Elastic Modulus Measurements on Large Diameter Nanowires Using a Nano-Assembled Platform
This paper presents atomic force spectroscopy (AFM) results from large diameter nanowires (NWs), which range in radius from 150 nm to 300 nm, within a nano-assembled platform. The nanomechanical platform is constructed by assembling single NWs across pairs of gold nano-electrodes using dielectrophor...
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creator | Palapati, Naveen K. R Muth, Adrienne Zhu, Yujie Wang, Chunsheng Subramanian, Arunkumar |
description | This paper presents atomic force spectroscopy (AFM) results from large diameter nanowires (NWs), which range in radius from 150 nm to 300 nm, within a nano-assembled platform. The nanomechanical platform is constructed by assembling single NWs across pairs of gold nano-electrodes using dielectrophoresis and contains a short, suspended segment of the NW (in air) between the assembly electrodes. Atomic force microscope (AFM) force spectroscopy measurements are obtained by indenting the NW within this suspended segment and result in deformation of the NW involving a combination of both, bending and nano-indentation modes. This paper demonstrates the measurement technique using lithium iron phosphate NWs as a model system and presents a finite element model to extract the Young's modulus from nanomechanical data. The estimated Young's modulus of this material, which is an electrode material system of interest for next-generation lithium-ion batteries, was found to be diameter dependent and was observed to range in values between 100 MPa and 575 MPa. |
doi_str_mv | 10.1115/1.4028045 |
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R ; Muth, Adrienne ; Zhu, Yujie ; Wang, Chunsheng ; Subramanian, Arunkumar</creator><creatorcontrib>Palapati, Naveen K. R ; Muth, Adrienne ; Zhu, Yujie ; Wang, Chunsheng ; Subramanian, Arunkumar ; Energy Frontier Research Centers (EFRC) ; Nanostructures for Electrical Energy Storage (NEES)</creatorcontrib><description>This paper presents atomic force spectroscopy (AFM) results from large diameter nanowires (NWs), which range in radius from 150 nm to 300 nm, within a nano-assembled platform. The nanomechanical platform is constructed by assembling single NWs across pairs of gold nano-electrodes using dielectrophoresis and contains a short, suspended segment of the NW (in air) between the assembly electrodes. Atomic force microscope (AFM) force spectroscopy measurements are obtained by indenting the NW within this suspended segment and result in deformation of the NW involving a combination of both, bending and nano-indentation modes. This paper demonstrates the measurement technique using lithium iron phosphate NWs as a model system and presents a finite element model to extract the Young's modulus from nanomechanical data. 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Atomic force microscope (AFM) force spectroscopy measurements are obtained by indenting the NW within this suspended segment and result in deformation of the NW involving a combination of both, bending and nano-indentation modes. This paper demonstrates the measurement technique using lithium iron phosphate NWs as a model system and presents a finite element model to extract the Young's modulus from nanomechanical data. The estimated Young's modulus of this material, which is an electrode material system of interest for next-generation lithium-ion batteries, was found to be diameter dependent and was observed to range in values between 100 MPa and 575 MPa.</description><subject>Atomic force microscopy</subject><subject>bio-inspired, energy storage (including batteries and capacitors), defects, charge transport, synthesis (novel materials), synthesis (self-assembly), synthesis (scalable processing)</subject><subject>Mathematical models</subject><subject>Modulus of elasticity</subject><subject>Nanostructure</subject><subject>Nanowires</subject><subject>Platforms</subject><subject>Segments</subject><subject>Spectroscopy</subject><issn>1949-2944</issn><issn>1949-2952</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqNkb1LxEAQxRdRUE8La5vFSovofibZ8vAb7tRCwW7Z7M1qjiR77iSI_73RO6xtZobhx4P3HiFHnJ1zzvUFP1dMlEzpLbLHjTKZMFps_91K7ZJ9xCVjea6Kco-8XjcO-9rTeVwMzYB0Dg6HBC10PdLY0ZlLb0CvatdCD4k-uC5-1gmQvmDdvVH3-8mmiNBWDSzoU-P6EFN7QHaCaxAON3tCXm6uny_vstnj7f3ldJY5oYs-k7n0wZdB8VJBqHLJlCyUr5gOUkMFgfEq-FwvFoKZ4LXw0ghTOqa1rkom5IScrHXjaMOir3vw7z52Hfjecp4XRsoROl1DqxQ_BsDetjV6aBrXQRzQ8lxzJaQ0_0GlZtKU45iQszXqU0RMEOwq1a1LX5Yz-9OG5XbTxsger1mHLdhlHFI3pmJHrwXL5Te0H4Oo</recordid><startdate>20140501</startdate><enddate>20140501</enddate><creator>Palapati, Naveen K. 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R</creatorcontrib><creatorcontrib>Muth, Adrienne</creatorcontrib><creatorcontrib>Zhu, Yujie</creatorcontrib><creatorcontrib>Wang, Chunsheng</creatorcontrib><creatorcontrib>Subramanian, Arunkumar</creatorcontrib><creatorcontrib>Energy Frontier Research Centers (EFRC)</creatorcontrib><creatorcontrib>Nanostructures for Electrical Energy Storage (NEES)</creatorcontrib><collection>CrossRef</collection><collection>Biotechnology Research Abstracts</collection><collection>Technology Research Database</collection><collection>Engineering Research Database</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Journal of Nanotechnology in Engineering and Medicine</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Palapati, Naveen K. R</au><au>Muth, Adrienne</au><au>Zhu, Yujie</au><au>Wang, Chunsheng</au><au>Subramanian, Arunkumar</au><aucorp>Energy Frontier Research Centers (EFRC)</aucorp><aucorp>Nanostructures for Electrical Energy Storage (NEES)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Elastic Modulus Measurements on Large Diameter Nanowires Using a Nano-Assembled Platform</atitle><jtitle>Journal of Nanotechnology in Engineering and Medicine</jtitle><stitle>J. Nanotechnol. Eng. Med</stitle><date>2014-05-01</date><risdate>2014</risdate><volume>5</volume><issue>2</issue><issn>1949-2944</issn><eissn>1949-2952</eissn><abstract>This paper presents atomic force spectroscopy (AFM) results from large diameter nanowires (NWs), which range in radius from 150 nm to 300 nm, within a nano-assembled platform. The nanomechanical platform is constructed by assembling single NWs across pairs of gold nano-electrodes using dielectrophoresis and contains a short, suspended segment of the NW (in air) between the assembly electrodes. Atomic force microscope (AFM) force spectroscopy measurements are obtained by indenting the NW within this suspended segment and result in deformation of the NW involving a combination of both, bending and nano-indentation modes. This paper demonstrates the measurement technique using lithium iron phosphate NWs as a model system and presents a finite element model to extract the Young's modulus from nanomechanical data. The estimated Young's modulus of this material, which is an electrode material system of interest for next-generation lithium-ion batteries, was found to be diameter dependent and was observed to range in values between 100 MPa and 575 MPa.</abstract><cop>United States</cop><pub>ASME</pub><doi>10.1115/1.4028045</doi></addata></record> |
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subjects | Atomic force microscopy bio-inspired, energy storage (including batteries and capacitors), defects, charge transport, synthesis (novel materials), synthesis (self-assembly), synthesis (scalable processing) Mathematical models Modulus of elasticity Nanostructure Nanowires Platforms Segments Spectroscopy |
title | Elastic Modulus Measurements on Large Diameter Nanowires Using a Nano-Assembled Platform |
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