Mechanical characterization of polymeric thin films by atomic force microscopy based techniques
Polymeric thin films have been awakening continuous and growing interest for application in nanotechnology. For such applications, the assessment of their (nano)mechanical properties is a key issue, since they may dramatically vary between the bulk and the thin film state, even for the same polymer....
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| Veröffentlicht in: | Analytical and bioanalytical chemistry 2013-02, Vol.405 (5), p.1463-1478 |
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| container_title | Analytical and bioanalytical chemistry |
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| creator | Passeri, Daniele Rossi, Marco Tamburri, Emanuela Terranova, Maria Letizia |
| description | Polymeric thin films have been awakening continuous and growing interest for application in nanotechnology. For such applications, the assessment of their (nano)mechanical properties is a key issue, since they may dramatically vary between the bulk and the thin film state, even for the same polymer. Therefore, techniques are required for the in situ characterization of mechanical properties of thin films that must be nondestructive or only minimally destructive. Also, they must also be able to probe nanometer-thick ultrathin films and layers and capable of imaging the mechanical properties of the sample with nanometer lateral resolution, since, for instance, at these scales blends or copolymers are not uniform, their phases being separated. Atomic force microscopy (AFM) has been proposed as a tool for the development of a number of techniques that match such requirements. In this review, we describe the state of the art of the main AFM-based methods for qualitative and quantitative single-point measurements and imaging of mechanical properties of polymeric thin films, illustrating their specific merits and limitations. |
| doi_str_mv | 10.1007/s00216-012-6419-3 |
| format | Article |
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For such applications, the assessment of their (nano)mechanical properties is a key issue, since they may dramatically vary between the bulk and the thin film state, even for the same polymer. Therefore, techniques are required for the in situ characterization of mechanical properties of thin films that must be nondestructive or only minimally destructive. Also, they must also be able to probe nanometer-thick ultrathin films and layers and capable of imaging the mechanical properties of the sample with nanometer lateral resolution, since, for instance, at these scales blends or copolymers are not uniform, their phases being separated. Atomic force microscopy (AFM) has been proposed as a tool for the development of a number of techniques that match such requirements. 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For such applications, the assessment of their (nano)mechanical properties is a key issue, since they may dramatically vary between the bulk and the thin film state, even for the same polymer. Therefore, techniques are required for the in situ characterization of mechanical properties of thin films that must be nondestructive or only minimally destructive. Also, they must also be able to probe nanometer-thick ultrathin films and layers and capable of imaging the mechanical properties of the sample with nanometer lateral resolution, since, for instance, at these scales blends or copolymers are not uniform, their phases being separated. Atomic force microscopy (AFM) has been proposed as a tool for the development of a number of techniques that match such requirements. In this review, we describe the state of the art of the main AFM-based methods for qualitative and quantitative single-point measurements and imaging of mechanical properties of polymeric thin films, illustrating their specific merits and limitations.</description><subject>Analytical Chemistry</subject><subject>Atomic force microscopy</subject><subject>Biochemistry</subject><subject>Blends</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Dielectric films</subject><subject>Equipment Design</subject><subject>Food Science</subject><subject>Identification and classification</subject><subject>Imaging</subject><subject>Laboratory Medicine</subject><subject>Mechanical Phenomena</subject><subject>Mechanical properties</subject><subject>Methods</subject><subject>Microscopy</subject><subject>Microscopy, Atomic Force - instrumentation</subject><subject>Microscopy, Atomic Force - methods</subject><subject>Monitoring/Environmental Analysis</subject><subject>Morphology</subject><subject>Nanocomposites</subject><subject>Nanostructure</subject><subject>Nanotechnology</subject><subject>Oxidation</subject><subject>Polyethylene</subject><subject>Polymeric composites</subject><subject>Polymeric films</subject><subject>Polymers</subject><subject>Polymers - 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For such applications, the assessment of their (nano)mechanical properties is a key issue, since they may dramatically vary between the bulk and the thin film state, even for the same polymer. Therefore, techniques are required for the in situ characterization of mechanical properties of thin films that must be nondestructive or only minimally destructive. Also, they must also be able to probe nanometer-thick ultrathin films and layers and capable of imaging the mechanical properties of the sample with nanometer lateral resolution, since, for instance, at these scales blends or copolymers are not uniform, their phases being separated. Atomic force microscopy (AFM) has been proposed as a tool for the development of a number of techniques that match such requirements. 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| subjects | Analytical Chemistry Atomic force microscopy Biochemistry Blends Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Dielectric films Equipment Design Food Science Identification and classification Imaging Laboratory Medicine Mechanical Phenomena Mechanical properties Methods Microscopy Microscopy, Atomic Force - instrumentation Microscopy, Atomic Force - methods Monitoring/Environmental Analysis Morphology Nanocomposites Nanostructure Nanotechnology Oxidation Polyethylene Polymeric composites Polymeric films Polymers Polymers - chemistry Review Surface Properties Temperature Thin films |
| title | Mechanical characterization of polymeric thin films by atomic force microscopy based techniques |
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