A facile synthesis of multi metal-doped rectangular ZnO nanocrystals using a nanocrystalline metal-organic framework template
A multi metal (M: Fe, Co, and Ni)-doped rectangular ZnO nanocrystal (r-ZnO:M) was synthesised using nanocrystalline metal-organic framework-5 (n-MOF-5). After calcination in air, M-inserted n-MOF-5 led to r-ZnO:M of the wurtzite crystal structure with a small amount (
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| Veröffentlicht in: | Nanoscale 2014-10, Vol.6 (19), p.10995-11001 |
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| container_issue | 19 |
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| container_title | Nanoscale |
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| creator | Lee, Dong Ki Park, Jung Hyo Choi, Ji Il Lee, Yeob Kim, Sang Jun Lee, Gyu-Heon Kim, Yong-Hoon Kang, Jeung Ku |
| description | A multi metal (M: Fe, Co, and Ni)-doped rectangular ZnO nanocrystal (r-ZnO:M) was synthesised using nanocrystalline metal-organic framework-5 (n-MOF-5). After calcination in air, M-inserted n-MOF-5 led to r-ZnO:M of the wurtzite crystal structure with a small amount ( |
| doi_str_mv | 10.1039/c4nr03424d |
| format | Article |
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After calcination in air, M-inserted n-MOF-5 led to r-ZnO:M of the wurtzite crystal structure with a small amount (<1%) of spinel ZnM2O4 phase. The inserted metal atoms of r-ZnO:M, replacing the Zn atoms of the wurtzite ZnO structure, were well-dispersed throughout the nanocrystal. Density functional theory calculations not only confirm the structural stability of wurtzite r-ZnO:M and negligible contribution of spinel ZnM2O4 but also elucidate the experimentally observed increase of visible light absorbance and appearance of ferromagnetism upon metal atom doping.</description><identifier>ISSN: 2040-3364</identifier><identifier>EISSN: 2040-3372</identifier><identifier>DOI: 10.1039/c4nr03424d</identifier><identifier>PMID: 25123292</identifier><language>eng</language><publisher>England</publisher><subject>Atomic structure ; Crystal structure ; Density functional theory ; Mathematical analysis ; Metal-organic frameworks ; Nanocrystals ; Spinel ; Wurtzite ; Zinc oxide</subject><ispartof>Nanoscale, 2014-10, Vol.6 (19), p.10995-11001</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c320t-b3b4bdf8f9b6df016b4aebb01d0b6bbbb43d272bd8299394a929dd14a52b73ce3</citedby><cites>FETCH-LOGICAL-c320t-b3b4bdf8f9b6df016b4aebb01d0b6bbbb43d272bd8299394a929dd14a52b73ce3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/25123292$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Lee, Dong Ki</creatorcontrib><creatorcontrib>Park, Jung Hyo</creatorcontrib><creatorcontrib>Choi, Ji Il</creatorcontrib><creatorcontrib>Lee, Yeob</creatorcontrib><creatorcontrib>Kim, Sang Jun</creatorcontrib><creatorcontrib>Lee, Gyu-Heon</creatorcontrib><creatorcontrib>Kim, Yong-Hoon</creatorcontrib><creatorcontrib>Kang, Jeung Ku</creatorcontrib><title>A facile synthesis of multi metal-doped rectangular ZnO nanocrystals using a nanocrystalline metal-organic framework template</title><title>Nanoscale</title><addtitle>Nanoscale</addtitle><description>A multi metal (M: Fe, Co, and Ni)-doped rectangular ZnO nanocrystal (r-ZnO:M) was synthesised using nanocrystalline metal-organic framework-5 (n-MOF-5). After calcination in air, M-inserted n-MOF-5 led to r-ZnO:M of the wurtzite crystal structure with a small amount (<1%) of spinel ZnM2O4 phase. The inserted metal atoms of r-ZnO:M, replacing the Zn atoms of the wurtzite ZnO structure, were well-dispersed throughout the nanocrystal. Density functional theory calculations not only confirm the structural stability of wurtzite r-ZnO:M and negligible contribution of spinel ZnM2O4 but also elucidate the experimentally observed increase of visible light absorbance and appearance of ferromagnetism upon metal atom doping.</description><subject>Atomic structure</subject><subject>Crystal structure</subject><subject>Density functional theory</subject><subject>Mathematical analysis</subject><subject>Metal-organic frameworks</subject><subject>Nanocrystals</subject><subject>Spinel</subject><subject>Wurtzite</subject><subject>Zinc oxide</subject><issn>2040-3364</issn><issn>2040-3372</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><recordid>eNqFkctKw0AUhgdRbK1ufACZpQjRueUyy1KvUCyIbtyEuZzUaDKJMwnShe9utLW482zO4ec73-ZH6JiSc0q4vDDCecIFE3YHjRkRJOI8ZbvbOxEjdBDCKyGJ5AnfRyMWU8aZZGP0OcWFMmUFOKxc9wKhDLgpcN1XXYlr6FQV2aYFiz2YTrllXymPn90CO-Ua41dhIALuQ-mWWP0Nq9LBRtD4pXKlwYVXNXw0_g13ULeV6uAQ7RXDPxxt9gQ9XV89zm6j-eLmbjadR4Yz0kWaa6FtkRVSJ7YgNNFCgdaEWqITPYzglqVM24xJyaVQkklrqVAx0yk3wCfodO1tffPeQ-jyugwGqko5aPqQ04QRkqWcxv-jcUJlygjPBvRsjRrfhOChyFtf1sqvckry72bymbh_-GnmcoBPNt5e12C36G8V_Asem4wB</recordid><startdate>20141007</startdate><enddate>20141007</enddate><creator>Lee, Dong Ki</creator><creator>Park, Jung Hyo</creator><creator>Choi, Ji Il</creator><creator>Lee, Yeob</creator><creator>Kim, Sang Jun</creator><creator>Lee, Gyu-Heon</creator><creator>Kim, Yong-Hoon</creator><creator>Kang, Jeung Ku</creator><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20141007</creationdate><title>A facile synthesis of multi metal-doped rectangular ZnO nanocrystals using a nanocrystalline metal-organic framework template</title><author>Lee, Dong Ki ; Park, Jung Hyo ; Choi, Ji Il ; Lee, Yeob ; Kim, Sang Jun ; Lee, Gyu-Heon ; Kim, Yong-Hoon ; Kang, Jeung Ku</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c320t-b3b4bdf8f9b6df016b4aebb01d0b6bbbb43d272bd8299394a929dd14a52b73ce3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Atomic structure</topic><topic>Crystal structure</topic><topic>Density functional theory</topic><topic>Mathematical analysis</topic><topic>Metal-organic frameworks</topic><topic>Nanocrystals</topic><topic>Spinel</topic><topic>Wurtzite</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lee, Dong Ki</creatorcontrib><creatorcontrib>Park, Jung Hyo</creatorcontrib><creatorcontrib>Choi, Ji Il</creatorcontrib><creatorcontrib>Lee, Yeob</creatorcontrib><creatorcontrib>Kim, Sang Jun</creatorcontrib><creatorcontrib>Lee, Gyu-Heon</creatorcontrib><creatorcontrib>Kim, Yong-Hoon</creatorcontrib><creatorcontrib>Kang, Jeung Ku</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Nanoscale</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lee, Dong Ki</au><au>Park, Jung Hyo</au><au>Choi, Ji Il</au><au>Lee, Yeob</au><au>Kim, Sang Jun</au><au>Lee, Gyu-Heon</au><au>Kim, Yong-Hoon</au><au>Kang, Jeung Ku</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>A facile synthesis of multi metal-doped rectangular ZnO nanocrystals using a nanocrystalline metal-organic framework template</atitle><jtitle>Nanoscale</jtitle><addtitle>Nanoscale</addtitle><date>2014-10-07</date><risdate>2014</risdate><volume>6</volume><issue>19</issue><spage>10995</spage><epage>11001</epage><pages>10995-11001</pages><issn>2040-3364</issn><eissn>2040-3372</eissn><abstract>A multi metal (M: Fe, Co, and Ni)-doped rectangular ZnO nanocrystal (r-ZnO:M) was synthesised using nanocrystalline metal-organic framework-5 (n-MOF-5). After calcination in air, M-inserted n-MOF-5 led to r-ZnO:M of the wurtzite crystal structure with a small amount (<1%) of spinel ZnM2O4 phase. The inserted metal atoms of r-ZnO:M, replacing the Zn atoms of the wurtzite ZnO structure, were well-dispersed throughout the nanocrystal. Density functional theory calculations not only confirm the structural stability of wurtzite r-ZnO:M and negligible contribution of spinel ZnM2O4 but also elucidate the experimentally observed increase of visible light absorbance and appearance of ferromagnetism upon metal atom doping.</abstract><cop>England</cop><pmid>25123292</pmid><doi>10.1039/c4nr03424d</doi><tpages>7</tpages></addata></record> |
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| ispartof | Nanoscale, 2014-10, Vol.6 (19), p.10995-11001 |
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| language | eng |
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| source | Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection |
| subjects | Atomic structure Crystal structure Density functional theory Mathematical analysis Metal-organic frameworks Nanocrystals Spinel Wurtzite Zinc oxide |
| title | A facile synthesis of multi metal-doped rectangular ZnO nanocrystals using a nanocrystalline metal-organic framework template |
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