Assessment of a new method for the analysis of decomposition gases of polymers by a combining thermogravimetric solid-phase extraction and thermal desorption gas chromatography mass spectrometry

•Alternative to common TGA–FTIR/MS techniques for analysing complex mixtures of thermal decomposition products of polymers.•Development of a new technique consisting of thermogravimetry (TGA)–solid-phase extraction (SPE)–thermal desorption (TDS)–gas chromatography mass spectrometry (GC–MS).•Ease of...

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Veröffentlicht in:	Journal of Chromatography A 2014-08, Vol.1354, p.117-128
Hauptverfasser:	Duemichen, E., Braun, U., Senz, R., Fabian, G., Sturm, H.
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Applied sciences Chemical reactions and properties Chemistry Chromatographic methods and physical methods associated with chromatography Decomposition Degradation Desorption Exact sciences and technology Extraction Gas chromatographic methods Gas chromatography Gas Chromatography-Mass Spectrometry - methods Infrared spectroscopy Mass spectrometry Organic polymers Physicochemistry of polymers Polybutylene terephthalates Polyesters - chemistry Polymer Polymers - chemistry Reproducibility of Results Solid Phase Extraction - methods Solid-phase extraction Spectra Spectroscopy, Fourier Transform Infrared TDS–GC–MS TGA–FTIR TGA–MS Thermogravimetry
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