Polymethacrylate monoliths with immobilized poly-3-mercaptopropyl methylsiloxane film for high-coverage surface functionalization by thiol-ene click reaction

•Poly-3-mercaptopropyl-methylsiloxane film was coated onto methacrylate monolith.•Functional polysiloxane film was then chemically crosslinked to the surface.•Resultant composite materials allow clickable high-density surface functionalization.•Concept was demonstrated by thiol-ene click reaction wi...

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Veröffentlicht in:	Journal of Chromatography A 2014-11, Vol.1367, p.123-130
Hauptverfasser:	Carrasco-Correa, Enrique Javier, Ramis-Ramos, Guillermo, Herrero-Martínez, José Manuel, Lämmerhofer, Michael
Format:	Artikel
Sprache:	eng
Schlagworte:	Analytical chemistry Capillary column Capillary Electrochromatography - methods Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Liquid - instrumentation Exact sciences and technology Hot Temperature Methylmethacrylates - chemistry O-9-tert-butylcarbamoyl quinine Other chromatographic methods Poly-3-mercaptopropyl methylsiloxane Polymethacrylic Acids - chemistry Reactive monolith Reproducibility of Results Siloxanes - chemistry Sulfhydryl Compounds - chemistry Surface Properties Thiol-covered surfaces Thiol-ene click reaction
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