Strategies for the analysis of highly reactive pinacolboronate esters

► A successful reversed-phase HPLC method for the analysis of pinacolboronate esters. ► Unusual high pH mobile phases (>pH 12) effectively stabilizes the analyte. ► Aprotic solvent mixture provides enough solubility for the analyte and its degradants. ► Aprotic solvent mixture eliminates sample d...

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Veröffentlicht in:	Journal of Chromatography A 2012-03, Vol.1229, p.216-222
Hauptverfasser:	Zhong, Qiqing, Ngim, Kenley K., Sun, Megan, Li, Jane, Deese, Alan, Chetwyn, Nik P.
Format:	Artikel
Sprache:	eng
Schlagworte:	Acetonitriles - chemistry Alkenes - analysis Boronic acid Boronic Acids - analysis Butanes - analysis Chemistry, Analytic Chemistry, Pharmaceutical Chromatography Chromatography, High Pressure Liquid - methods Coupling (molecular) Esters Esters - analysis High performance liquid chromatography hydrolysis Methylene Chloride - chemistry On-column hydrolysis Phases Pinacolboronate ester Purity Separation solvents Strategy Suzuki coupling Synthesis
Online-Zugang:	Volltext
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