Synthetic Ni-talc as filler for producing polyurethane nanocomposites
ABSTRACT New synthetic Ni‐talc was used as filler in the synthesis of polyurethane (PU) nanocomposites by in situ polymerization and to emphasize the contribution of the new material compared with natural talc. Good dispersion of Ni‐talc was supported by homogeneous green coloration observed in the...
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| Veröffentlicht in: | Journal of applied polymer science 2015-04, Vol.132 (16), p.np-n/a |
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| container_title | Journal of applied polymer science |
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| creator | Prado, Manoela Argenton Dias, Guilherme Carone, Carlos Ligabue, Rosane Dumas, Angela Le Roux, Christophe Micoud, Pierre Martin, François Einloft, Sandra |
| description | ABSTRACT
New synthetic Ni‐talc was used as filler in the synthesis of polyurethane (PU) nanocomposites by in situ polymerization and to emphasize the contribution of the new material compared with natural talc. Good dispersion of Ni‐talc was supported by homogeneous green coloration observed in the polymer matrix. X‐ray diffraction (XRD) analyses indicate the intercalation of polymeric matrix into the filler layers by the increase in d001‐spacing value of the Ni‐talc for the nanocomposites when compared to the pristine filler. The nanocomposites obtained with synthetic talc showed an improvement in the crystallization temperature and in thermal stability when compared to pure PU and the composite obtained with natural talc. The young modulus of PU/talc materials containing both Ni‐talc and natural talc were slight higher than pure PU. As shown by scanning electron microscope (SEM), Ni‐talc fillers were well dispersed into the polymeric matrix probably due to the good compatibility of both phases filler/polymer mainly achieved by the filler OH interaction with the urethane group of the polymeric chain. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015, 132, 41854. |
| doi_str_mv | 10.1002/app.41854 |
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New synthetic Ni‐talc was used as filler in the synthesis of polyurethane (PU) nanocomposites by in situ polymerization and to emphasize the contribution of the new material compared with natural talc. Good dispersion of Ni‐talc was supported by homogeneous green coloration observed in the polymer matrix. X‐ray diffraction (XRD) analyses indicate the intercalation of polymeric matrix into the filler layers by the increase in d001‐spacing value of the Ni‐talc for the nanocomposites when compared to the pristine filler. The nanocomposites obtained with synthetic talc showed an improvement in the crystallization temperature and in thermal stability when compared to pure PU and the composite obtained with natural talc. The young modulus of PU/talc materials containing both Ni‐talc and natural talc were slight higher than pure PU. As shown by scanning electron microscope (SEM), Ni‐talc fillers were well dispersed into the polymeric matrix probably due to the good compatibility of both phases filler/polymer mainly achieved by the filler OH interaction with the urethane group of the polymeric chain. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015, 132, 41854.</description><identifier>ISSN: 0021-8995</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.41854</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Blackwell Publishing Ltd</publisher><subject>composites ; Fillers ; Materials science ; mechanical properties ; Nanocomposites ; nanoparticles ; nanowires and nanocrystals ; Nickel ; Polymerization ; Polymers ; Polyurethane resins ; Scanning electron microscopy ; Talcs</subject><ispartof>Journal of applied polymer science, 2015-04, Vol.132 (16), p.np-n/a</ispartof><rights>2014 Wiley Periodicals, Inc.</rights><rights>2015 Wiley Periodicals, Inc.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4054-6c11d12977968380afaf37e06ba1630ab41bbc98e017733f751b969ffe6af81f3</citedby><cites>FETCH-LOGICAL-c4054-6c11d12977968380afaf37e06ba1630ab41bbc98e017733f751b969ffe6af81f3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.41854$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.41854$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids></links><search><creatorcontrib>Prado, Manoela Argenton</creatorcontrib><creatorcontrib>Dias, Guilherme</creatorcontrib><creatorcontrib>Carone, Carlos</creatorcontrib><creatorcontrib>Ligabue, Rosane</creatorcontrib><creatorcontrib>Dumas, Angela</creatorcontrib><creatorcontrib>Le Roux, Christophe</creatorcontrib><creatorcontrib>Micoud, Pierre</creatorcontrib><creatorcontrib>Martin, François</creatorcontrib><creatorcontrib>Einloft, Sandra</creatorcontrib><title>Synthetic Ni-talc as filler for producing polyurethane nanocomposites</title><title>Journal of applied polymer science</title><addtitle>J. Appl. Polym. Sci</addtitle><description>ABSTRACT
New synthetic Ni‐talc was used as filler in the synthesis of polyurethane (PU) nanocomposites by in situ polymerization and to emphasize the contribution of the new material compared with natural talc. Good dispersion of Ni‐talc was supported by homogeneous green coloration observed in the polymer matrix. X‐ray diffraction (XRD) analyses indicate the intercalation of polymeric matrix into the filler layers by the increase in d001‐spacing value of the Ni‐talc for the nanocomposites when compared to the pristine filler. The nanocomposites obtained with synthetic talc showed an improvement in the crystallization temperature and in thermal stability when compared to pure PU and the composite obtained with natural talc. The young modulus of PU/talc materials containing both Ni‐talc and natural talc were slight higher than pure PU. As shown by scanning electron microscope (SEM), Ni‐talc fillers were well dispersed into the polymeric matrix probably due to the good compatibility of both phases filler/polymer mainly achieved by the filler OH interaction with the urethane group of the polymeric chain. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015, 132, 41854.</description><subject>composites</subject><subject>Fillers</subject><subject>Materials science</subject><subject>mechanical properties</subject><subject>Nanocomposites</subject><subject>nanoparticles</subject><subject>nanowires and nanocrystals</subject><subject>Nickel</subject><subject>Polymerization</subject><subject>Polymers</subject><subject>Polyurethane resins</subject><subject>Scanning electron microscopy</subject><subject>Talcs</subject><issn>0021-8995</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><recordid>eNp10MlOwzAUBVALgUQZFvxBJDawSOvXJB6WVVUGiaGIUWwsx9jUJY2DnQj69xgKLJBYeeFzn64uQnuA-4DxcCCbpp8DK_I11APMaZqTIVtHvfgHKeO82ERbIcwxBigw6aHJ9bJuZ7q1KrmwaSsrlciQGFtV2ifG-aTx7qlTtn5OGlctO6_bmax1UsvaKbdoXLCtDjtow8gq6N3vdxvdHk1uxifp2eXx6Xh0lqocF3lKFMATDDmlnLCMYWmkyajGpJRAMizLHMpScaYxUJplhhZQcsKN0UQaBibbRgeru7HVa6dDKxY2KF1VsZLrggBCMOaYsWGk-3_o3HW-ju2iymksUQCP6nCllHcheG1E4-1C-qUALD4HFXFQ8TVotIOVfbOVXv4PxWg6_Umkq4QNrX7_TUj_IgjNaCHuL47F49X44YidT8Vd9gEgkYXp</recordid><startdate>20150420</startdate><enddate>20150420</enddate><creator>Prado, Manoela Argenton</creator><creator>Dias, Guilherme</creator><creator>Carone, Carlos</creator><creator>Ligabue, Rosane</creator><creator>Dumas, Angela</creator><creator>Le Roux, Christophe</creator><creator>Micoud, Pierre</creator><creator>Martin, François</creator><creator>Einloft, Sandra</creator><general>Blackwell Publishing Ltd</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>7U5</scope><scope>L7M</scope></search><sort><creationdate>20150420</creationdate><title>Synthetic Ni-talc as filler for producing polyurethane nanocomposites</title><author>Prado, Manoela Argenton ; Dias, Guilherme ; Carone, Carlos ; Ligabue, Rosane ; Dumas, Angela ; Le Roux, Christophe ; Micoud, Pierre ; Martin, François ; Einloft, Sandra</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4054-6c11d12977968380afaf37e06ba1630ab41bbc98e017733f751b969ffe6af81f3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2015</creationdate><topic>composites</topic><topic>Fillers</topic><topic>Materials science</topic><topic>mechanical properties</topic><topic>Nanocomposites</topic><topic>nanoparticles</topic><topic>nanowires and nanocrystals</topic><topic>Nickel</topic><topic>Polymerization</topic><topic>Polymers</topic><topic>Polyurethane resins</topic><topic>Scanning electron microscopy</topic><topic>Talcs</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Prado, Manoela Argenton</creatorcontrib><creatorcontrib>Dias, Guilherme</creatorcontrib><creatorcontrib>Carone, Carlos</creatorcontrib><creatorcontrib>Ligabue, Rosane</creatorcontrib><creatorcontrib>Dumas, Angela</creatorcontrib><creatorcontrib>Le Roux, Christophe</creatorcontrib><creatorcontrib>Micoud, Pierre</creatorcontrib><creatorcontrib>Martin, François</creatorcontrib><creatorcontrib>Einloft, Sandra</creatorcontrib><collection>Istex</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Prado, Manoela Argenton</au><au>Dias, Guilherme</au><au>Carone, Carlos</au><au>Ligabue, Rosane</au><au>Dumas, Angela</au><au>Le Roux, Christophe</au><au>Micoud, Pierre</au><au>Martin, François</au><au>Einloft, Sandra</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthetic Ni-talc as filler for producing polyurethane nanocomposites</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. Appl. Polym. Sci</addtitle><date>2015-04-20</date><risdate>2015</risdate><volume>132</volume><issue>16</issue><spage>np</spage><epage>n/a</epage><pages>np-n/a</pages><issn>0021-8995</issn><eissn>1097-4628</eissn><coden>JAPNAB</coden><abstract>ABSTRACT
New synthetic Ni‐talc was used as filler in the synthesis of polyurethane (PU) nanocomposites by in situ polymerization and to emphasize the contribution of the new material compared with natural talc. Good dispersion of Ni‐talc was supported by homogeneous green coloration observed in the polymer matrix. X‐ray diffraction (XRD) analyses indicate the intercalation of polymeric matrix into the filler layers by the increase in d001‐spacing value of the Ni‐talc for the nanocomposites when compared to the pristine filler. The nanocomposites obtained with synthetic talc showed an improvement in the crystallization temperature and in thermal stability when compared to pure PU and the composite obtained with natural talc. The young modulus of PU/talc materials containing both Ni‐talc and natural talc were slight higher than pure PU. As shown by scanning electron microscope (SEM), Ni‐talc fillers were well dispersed into the polymeric matrix probably due to the good compatibility of both phases filler/polymer mainly achieved by the filler OH interaction with the urethane group of the polymeric chain. © 2014 Wiley Periodicals, Inc. J. Appl. Polym. Sci. 2015, 132, 41854.</abstract><cop>Hoboken</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1002/app.41854</doi><tpages>8</tpages></addata></record> |
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| subjects | composites Fillers Materials science mechanical properties Nanocomposites nanoparticles nanowires and nanocrystals Nickel Polymerization Polymers Polyurethane resins Scanning electron microscopy Talcs |
| title | Synthetic Ni-talc as filler for producing polyurethane nanocomposites |
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