Zinc oxide |
| title | Rapid Hydrothermal Synthesis of Zinc Oxide Nanowires by Annealing Methods on Seed Layers |
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