UV radiation: a promising tool in the synthesis of multicomponent nano-oxides
Photochemical synthesis of selected multicomponent compounds, namely cadmium or magnesium zinc oxides doped with Ga 3+ ions—Zn 1− x Cd x (Mg x )O:Ga—and lutetium aluminum garnets Lu 3 Al 5 O 12 (LuAG) doped with Pr 3+ or Eu 3+ ions (LuAG:Pr(Eu)), was successfully performed. The synthesis is based on...
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| Veröffentlicht in: | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology 2014-11, Vol.16 (11), p.1-7, Article 2686 |
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| creator | Čuba, Václav Procházková, Lenka Bárta, Jan Vondrášková, Apolena Pavelková, Tereza Mihóková, Eva Jarý, Vítězslav Nikl, Martin |
| description | Photochemical synthesis of selected multicomponent compounds, namely cadmium or magnesium zinc oxides doped with Ga
3+
ions—Zn
1−
x
Cd
x
(Mg
x
)O:Ga—and lutetium aluminum garnets Lu
3
Al
5
O
12
(LuAG) doped with Pr
3+
or Eu
3+
ions (LuAG:Pr(Eu)), was successfully performed. The synthesis is based on photo-induced precipitation of solid precursors from aqueous solutions containing formate anion and soluble metal salts (nitrates or chlorides). Low pressure mercury lamps were used for the irradiation of solutions. Solid precursors were subsequently separated from aqueous phase and calcined to obtain the final products. Prepared materials feature high chemical purity, good crystallinity, and nano-dimensions in the range of 10–100 nm. Due to the high level of interaction among individual components in photo-precipitated precursors, no additional oxide phases were observed after calcination apart from the desired solid phase. Moreover, highly intensive radioluminescence or shift of excitonic luminescence has been observed, depending on type and composition of prepared materials. Results indicate that prepared nanomaterials may be prospectively utilized as highly efficient nanoscintillators for preparation of optical ceramics or band-gap engineered nanophosphors. |
| doi_str_mv | 10.1007/s11051-014-2686-6 |
| format | Article |
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3+
ions—Zn
1−
x
Cd
x
(Mg
x
)O:Ga—and lutetium aluminum garnets Lu
3
Al
5
O
12
(LuAG) doped with Pr
3+
or Eu
3+
ions (LuAG:Pr(Eu)), was successfully performed. The synthesis is based on photo-induced precipitation of solid precursors from aqueous solutions containing formate anion and soluble metal salts (nitrates or chlorides). Low pressure mercury lamps were used for the irradiation of solutions. Solid precursors were subsequently separated from aqueous phase and calcined to obtain the final products. Prepared materials feature high chemical purity, good crystallinity, and nano-dimensions in the range of 10–100 nm. Due to the high level of interaction among individual components in photo-precipitated precursors, no additional oxide phases were observed after calcination apart from the desired solid phase. Moreover, highly intensive radioluminescence or shift of excitonic luminescence has been observed, depending on type and composition of prepared materials. Results indicate that prepared nanomaterials may be prospectively utilized as highly efficient nanoscintillators for preparation of optical ceramics or band-gap engineered nanophosphors.</description><identifier>ISSN: 1388-0764</identifier><identifier>EISSN: 1572-896X</identifier><identifier>DOI: 10.1007/s11051-014-2686-6</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Aluminum ; Cadmium ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Chlorides ; Composite Nanoparticles ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Electron states and collective excitations in thin films, multilayers, quantum wells, mesoscopic and nanoscale systems ; Electronic structure and electrical properties of surfaces, interfaces, thin films and low-dimensional structures ; Exact sciences and technology ; Formates ; Inorganic Chemistry ; Ions ; Irradiation ; Lasers ; Lutetium ; Magnesium ; Materials Science ; Mercury ; Nanocrystalline materials ; Nanoparticles ; Nanoscale materials and structures: fabrication and characterization ; Nanostructure ; Nanotechnology ; Optical Devices ; Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation ; Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures ; Optics ; Photochemicals ; Photonics ; Physical Chemistry ; Physics ; Precursors ; Radiation effects on specific materials ; Research Paper ; Structure of solids and liquids; crystallography ; Synthesis ; Ultraviolet radiation</subject><ispartof>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2014-11, Vol.16 (11), p.1-7, Article 2686</ispartof><rights>Springer Science+Business Media Dordrecht 2014</rights><rights>2015 INIST-CNRS</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c379t-ae0f6261db2c2fd4e25a19a7a85fb9d7c6ef78b6b35847a24f124b482fb626083</citedby><cites>FETCH-LOGICAL-c379t-ae0f6261db2c2fd4e25a19a7a85fb9d7c6ef78b6b35847a24f124b482fb626083</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11051-014-2686-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11051-014-2686-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=29037377$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Čuba, Václav</creatorcontrib><creatorcontrib>Procházková, Lenka</creatorcontrib><creatorcontrib>Bárta, Jan</creatorcontrib><creatorcontrib>Vondrášková, Apolena</creatorcontrib><creatorcontrib>Pavelková, Tereza</creatorcontrib><creatorcontrib>Mihóková, Eva</creatorcontrib><creatorcontrib>Jarý, Vítězslav</creatorcontrib><creatorcontrib>Nikl, Martin</creatorcontrib><title>UV radiation: a promising tool in the synthesis of multicomponent nano-oxides</title><title>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</title><addtitle>J Nanopart Res</addtitle><description>Photochemical synthesis of selected multicomponent compounds, namely cadmium or magnesium zinc oxides doped with Ga
3+
ions—Zn
1−
x
Cd
x
(Mg
x
)O:Ga—and lutetium aluminum garnets Lu
3
Al
5
O
12
(LuAG) doped with Pr
3+
or Eu
3+
ions (LuAG:Pr(Eu)), was successfully performed. The synthesis is based on photo-induced precipitation of solid precursors from aqueous solutions containing formate anion and soluble metal salts (nitrates or chlorides). Low pressure mercury lamps were used for the irradiation of solutions. Solid precursors were subsequently separated from aqueous phase and calcined to obtain the final products. Prepared materials feature high chemical purity, good crystallinity, and nano-dimensions in the range of 10–100 nm. Due to the high level of interaction among individual components in photo-precipitated precursors, no additional oxide phases were observed after calcination apart from the desired solid phase. Moreover, highly intensive radioluminescence or shift of excitonic luminescence has been observed, depending on type and composition of prepared materials. Results indicate that prepared nanomaterials may be prospectively utilized as highly efficient nanoscintillators for preparation of optical ceramics or band-gap engineered nanophosphors.</description><subject>Aluminum</subject><subject>Cadmium</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Chlorides</subject><subject>Composite Nanoparticles</subject><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Electron states and collective excitations in thin films, multilayers, quantum wells, mesoscopic and nanoscale systems</subject><subject>Electronic structure and electrical properties of surfaces, interfaces, thin films and low-dimensional structures</subject><subject>Exact sciences and technology</subject><subject>Formates</subject><subject>Inorganic Chemistry</subject><subject>Ions</subject><subject>Irradiation</subject><subject>Lasers</subject><subject>Lutetium</subject><subject>Magnesium</subject><subject>Materials Science</subject><subject>Mercury</subject><subject>Nanocrystalline materials</subject><subject>Nanoparticles</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Nanostructure</subject><subject>Nanotechnology</subject><subject>Optical Devices</subject><subject>Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation</subject><subject>Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures</subject><subject>Optics</subject><subject>Photochemicals</subject><subject>Photonics</subject><subject>Physical Chemistry</subject><subject>Physics</subject><subject>Precursors</subject><subject>Radiation effects on specific materials</subject><subject>Research Paper</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Synthesis</subject><subject>Ultraviolet radiation</subject><issn>1388-0764</issn><issn>1572-896X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp1kEtLAzEYRYMoWKs_wF1ABDfRPGaSjDsRX1BxY8VdyMwkNWUmqckM2H9vSouI4OoL5NzD5QJwSvAlwVhcJUJwSRAmBaJccsT3wISUgiJZ8ff9_GZSIix4cQiOUlpiTDit6AQ8z99g1K3Tgwv-Gmq4iqF3yfkFHELooPNw-DAwrX0-ySUYLOzHbnBN6FfBGz9Ar31A4cu1Jh2DA6u7ZE52dwrm93evt49o9vLwdHszQw0T1YC0wZZTTtqaNtS2haGlJpUWWpa2rlrRcGOFrHnNSlkITQtLaFEXkto6x7BkU3Cx9ea2n6NJg8qdG9N12pswJkV4SVjFOccZPfuDLsMYfW6XKSayj5GNkGypJoaUorFqFV2v41oRrDYDq-3AKg-sNgMrnjPnO7NOje5s1L5x6SdIK8wEEyJzdMul_OUXJv5q8K_8G0Ldikc</recordid><startdate>20141101</startdate><enddate>20141101</enddate><creator>Čuba, Václav</creator><creator>Procházková, Lenka</creator><creator>Bárta, Jan</creator><creator>Vondrášková, Apolena</creator><creator>Pavelková, Tereza</creator><creator>Mihóková, Eva</creator><creator>Jarý, Vítězslav</creator><creator>Nikl, Martin</creator><general>Springer Netherlands</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QO</scope><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>7U7</scope><scope>7X7</scope><scope>7XB</scope><scope>8AO</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>K9.</scope><scope>KB.</scope><scope>L6V</scope><scope>L7M</scope><scope>LK8</scope><scope>M0S</scope><scope>M7P</scope><scope>M7S</scope><scope>P5Z</scope><scope>P62</scope><scope>P64</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>7QF</scope><scope>7QQ</scope></search><sort><creationdate>20141101</creationdate><title>UV radiation: a promising tool in the synthesis of multicomponent nano-oxides</title><author>Čuba, Václav ; 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crystallography</topic><topic>Synthesis</topic><topic>Ultraviolet radiation</topic><toplevel>online_resources</toplevel><creatorcontrib>Čuba, Václav</creatorcontrib><creatorcontrib>Procházková, Lenka</creatorcontrib><creatorcontrib>Bárta, Jan</creatorcontrib><creatorcontrib>Vondrášková, Apolena</creatorcontrib><creatorcontrib>Pavelková, Tereza</creatorcontrib><creatorcontrib>Mihóková, Eva</creatorcontrib><creatorcontrib>Jarý, Vítězslav</creatorcontrib><creatorcontrib>Nikl, Martin</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Biotechnology Research Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Toxicology Abstracts</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ProQuest Pharma Collection</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>ProQuest Biological Science Collection</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Biological Science Database</collection><collection>Engineering Database</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>Aluminium Industry Abstracts</collection><collection>Ceramic Abstracts</collection><jtitle>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Čuba, Václav</au><au>Procházková, Lenka</au><au>Bárta, Jan</au><au>Vondrášková, Apolena</au><au>Pavelková, Tereza</au><au>Mihóková, Eva</au><au>Jarý, Vítězslav</au><au>Nikl, Martin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>UV radiation: a promising tool in the synthesis of multicomponent nano-oxides</atitle><jtitle>Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology</jtitle><stitle>J Nanopart Res</stitle><date>2014-11-01</date><risdate>2014</risdate><volume>16</volume><issue>11</issue><spage>1</spage><epage>7</epage><pages>1-7</pages><artnum>2686</artnum><issn>1388-0764</issn><eissn>1572-896X</eissn><abstract>Photochemical synthesis of selected multicomponent compounds, namely cadmium or magnesium zinc oxides doped with Ga
3+
ions—Zn
1−
x
Cd
x
(Mg
x
)O:Ga—and lutetium aluminum garnets Lu
3
Al
5
O
12
(LuAG) doped with Pr
3+
or Eu
3+
ions (LuAG:Pr(Eu)), was successfully performed. The synthesis is based on photo-induced precipitation of solid precursors from aqueous solutions containing formate anion and soluble metal salts (nitrates or chlorides). Low pressure mercury lamps were used for the irradiation of solutions. Solid precursors were subsequently separated from aqueous phase and calcined to obtain the final products. Prepared materials feature high chemical purity, good crystallinity, and nano-dimensions in the range of 10–100 nm. Due to the high level of interaction among individual components in photo-precipitated precursors, no additional oxide phases were observed after calcination apart from the desired solid phase. Moreover, highly intensive radioluminescence or shift of excitonic luminescence has been observed, depending on type and composition of prepared materials. Results indicate that prepared nanomaterials may be prospectively utilized as highly efficient nanoscintillators for preparation of optical ceramics or band-gap engineered nanophosphors.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s11051-014-2686-6</doi><tpages>7</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1388-0764 |
| ispartof | Journal of nanoparticle research : an interdisciplinary forum for nanoscale science and technology, 2014-11, Vol.16 (11), p.1-7, Article 2686 |
| issn | 1388-0764 1572-896X |
| language | eng |
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| source | Springer Nature - Complete Springer Journals |
| subjects | Aluminum Cadmium Characterization and Evaluation of Materials Chemistry and Materials Science Chlorides Composite Nanoparticles Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Electron states and collective excitations in thin films, multilayers, quantum wells, mesoscopic and nanoscale systems Electronic structure and electrical properties of surfaces, interfaces, thin films and low-dimensional structures Exact sciences and technology Formates Inorganic Chemistry Ions Irradiation Lasers Lutetium Magnesium Materials Science Mercury Nanocrystalline materials Nanoparticles Nanoscale materials and structures: fabrication and characterization Nanostructure Nanotechnology Optical Devices Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures Optics Photochemicals Photonics Physical Chemistry Physics Precursors Radiation effects on specific materials Research Paper Structure of solids and liquids crystallography Synthesis Ultraviolet radiation |
| title | UV radiation: a promising tool in the synthesis of multicomponent nano-oxides |
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