Solution combustion method for synthesis of nanostructured hydroxyapatite, fluorapatite and chlorapatite
•We report a synthesis of HA, Fap and Clap vio a modified solution combustion method. The nucleation of β-TCP was inhibited in the abundant-calcium system (Ca/P=2.3>>1.67) in this study. F− brushed into the structure of HA and replace the position of OH− is easier than that of Cl−. Hydroxyapat...
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| Veröffentlicht in: | Applied surface science 2014-09, Vol.314, p.1026-1033 |
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| creator | Zhao, Junjie Dong, Xiaochen Bian, Mengmeng Zhao, Junfeng Zhang, Yao Sun, Yue Chen, JianHua Wang, XuHong |
| description | •We report a synthesis of HA, Fap and Clap vio a modified solution combustion method. The nucleation of β-TCP was inhibited in the abundant-calcium system (Ca/P=2.3>>1.67) in this study. F− brushed into the structure of HA and replace the position of OH− is easier than that of Cl−.
Hydroxyapatite (HAP), fluorapatite (Fap) and chlorapatite (Clap) were prepared by solution combustion method with further annealing at 800°C. The characterization and structural features of the synthesized powders were evaluated by the powder X-ray diffraction (XRD, Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and transmission electron microscopy (TEM) techniques. Characterization results from XRD and Rietveld analysis revealed that OH− in the HAP lattice were gradually substituted with the increase of F− and Cl− content and totally substituted at the molar concentration of 0.28 and 0.6, respectively. The results from FI-IR have also confirmed the incorporation of substituted anions in the apatite structure. |
| doi_str_mv | 10.1016/j.apsusc.2014.06.075 |
| format | Article |
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Hydroxyapatite (HAP), fluorapatite (Fap) and chlorapatite (Clap) were prepared by solution combustion method with further annealing at 800°C. The characterization and structural features of the synthesized powders were evaluated by the powder X-ray diffraction (XRD, Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and transmission electron microscopy (TEM) techniques. Characterization results from XRD and Rietveld analysis revealed that OH− in the HAP lattice were gradually substituted with the increase of F− and Cl− content and totally substituted at the molar concentration of 0.28 and 0.6, respectively. The results from FI-IR have also confirmed the incorporation of substituted anions in the apatite structure.</description><identifier>ISSN: 0169-4332</identifier><identifier>EISSN: 1873-5584</identifier><identifier>DOI: 10.1016/j.apsusc.2014.06.075</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Apatite ; Chlorapatite (Clap) ; Combustion ; Condensed matter: electronic structure, electrical, magnetic, and optical properties ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Fluorapatite ; Fluorapatite (Fap) ; Fourier transforms ; Hydroxyapatite ; Hydroxyapatite (HAP) ; Infrared spectroscopy ; Physics ; Rietveld refinement ; Scanning electron microscopy ; Solution combustion method ; X-ray diffraction</subject><ispartof>Applied surface science, 2014-09, Vol.314, p.1026-1033</ispartof><rights>2014 Elsevier B.V.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c369t-1cf9522b317e12380d4f0c72d2aa49f538512e5a33344d15ea55b03b96678ac43</citedby><cites>FETCH-LOGICAL-c369t-1cf9522b317e12380d4f0c72d2aa49f538512e5a33344d15ea55b03b96678ac43</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0169433214013609$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=28744341$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhao, Junjie</creatorcontrib><creatorcontrib>Dong, Xiaochen</creatorcontrib><creatorcontrib>Bian, Mengmeng</creatorcontrib><creatorcontrib>Zhao, Junfeng</creatorcontrib><creatorcontrib>Zhang, Yao</creatorcontrib><creatorcontrib>Sun, Yue</creatorcontrib><creatorcontrib>Chen, JianHua</creatorcontrib><creatorcontrib>Wang, XuHong</creatorcontrib><title>Solution combustion method for synthesis of nanostructured hydroxyapatite, fluorapatite and chlorapatite</title><title>Applied surface science</title><description>•We report a synthesis of HA, Fap and Clap vio a modified solution combustion method. The nucleation of β-TCP was inhibited in the abundant-calcium system (Ca/P=2.3>>1.67) in this study. F− brushed into the structure of HA and replace the position of OH− is easier than that of Cl−.
Hydroxyapatite (HAP), fluorapatite (Fap) and chlorapatite (Clap) were prepared by solution combustion method with further annealing at 800°C. The characterization and structural features of the synthesized powders were evaluated by the powder X-ray diffraction (XRD, Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and transmission electron microscopy (TEM) techniques. Characterization results from XRD and Rietveld analysis revealed that OH− in the HAP lattice were gradually substituted with the increase of F− and Cl− content and totally substituted at the molar concentration of 0.28 and 0.6, respectively. The results from FI-IR have also confirmed the incorporation of substituted anions in the apatite structure.</description><subject>Apatite</subject><subject>Chlorapatite (Clap)</subject><subject>Combustion</subject><subject>Condensed matter: electronic structure, electrical, magnetic, and optical properties</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Fluorapatite</subject><subject>Fluorapatite (Fap)</subject><subject>Fourier transforms</subject><subject>Hydroxyapatite</subject><subject>Hydroxyapatite (HAP)</subject><subject>Infrared spectroscopy</subject><subject>Physics</subject><subject>Rietveld refinement</subject><subject>Scanning electron microscopy</subject><subject>Solution combustion method</subject><subject>X-ray diffraction</subject><issn>0169-4332</issn><issn>1873-5584</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNp9kE1rGzEQhkVIoK7Tf9CDLoEcult97sclEEL6AYYempyFLI1YmfXK0WhL_e-7qU2OOWmkeWZe9BDymbOaM9583dX2gDO6WjCuatbUrNUXZMW7VlZad-qSrBasr5SU4gP5iLhjjIuluyLD7zTOJaaJurTfzvi_3EMZkqchZYrHqQyAEWkKdLJTwpJnV-YMng5Hn9Pfoz3YEgt8oWGcUz7fqJ08dcP49nBNroIdET6dzzV5_vb49PCj2vz6_vPhflM52fSl4i70Woit5C1wITvmVWCuFV5Yq_qgZae5AG2llEp5rsFqvWVy2zdN21mn5JrcnvYecnqZAYvZR3QwjnaCNKPhjRKC60a0C6pOqMsJMUMwhxz3Nh8NZ-ZVrNmZk1jzKtawxixil7Gbc4JFZ8eQ7eQivs0uXpWSii_c3YmD5bt_ImSDLsLkwMcMrhif4vtB_wCWupLO</recordid><startdate>20140930</startdate><enddate>20140930</enddate><creator>Zhao, Junjie</creator><creator>Dong, Xiaochen</creator><creator>Bian, Mengmeng</creator><creator>Zhao, Junfeng</creator><creator>Zhang, Yao</creator><creator>Sun, Yue</creator><creator>Chen, JianHua</creator><creator>Wang, XuHong</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20140930</creationdate><title>Solution combustion method for synthesis of nanostructured hydroxyapatite, fluorapatite and chlorapatite</title><author>Zhao, Junjie ; Dong, Xiaochen ; Bian, Mengmeng ; Zhao, Junfeng ; Zhang, Yao ; Sun, Yue ; Chen, JianHua ; Wang, XuHong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c369t-1cf9522b317e12380d4f0c72d2aa49f538512e5a33344d15ea55b03b96678ac43</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Apatite</topic><topic>Chlorapatite (Clap)</topic><topic>Combustion</topic><topic>Condensed matter: electronic structure, electrical, magnetic, and optical properties</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Fluorapatite</topic><topic>Fluorapatite (Fap)</topic><topic>Fourier transforms</topic><topic>Hydroxyapatite</topic><topic>Hydroxyapatite (HAP)</topic><topic>Infrared spectroscopy</topic><topic>Physics</topic><topic>Rietveld refinement</topic><topic>Scanning electron microscopy</topic><topic>Solution combustion method</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhao, Junjie</creatorcontrib><creatorcontrib>Dong, Xiaochen</creatorcontrib><creatorcontrib>Bian, Mengmeng</creatorcontrib><creatorcontrib>Zhao, Junfeng</creatorcontrib><creatorcontrib>Zhang, Yao</creatorcontrib><creatorcontrib>Sun, Yue</creatorcontrib><creatorcontrib>Chen, JianHua</creatorcontrib><creatorcontrib>Wang, XuHong</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Applied surface science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhao, Junjie</au><au>Dong, Xiaochen</au><au>Bian, Mengmeng</au><au>Zhao, Junfeng</au><au>Zhang, Yao</au><au>Sun, Yue</au><au>Chen, JianHua</au><au>Wang, XuHong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Solution combustion method for synthesis of nanostructured hydroxyapatite, fluorapatite and chlorapatite</atitle><jtitle>Applied surface science</jtitle><date>2014-09-30</date><risdate>2014</risdate><volume>314</volume><spage>1026</spage><epage>1033</epage><pages>1026-1033</pages><issn>0169-4332</issn><eissn>1873-5584</eissn><abstract>•We report a synthesis of HA, Fap and Clap vio a modified solution combustion method. The nucleation of β-TCP was inhibited in the abundant-calcium system (Ca/P=2.3>>1.67) in this study. F− brushed into the structure of HA and replace the position of OH− is easier than that of Cl−.
Hydroxyapatite (HAP), fluorapatite (Fap) and chlorapatite (Clap) were prepared by solution combustion method with further annealing at 800°C. The characterization and structural features of the synthesized powders were evaluated by the powder X-ray diffraction (XRD, Fourier transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM) and transmission electron microscopy (TEM) techniques. Characterization results from XRD and Rietveld analysis revealed that OH− in the HAP lattice were gradually substituted with the increase of F− and Cl− content and totally substituted at the molar concentration of 0.28 and 0.6, respectively. The results from FI-IR have also confirmed the incorporation of substituted anions in the apatite structure.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.apsusc.2014.06.075</doi><tpages>8</tpages></addata></record> |
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| subjects | Apatite Chlorapatite (Clap) Combustion Condensed matter: electronic structure, electrical, magnetic, and optical properties Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Exact sciences and technology Fluorapatite Fluorapatite (Fap) Fourier transforms Hydroxyapatite Hydroxyapatite (HAP) Infrared spectroscopy Physics Rietveld refinement Scanning electron microscopy Solution combustion method X-ray diffraction |
| title | Solution combustion method for synthesis of nanostructured hydroxyapatite, fluorapatite and chlorapatite |
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