Comparison on photo-initiators for the preparation of methacrylate monolithic columns for capillary electrochromatography

The synthesis of lauryl methacrylate monoliths for capillary electrochromatography by UV polymerization using several free-radical initiators (α,α′-azobisisobutyronitrile, 2,2-dimethoxy-2-phenylacetophenone, dibenzoyl peroxide (BPO) and lauroyl peroxide (LPO)) has been investigated. Using a 1,4-buta...

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Veröffentlicht in:	Journal of Chromatography A 2010-05, Vol.1217 (19), p.3231-3237
Hauptverfasser:	Bernabé-Zafón, V., Beneito-Cambra, M., Simó-Alfonso, E.F., Herrero-Martínez, J.M.
Format:	Artikel
Sprache:	eng
Schlagworte:	2,2-Dimethoxy-2-phenylacetophenone Acetophenones - chemistry Analytical chemistry Benzoyl peroxide Benzoyl Peroxide - chemistry Capillary electrochromatography Capillary Electrochromatography - methods Chemistry Chromatographic methods and physical methods associated with chromatography Exact sciences and technology Lauroyl peroxide Lauryl methacrylate Lipid Peroxides - chemistry Methacrylates - chemical synthesis Methacrylates - chemistry Microscopy, Electron, Scanning Nitriles - chemistry Other chromatographic methods Photo-initiators Photochemistry - methods Reproducibility of Results UV initiation α,α′-Azobisisobutyronitrile
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