The influence of Si concentrations on the oxidation resistance of Mo-Si-B-(N) coatings
The influence of the silicon concentration on the oxidation resistance of Mo-Si-B-N coatings prepared by magnetron sputtering is investigated. The Si content in them was controlled by the composite-target composition, as well as by various areas of silicon segments placed into the target-erosion zon...
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| Veröffentlicht in: | Russian journal of non-ferrous metals 2014-11, Vol.55 (6), p.645-651 |
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| container_title | Russian journal of non-ferrous metals |
| container_volume | 55 |
| creator | Kiryukhantsev-Korneev, Ph. V. Andreev, S. O. Shvyndina, N. V. Levashov, E. A. Timofeev, A. N. Shtansky, D. V. |
| description | The influence of the silicon concentration on the oxidation resistance of Mo-Si-B-N coatings prepared by magnetron sputtering is investigated. The Si content in them was controlled by the composite-target composition, as well as by various areas of silicon segments placed into the target-erosion zone. The composition and structure of coatings after deposition and annealing in air at temperatures of 500–1300°C are investigated using transmission and scanning electron microscopy, energy-dispersive analysis, and glow-discharge optical emission spectroscopy. It is established that oxidation resistance increases as the Si concentration in coatings increases, which is caused by the formation of a silicon oxide-based dense layer; this layer prevents oxygen propagation into the coating depth upon heating. The maximal oxidation resistance at a level of 1300°C is attained in Mo-Si-B-N coatings containing 40 at % Si. |
| doi_str_mv | 10.3103/S106782121406011X |
| format | Article |
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It is established that oxidation resistance increases as the Si concentration in coatings increases, which is caused by the formation of a silicon oxide-based dense layer; this layer prevents oxygen propagation into the coating depth upon heating. 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The composition and structure of coatings after deposition and annealing in air at temperatures of 500–1300°C are investigated using transmission and scanning electron microscopy, energy-dispersive analysis, and glow-discharge optical emission spectroscopy. It is established that oxidation resistance increases as the Si concentration in coatings increases, which is caused by the formation of a silicon oxide-based dense layer; this layer prevents oxygen propagation into the coating depth upon heating. The maximal oxidation resistance at a level of 1300°C is attained in Mo-Si-B-N coatings containing 40 at % Si.</description><subject>Chemistry and Materials Science</subject><subject>Coatings</subject><subject>Concentration (composition)</subject><subject>Deposition</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Molybdenum</subject><subject>Nanostructured Materials and Functional Coatings</subject><subject>Nonferrous metals</subject><subject>Optical emission spectroscopy</subject><subject>Oxidation resistance</subject><subject>Segments</subject><subject>Silicon</subject><issn>1067-8212</issn><issn>1934-970X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNp1kD1PwzAQhi0EEqXwA9gisZQhcBc7cTxCxZdUYGhB3SLXcYqr1i52IsG_x6UdEIjJ57vnOZ1eQk4RLigCvRwjFLzMMEMGBSBO90gPBWWp4DDdj3Ucp5v5ITkKYQGQ5yIXPfI6edOJsc2y01bpxDXJ2CTKxdq2XrbG2ZA4m7SRch-m_u4kXgcTWrkTHl06Nul1Ong6j2Yk7Dwck4NGLoM-2b198nJ7Mxnep6Pnu4fh1ShVlIk2pQ3SjAPmrMYZL0FxITmCaqAuC6wzVdaMMTGLf54pKXjelCVKAZrXqmRA-2Sw3bv27r3Toa1WJii9XEqrXRcqLAoAwSmIiJ79Qheu8zZeFykWQyzyLIsUbinlXQheN9Xam5X0nxVCtUm6-pN0dLKtEyJr59r_2Pyv9AUaW32N</recordid><startdate>20141101</startdate><enddate>20141101</enddate><creator>Kiryukhantsev-Korneev, Ph. 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Non-ferrous Metals</stitle><date>2014-11-01</date><risdate>2014</risdate><volume>55</volume><issue>6</issue><spage>645</spage><epage>651</epage><pages>645-651</pages><issn>1067-8212</issn><eissn>1934-970X</eissn><abstract>The influence of the silicon concentration on the oxidation resistance of Mo-Si-B-N coatings prepared by magnetron sputtering is investigated. The Si content in them was controlled by the composite-target composition, as well as by various areas of silicon segments placed into the target-erosion zone. The composition and structure of coatings after deposition and annealing in air at temperatures of 500–1300°C are investigated using transmission and scanning electron microscopy, energy-dispersive analysis, and glow-discharge optical emission spectroscopy. It is established that oxidation resistance increases as the Si concentration in coatings increases, which is caused by the formation of a silicon oxide-based dense layer; this layer prevents oxygen propagation into the coating depth upon heating. The maximal oxidation resistance at a level of 1300°C is attained in Mo-Si-B-N coatings containing 40 at % Si.</abstract><cop>Heidelberg</cop><pub>Allerton Press</pub><doi>10.3103/S106782121406011X</doi><tpages>7</tpages></addata></record> |
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| ispartof | Russian journal of non-ferrous metals, 2014-11, Vol.55 (6), p.645-651 |
| issn | 1067-8212 1934-970X |
| language | eng |
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| source | SpringerNature Complete Journals |
| subjects | Chemistry and Materials Science Coatings Concentration (composition) Deposition Materials Science Metallic Materials Molybdenum Nanostructured Materials and Functional Coatings Nonferrous metals Optical emission spectroscopy Oxidation resistance Segments Silicon |
| title | The influence of Si concentrations on the oxidation resistance of Mo-Si-B-(N) coatings |
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