Top-Seeded Solution Growth of 3 Inch Diameter 4H-SiC Bulk Crystal Using Metal Solvents

We performed top-seeded solution growth of 4H-SiC for obtaining longer length crystal. Si-Cr and Si-Ti melts were used as solvents. Meniscus formation technique was applied to the present study. Special attention was paid to improve the process stability during long-term growth. One of major technol...

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Veröffentlicht in:Materials science forum 2014-02, Vol.778-780, p.79-82
Hauptverfasser: Sakamoto, Hidemitsu, Kamei, Kazuhito, Bessho, Takeshi, Daikoku, Hironori, Moriguchi, Koji, Kaido, Hiroshi, Kado, Motohisa, Okada, Nobuhiro, Danno, Katsunori, Ujihara, Toru, Kusunoki, Kazuhiko
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container_title Materials science forum
container_volume 778-780
creator Sakamoto, Hidemitsu
Kamei, Kazuhito
Bessho, Takeshi
Daikoku, Hironori
Moriguchi, Koji
Kaido, Hiroshi
Kado, Motohisa
Okada, Nobuhiro
Danno, Katsunori
Ujihara, Toru
Kusunoki, Kazuhiko
description We performed top-seeded solution growth of 4H-SiC for obtaining longer length crystal. Si-Cr and Si-Ti melts were used as solvents. Meniscus formation technique was applied to the present study. Special attention was paid to improve the process stability during long-term growth. One of major technological problems in the solution growth is that the precipitation of polycrystalline SiC which hiders the stable single crystal growth. Another problem is the fluctuation of supersaturation at the growth interface during the growth. Through the optimization of growth process conditions, we have successfully grown 4H-SiC single crystals up to 14 mm long with three-inch-diameter, and evaluated their crystalline quality.
doi_str_mv 10.4028/www.scientific.net/MSF.778-780.79
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subjects Crystal structure
Crystals
Melts
Optimization
Precipitation
Silicon carbide
Single crystals
Solvents
title Top-Seeded Solution Growth of 3 Inch Diameter 4H-SiC Bulk Crystal Using Metal Solvents
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