Extraction and identification of a plasticizer, di-(2-ethylhexyl)phthalate, from a plastic bag containing contaminated corn

Residues of the plasticizer di-(2-ethylhexyl)phthalate (DEHP) were extracted along with deoxynivalenol from plastic bags containing corn contaminated by the fungus Fusarium graminearum. Residue concentration/extraction entailed a series of silica gel-400 chromatography columns followed by purificati...

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Veröffentlicht in:Archives of environmental contamination and toxicology 1991-04, Vol.20 (3), p.437-440
Hauptverfasser: Cohen, H. (Agriculture Canada, Ottawa, Ontario, Canada), Charrier, C, Sarfaty, J
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creator Cohen, H. (Agriculture Canada, Ottawa, Ontario, Canada)
Charrier, C
Sarfaty, J
description Residues of the plasticizer di-(2-ethylhexyl)phthalate (DEHP) were extracted along with deoxynivalenol from plastic bags containing corn contaminated by the fungus Fusarium graminearum. Residue concentration/extraction entailed a series of silica gel-400 chromatography columns followed by purification by semi-preparative column chromatography. Identification was facilitated by nuclear magnetic response and mass spectrometry, and quantification of DEHP was also performed by high performance liquid chromatography. Leaching can introduce DEHP into corn whether the latter is contaminated with fungi or not.
doi_str_mv 10.1007/BF01064417
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identifier ISSN: 0090-4341
ispartof Archives of environmental contamination and toxicology, 1991-04, Vol.20 (3), p.437-440
issn 0090-4341
1432-0703
language eng
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source SpringerLink (Online service)
subjects ALIMENTOS
Biological and medical sciences
CONTAMINACION
CONTAMINATION
FOODS
Fusarium graminearum
GIBBERELLA
GIBBERELLA ZEAE
IDENTIFICACION
IDENTIFICATION
MAIS
MAIZ
MAIZE
MATIERE PLASTIQUE
Medical sciences
Plant poisons toxicology
PLASTICOS
PLASTICS
PRODUIT ALIMENTAIRE
RESIDU
RESIDUES
RESIDUOS
SAC
SACKS
SACOS
Toxicology
Zea mays
title Extraction and identification of a plasticizer, di-(2-ethylhexyl)phthalate, from a plastic bag containing contaminated corn
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