Role of chromatography in the development of Standard Reference Materials for organic analysis
► Key to independent method for SRM certification is separation science. ► For SRMs, the goal is to maximize the differences in extraction, separation and detection. ► Differences in stationary phase selectivity in LC and GC provide independence. ► SRMs for environmental, food, and dietary supplemen...
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| Veröffentlicht in: | Journal of Chromatography A 2012-10, Vol.1261, p.3-22 |
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| container_title | Journal of Chromatography A |
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| creator | Wise, Stephen A. Phinney, Karen W. Sander, Lane C. Schantz, Michele M. |
| description | ► Key to independent method for SRM certification is separation science. ► For SRMs, the goal is to maximize the differences in extraction, separation and detection. ► Differences in stationary phase selectivity in LC and GC provide independence. ► SRMs for environmental, food, and dietary supplement analysis are described.
The certification of chemical constituents in natural-matrix Standard Reference Materials (SRMs) at the National Institute of Standards and Technology (NIST) can require the use of two or more independent analytical methods. The independence among the methods is generally achieved by taking advantage of differences in extraction, separation, and detection selectivity. This review describes the development of the independent analytical methods approach at NIST, and its implementation in the measurement of organic constituents such as contaminants in environmental materials, nutrients and marker compounds in food and dietary supplement matrices, and health diagnostic and nutritional assessment markers in human serum. The focus of this review is the important and critical role that separation science techniques play in achieving the necessary independence of the analytical steps in the measurement of trace-level organic constituents in natural matrix SRMs. |
| doi_str_mv | 10.1016/j.chroma.2012.05.093 |
| format | Article |
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The certification of chemical constituents in natural-matrix Standard Reference Materials (SRMs) at the National Institute of Standards and Technology (NIST) can require the use of two or more independent analytical methods. The independence among the methods is generally achieved by taking advantage of differences in extraction, separation, and detection selectivity. This review describes the development of the independent analytical methods approach at NIST, and its implementation in the measurement of organic constituents such as contaminants in environmental materials, nutrients and marker compounds in food and dietary supplement matrices, and health diagnostic and nutritional assessment markers in human serum. The focus of this review is the important and critical role that separation science techniques play in achieving the necessary independence of the analytical steps in the measurement of trace-level organic constituents in natural matrix SRMs.</description><identifier>ISSN: 0021-9673</identifier><identifier>EISSN: 1873-3778</identifier><identifier>DOI: 10.1016/j.chroma.2012.05.093</identifier><identifier>PMID: 22721765</identifier><language>eng</language><publisher>Netherlands: Elsevier B.V</publisher><subject>Assessments ; blood serum ; Carotenoids ; certification ; Chromatographic selectivity ; Chromatography ; Chromatography - methods ; Chromatography - standards ; Constituents ; dietary supplements ; food contamination ; food matrix ; Gas chromatography–mass spectrometry (GC–MS) ; humans ; Liquid chromatography–mass spectrometry (LC–MS) ; Markers ; Mass Spectrometry - methods ; Mass Spectrometry - standards ; Mathematical analysis ; nutrient content ; nutrients ; nutrition assessment ; Organic Chemicals - analysis ; Polycyclic aromatic hydrocarbons (PAHs) ; Reference Standards ; Separation ; Standard Reference Material (SRM) ; Standard reference materials ; water pollution</subject><ispartof>Journal of Chromatography A, 2012-10, Vol.1261, p.3-22</ispartof><rights>2012</rights><rights>Published by Elsevier B.V.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c518t-85deaff41d557f6d32e1a2c84fd47611ec18e0bcf8aac37d9888fc3e804a4a153</citedby><cites>FETCH-LOGICAL-c518t-85deaff41d557f6d32e1a2c84fd47611ec18e0bcf8aac37d9888fc3e804a4a153</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.chroma.2012.05.093$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>315,781,785,3551,27929,27930,46000</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22721765$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Wise, Stephen A.</creatorcontrib><creatorcontrib>Phinney, Karen W.</creatorcontrib><creatorcontrib>Sander, Lane C.</creatorcontrib><creatorcontrib>Schantz, Michele M.</creatorcontrib><title>Role of chromatography in the development of Standard Reference Materials for organic analysis</title><title>Journal of Chromatography A</title><addtitle>J Chromatogr A</addtitle><description>► Key to independent method for SRM certification is separation science. ► For SRMs, the goal is to maximize the differences in extraction, separation and detection. ► Differences in stationary phase selectivity in LC and GC provide independence. ► SRMs for environmental, food, and dietary supplement analysis are described.
The certification of chemical constituents in natural-matrix Standard Reference Materials (SRMs) at the National Institute of Standards and Technology (NIST) can require the use of two or more independent analytical methods. The independence among the methods is generally achieved by taking advantage of differences in extraction, separation, and detection selectivity. This review describes the development of the independent analytical methods approach at NIST, and its implementation in the measurement of organic constituents such as contaminants in environmental materials, nutrients and marker compounds in food and dietary supplement matrices, and health diagnostic and nutritional assessment markers in human serum. The focus of this review is the important and critical role that separation science techniques play in achieving the necessary independence of the analytical steps in the measurement of trace-level organic constituents in natural matrix SRMs.</description><subject>Assessments</subject><subject>blood serum</subject><subject>Carotenoids</subject><subject>certification</subject><subject>Chromatographic selectivity</subject><subject>Chromatography</subject><subject>Chromatography - methods</subject><subject>Chromatography - standards</subject><subject>Constituents</subject><subject>dietary supplements</subject><subject>food contamination</subject><subject>food matrix</subject><subject>Gas chromatography–mass spectrometry (GC–MS)</subject><subject>humans</subject><subject>Liquid chromatography–mass spectrometry (LC–MS)</subject><subject>Markers</subject><subject>Mass Spectrometry - methods</subject><subject>Mass Spectrometry - standards</subject><subject>Mathematical analysis</subject><subject>nutrient content</subject><subject>nutrients</subject><subject>nutrition assessment</subject><subject>Organic Chemicals - analysis</subject><subject>Polycyclic aromatic hydrocarbons (PAHs)</subject><subject>Reference Standards</subject><subject>Separation</subject><subject>Standard Reference Material (SRM)</subject><subject>Standard reference materials</subject><subject>water pollution</subject><issn>0021-9673</issn><issn>1873-3778</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkU1v1DAQhi0EokvhHyDwkUuCP-LYuSChqlCkIqSWXrGm9njXqyRe7Gyl_fckSukRTj7MM-9Y70PIW85qznj7cV-7XU4D1IJxUTNVs04-IxtutKyk1uY52TAmeNW1Wp6RV6XsGeOaafGSnAmhBdet2pBfN6lHmgJdw6a0zXDYnWgc6bRD6vEB-3QYcJwW6HaC0UP29AYDZhwd0u8wYY7QFxpSpilvYYyOwgj9qcTymrwI8wzfPL7n5O7L5c-Lq-r6x9dvF5-vK6e4mSqjPEIIDfdK6dB6KZCDcKYJvtEt5-i4QXbvggFwUvvOGBOcRMMaaIAreU4-rLmHnH4fsUx2iMVh38OI6Vgsbxsh2lZ15v8ol63SzMgltVlRl1MpGYM95DhAPlnO7CLB7u3am10kWKbsLGFee_d44Xg_oH9a-tv6DLxfgQDJwjbHYu9u5wQ1GzKzr24mPq0EzqU9RMy2uLj07WNGN1mf4r__8Ae406Qx</recordid><startdate>20121026</startdate><enddate>20121026</enddate><creator>Wise, Stephen A.</creator><creator>Phinney, Karen W.</creator><creator>Sander, Lane C.</creator><creator>Schantz, Michele M.</creator><general>Elsevier B.V</general><scope>FBQ</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7QH</scope><scope>7TV</scope><scope>7UA</scope><scope>C1K</scope><scope>F1W</scope><scope>H97</scope><scope>L.G</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope></search><sort><creationdate>20121026</creationdate><title>Role of chromatography in the development of Standard Reference Materials for organic analysis</title><author>Wise, Stephen A. ; Phinney, Karen W. ; Sander, Lane C. ; Schantz, Michele M.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c518t-85deaff41d557f6d32e1a2c84fd47611ec18e0bcf8aac37d9888fc3e804a4a153</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Assessments</topic><topic>blood serum</topic><topic>Carotenoids</topic><topic>certification</topic><topic>Chromatographic selectivity</topic><topic>Chromatography</topic><topic>Chromatography - methods</topic><topic>Chromatography - standards</topic><topic>Constituents</topic><topic>dietary supplements</topic><topic>food contamination</topic><topic>food matrix</topic><topic>Gas chromatography–mass spectrometry (GC–MS)</topic><topic>humans</topic><topic>Liquid chromatography–mass spectrometry (LC–MS)</topic><topic>Markers</topic><topic>Mass Spectrometry - methods</topic><topic>Mass Spectrometry - standards</topic><topic>Mathematical analysis</topic><topic>nutrient content</topic><topic>nutrients</topic><topic>nutrition assessment</topic><topic>Organic Chemicals - analysis</topic><topic>Polycyclic aromatic hydrocarbons (PAHs)</topic><topic>Reference Standards</topic><topic>Separation</topic><topic>Standard Reference Material (SRM)</topic><topic>Standard reference materials</topic><topic>water pollution</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wise, Stephen A.</creatorcontrib><creatorcontrib>Phinney, Karen W.</creatorcontrib><creatorcontrib>Sander, Lane C.</creatorcontrib><creatorcontrib>Schantz, Michele M.</creatorcontrib><collection>AGRIS</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Aqualine</collection><collection>Pollution Abstracts</collection><collection>Water Resources Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ASFA: Aquatic Sciences and Fisheries Abstracts</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) 3: Aquatic Pollution & Environmental Quality</collection><collection>Aquatic Science & Fisheries Abstracts (ASFA) Professional</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of Chromatography A</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wise, Stephen A.</au><au>Phinney, Karen W.</au><au>Sander, Lane C.</au><au>Schantz, Michele M.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Role of chromatography in the development of Standard Reference Materials for organic analysis</atitle><jtitle>Journal of Chromatography A</jtitle><addtitle>J Chromatogr A</addtitle><date>2012-10-26</date><risdate>2012</risdate><volume>1261</volume><spage>3</spage><epage>22</epage><pages>3-22</pages><issn>0021-9673</issn><eissn>1873-3778</eissn><abstract>► Key to independent method for SRM certification is separation science. ► For SRMs, the goal is to maximize the differences in extraction, separation and detection. ► Differences in stationary phase selectivity in LC and GC provide independence. ► SRMs for environmental, food, and dietary supplement analysis are described.
The certification of chemical constituents in natural-matrix Standard Reference Materials (SRMs) at the National Institute of Standards and Technology (NIST) can require the use of two or more independent analytical methods. The independence among the methods is generally achieved by taking advantage of differences in extraction, separation, and detection selectivity. This review describes the development of the independent analytical methods approach at NIST, and its implementation in the measurement of organic constituents such as contaminants in environmental materials, nutrients and marker compounds in food and dietary supplement matrices, and health diagnostic and nutritional assessment markers in human serum. The focus of this review is the important and critical role that separation science techniques play in achieving the necessary independence of the analytical steps in the measurement of trace-level organic constituents in natural matrix SRMs.</abstract><cop>Netherlands</cop><pub>Elsevier B.V</pub><pmid>22721765</pmid><doi>10.1016/j.chroma.2012.05.093</doi><tpages>20</tpages></addata></record> |
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| subjects | Assessments blood serum Carotenoids certification Chromatographic selectivity Chromatography Chromatography - methods Chromatography - standards Constituents dietary supplements food contamination food matrix Gas chromatography–mass spectrometry (GC–MS) humans Liquid chromatography–mass spectrometry (LC–MS) Markers Mass Spectrometry - methods Mass Spectrometry - standards Mathematical analysis nutrient content nutrients nutrition assessment Organic Chemicals - analysis Polycyclic aromatic hydrocarbons (PAHs) Reference Standards Separation Standard Reference Material (SRM) Standard reference materials water pollution |
| title | Role of chromatography in the development of Standard Reference Materials for organic analysis |
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