Synthesis mechanism of new morphology LiMnPO sub(4) nanofibers using electrospinning process
Lithium manganese phosphate (LiMnPO sub(4)) porous hollow nanofibers have been obtained by electrospinning method with LiNO sub(3), Mn(NO sub(3)) sub(2) times 4H sub(2)O, and NH sub(4)H sub(2)PO sub(4) as starting materials. The results show that the external diameter of the LiMnPO sub(4) hollow nan...
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| Veröffentlicht in: | Journal of electroceramics 2014-10, Vol.33 (1-2), p.7-11 |
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| creator | Kim, C Kim, B R Son, J T |
| description | Lithium manganese phosphate (LiMnPO sub(4)) porous hollow nanofibers have been obtained by electrospinning method with LiNO sub(3), Mn(NO sub(3)) sub(2) times 4H sub(2)O, and NH sub(4)H sub(2)PO sub(4) as starting materials. The results show that the external diameter of the LiMnPO sub(4) hollow nanofibers was in the range of 500-800 nm and the internal diameter was in the range of 50-500 nm at 750 degree C for 5 h in N sub(2) atmosphere. The porous hollow nanofibers obtained were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscopy (TEM). The results show that fibers with porous and hollow morphology were successfully formed by controlling the electrospinning parameters and calcination temperature. It is to be easy of uniform distribution of PVP and make hollow structure. |
| doi_str_mv | 10.1007/s10832-014-9893-5 |
| format | Article |
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The results show that the external diameter of the LiMnPO sub(4) hollow nanofibers was in the range of 500-800 nm and the internal diameter was in the range of 50-500 nm at 750 degree C for 5 h in N sub(2) atmosphere. The porous hollow nanofibers obtained were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscopy (TEM). The results show that fibers with porous and hollow morphology were successfully formed by controlling the electrospinning parameters and calcination temperature. It is to be easy of uniform distribution of PVP and make hollow structure.</description><identifier>ISSN: 1385-3449</identifier><identifier>EISSN: 1573-8663</identifier><identifier>DOI: 10.1007/s10832-014-9893-5</identifier><language>eng</language><subject>Ceramics ; Diffraction ; Electrospinning ; Morphology ; Nanofibers ; Scanning electron microscopy ; Transmission electron microscopy ; X-ray diffraction</subject><ispartof>Journal of electroceramics, 2014-10, Vol.33 (1-2), p.7-11</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids></links><search><creatorcontrib>Kim, C</creatorcontrib><creatorcontrib>Kim, B R</creatorcontrib><creatorcontrib>Son, J T</creatorcontrib><title>Synthesis mechanism of new morphology LiMnPO sub(4) nanofibers using electrospinning process</title><title>Journal of electroceramics</title><description>Lithium manganese phosphate (LiMnPO sub(4)) porous hollow nanofibers have been obtained by electrospinning method with LiNO sub(3), Mn(NO sub(3)) sub(2) times 4H sub(2)O, and NH sub(4)H sub(2)PO sub(4) as starting materials. The results show that the external diameter of the LiMnPO sub(4) hollow nanofibers was in the range of 500-800 nm and the internal diameter was in the range of 50-500 nm at 750 degree C for 5 h in N sub(2) atmosphere. The porous hollow nanofibers obtained were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscopy (TEM). The results show that fibers with porous and hollow morphology were successfully formed by controlling the electrospinning parameters and calcination temperature. It is to be easy of uniform distribution of PVP and make hollow structure.</description><subject>Ceramics</subject><subject>Diffraction</subject><subject>Electrospinning</subject><subject>Morphology</subject><subject>Nanofibers</subject><subject>Scanning electron microscopy</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><issn>1385-3449</issn><issn>1573-8663</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqVistKxEAQRRtRcHx8gLtajovWqulOprMWxYWioEthyITKpKVTHVMJMn_vCP6Aq3sO5xpzRXhDiOtbJQxuZZG8rULlbHFkFlSsnQ1l6Y4P7EJhnffVqTlT_UTEKnhamI-3vUwda1TouelqidpDbkH4G_o8Dl1OebeHp_gsry-g83bpr0FqyW3c8qgwa5QdcOJmGrMOUeTXhzE3rHphTto6KV_-7blZPty_3z3aQ_-aWadNH7XhlGrhPOuGyoI84coF94_rDxpGTnE</recordid><startdate>20141001</startdate><enddate>20141001</enddate><creator>Kim, C</creator><creator>Kim, B R</creator><creator>Son, J T</creator><scope>7QQ</scope><scope>7SP</scope><scope>7SR</scope><scope>7U5</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20141001</creationdate><title>Synthesis mechanism of new morphology LiMnPO sub(4) nanofibers using electrospinning process</title><author>Kim, C ; Kim, B R ; Son, J T</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-proquest_miscellaneous_16514102383</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Ceramics</topic><topic>Diffraction</topic><topic>Electrospinning</topic><topic>Morphology</topic><topic>Nanofibers</topic><topic>Scanning electron microscopy</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kim, C</creatorcontrib><creatorcontrib>Kim, B R</creatorcontrib><creatorcontrib>Son, J T</creatorcontrib><collection>Ceramic Abstracts</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of electroceramics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kim, C</au><au>Kim, B R</au><au>Son, J T</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis mechanism of new morphology LiMnPO sub(4) nanofibers using electrospinning process</atitle><jtitle>Journal of electroceramics</jtitle><date>2014-10-01</date><risdate>2014</risdate><volume>33</volume><issue>1-2</issue><spage>7</spage><epage>11</epage><pages>7-11</pages><issn>1385-3449</issn><eissn>1573-8663</eissn><abstract>Lithium manganese phosphate (LiMnPO sub(4)) porous hollow nanofibers have been obtained by electrospinning method with LiNO sub(3), Mn(NO sub(3)) sub(2) times 4H sub(2)O, and NH sub(4)H sub(2)PO sub(4) as starting materials. The results show that the external diameter of the LiMnPO sub(4) hollow nanofibers was in the range of 500-800 nm and the internal diameter was in the range of 50-500 nm at 750 degree C for 5 h in N sub(2) atmosphere. The porous hollow nanofibers obtained were characterized by X-ray diffraction (XRD), scanning electron microscope (SEM) and transmission electron microscopy (TEM). The results show that fibers with porous and hollow morphology were successfully formed by controlling the electrospinning parameters and calcination temperature. It is to be easy of uniform distribution of PVP and make hollow structure.</abstract><doi>10.1007/s10832-014-9893-5</doi></addata></record> |
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| subjects | Ceramics Diffraction Electrospinning Morphology Nanofibers Scanning electron microscopy Transmission electron microscopy X-ray diffraction |
| title | Synthesis mechanism of new morphology LiMnPO sub(4) nanofibers using electrospinning process |
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