Regulation of Cu precipitation by intercritical tempering in a HSLA steel
A multistep heat treatment process consisting of intercritical tempering between quenching and conventional tempering contributed to the development of a ferrite–martensite dual-phase structure in a Ni- and Cu-containing high-strength low-alloy steel. By using electron backscatter diffraction and sc...
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Veröffentlicht in: | Journal of materials research 2014-04, Vol.29 (8), p.950-958 |
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description | A multistep heat treatment process consisting of intercritical tempering between quenching and conventional tempering contributed to the development of a ferrite–martensite dual-phase structure in a Ni- and Cu-containing high-strength low-alloy steel. By using electron backscatter diffraction and scanning transmission electron microscopy, the microstructures were found to have an elongated lathlike morphology with carbide and Cu precipitates located especially at the boundaries of ferrite and martensite crystals. Atom probe tomography reveals at atomic scale the existence of solute-diluted ferrite and solute-rich martensite, and the later phase was considered to be transformed from the reverse austenite that was formed during intercritical tempering. Cu precipitation greatly correlates with the microconstituents, resulting in different distributional characteristics of Cu precipitates within these two phases and at their boundaries. It is a promising process to utilize Cu precipitation strengthening and phase transformation toughening simultaneously in alloy steels. |
doi_str_mv | 10.1557/jmr.2014.66 |
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By using electron backscatter diffraction and scanning transmission electron microscopy, the microstructures were found to have an elongated lathlike morphology with carbide and Cu precipitates located especially at the boundaries of ferrite and martensite crystals. Atom probe tomography reveals at atomic scale the existence of solute-diluted ferrite and solute-rich martensite, and the later phase was considered to be transformed from the reverse austenite that was formed during intercritical tempering. Cu precipitation greatly correlates with the microconstituents, resulting in different distributional characteristics of Cu precipitates within these two phases and at their boundaries. It is a promising process to utilize Cu precipitation strengthening and phase transformation toughening simultaneously in alloy steels.</description><identifier>ISSN: 0884-2914</identifier><identifier>EISSN: 2044-5326</identifier><identifier>DOI: 10.1557/jmr.2014.66</identifier><identifier>CODEN: JMREEE</identifier><language>eng</language><publisher>New York, USA: Cambridge University Press</publisher><subject>Applied and Technical Physics ; Biomaterials ; Boundaries ; Copper ; Experiments ; Ferrite ; Grain boundaries ; Heat treating ; High strength low alloy steels ; Inorganic Chemistry ; Martensite ; Materials Engineering ; Materials research ; Materials Science ; Metalworking industry ; Microstructure ; Morphology ; Nanotechnology ; Precipitates ; Precipitation ; Precipitation hardening ; Steel ; Studies ; Tempering</subject><ispartof>Journal of materials research, 2014-04, Vol.29 (8), p.950-958</ispartof><rights>Copyright © Materials Research Society 2014</rights><rights>The Materials Research Society 2014</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c369t-a7ced53504ed9a36b7981f34bda8d8ec46e14ff6a6d37309743ffd7725e10c943</citedby><cites>FETCH-LOGICAL-c369t-a7ced53504ed9a36b7981f34bda8d8ec46e14ff6a6d37309743ffd7725e10c943</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1557/jmr.2014.66$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://www.cambridge.org/core/product/identifier/S0884291414000661/type/journal_article$$EHTML$$P50$$Gcambridge$$H</linktohtml><link.rule.ids>164,314,776,780,27901,27902,41464,42533,51294,55603</link.rule.ids></links><search><creatorcontrib>Liu, Qing-Dong</creatorcontrib><creatorcontrib>Gu, Jian-Feng</creatorcontrib><creatorcontrib>Li, Chuan-Wei</creatorcontrib><title>Regulation of Cu precipitation by intercritical tempering in a HSLA steel</title><title>Journal of materials research</title><addtitle>Journal of Materials Research</addtitle><addtitle>J. Mater. Res</addtitle><description>A multistep heat treatment process consisting of intercritical tempering between quenching and conventional tempering contributed to the development of a ferrite–martensite dual-phase structure in a Ni- and Cu-containing high-strength low-alloy steel. By using electron backscatter diffraction and scanning transmission electron microscopy, the microstructures were found to have an elongated lathlike morphology with carbide and Cu precipitates located especially at the boundaries of ferrite and martensite crystals. Atom probe tomography reveals at atomic scale the existence of solute-diluted ferrite and solute-rich martensite, and the later phase was considered to be transformed from the reverse austenite that was formed during intercritical tempering. Cu precipitation greatly correlates with the microconstituents, resulting in different distributional characteristics of Cu precipitates within these two phases and at their boundaries. It is a promising process to utilize Cu precipitation strengthening and phase transformation toughening simultaneously in alloy steels.</description><subject>Applied and Technical Physics</subject><subject>Biomaterials</subject><subject>Boundaries</subject><subject>Copper</subject><subject>Experiments</subject><subject>Ferrite</subject><subject>Grain boundaries</subject><subject>Heat treating</subject><subject>High strength low alloy steels</subject><subject>Inorganic Chemistry</subject><subject>Martensite</subject><subject>Materials Engineering</subject><subject>Materials research</subject><subject>Materials Science</subject><subject>Metalworking industry</subject><subject>Microstructure</subject><subject>Morphology</subject><subject>Nanotechnology</subject><subject>Precipitates</subject><subject>Precipitation</subject><subject>Precipitation hardening</subject><subject>Steel</subject><subject>Studies</subject><subject>Tempering</subject><issn>0884-2914</issn><issn>2044-5326</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9kEtLAzEURoMoWKsr_0DAjaBTk0kmmVmW4qNQEHyshzRzU1LmZZJZ9N-bYboQEVcXPg6Hy0HompIFzTL5sG_cIiWUL4Q4QbOUcJ5kLBWnaEbynCdpQfk5uvB-TwjNiOQztH6D3VCrYLsWdwavBtw70La3Ydq2B2zbAE47G6xWNQ7Q9OBsu4s7VvjlfbPEPgDUl-jMqNrD1fHO0efT48fqJdm8Pq9Xy02imShCoqSGKmMZ4VAViomtLHJqGN9WKq9y0FwA5cYIJSomGSkkZ8ZUUqYZUKILzubodvL2rvsawIeysV5DXasWusGXMUQhiWRMRPTmF7rvBtfG7yIVOxEqeBqpu4nSrvPegSl7ZxvlDiUlo02WMWs5Zi3F6LyfaN-PFcD9cP6JJ0e5arbOVjv4n_8GguyHmg</recordid><startdate>20140428</startdate><enddate>20140428</enddate><creator>Liu, Qing-Dong</creator><creator>Gu, Jian-Feng</creator><creator>Li, Chuan-Wei</creator><general>Cambridge University Press</general><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>0U~</scope><scope>1-H</scope><scope>3V.</scope><scope>7SR</scope><scope>7WY</scope><scope>7WZ</scope><scope>7XB</scope><scope>87Z</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8FL</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FRNLG</scope><scope>F~G</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>K60</scope><scope>K6~</scope><scope>KB.</scope><scope>L.-</scope><scope>L.0</scope><scope>M0C</scope><scope>PDBOC</scope><scope>PQBIZ</scope><scope>PQBZA</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>Q9U</scope><scope>S0W</scope></search><sort><creationdate>20140428</creationdate><title>Regulation of Cu precipitation by intercritical tempering in a HSLA steel</title><author>Liu, Qing-Dong ; Gu, Jian-Feng ; Li, Chuan-Wei</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c369t-a7ced53504ed9a36b7981f34bda8d8ec46e14ff6a6d37309743ffd7725e10c943</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Applied and Technical Physics</topic><topic>Biomaterials</topic><topic>Boundaries</topic><topic>Copper</topic><topic>Experiments</topic><topic>Ferrite</topic><topic>Grain boundaries</topic><topic>Heat treating</topic><topic>High strength low alloy steels</topic><topic>Inorganic Chemistry</topic><topic>Martensite</topic><topic>Materials Engineering</topic><topic>Materials research</topic><topic>Materials Science</topic><topic>Metalworking industry</topic><topic>Microstructure</topic><topic>Morphology</topic><topic>Nanotechnology</topic><topic>Precipitates</topic><topic>Precipitation</topic><topic>Precipitation hardening</topic><topic>Steel</topic><topic>Studies</topic><topic>Tempering</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Liu, Qing-Dong</creatorcontrib><creatorcontrib>Gu, Jian-Feng</creatorcontrib><creatorcontrib>Li, Chuan-Wei</creatorcontrib><collection>CrossRef</collection><collection>Global News & ABI/Inform Professional</collection><collection>Trade PRO</collection><collection>ProQuest Central (Corporate)</collection><collection>Engineered Materials Abstracts</collection><collection>ABI/INFORM Collection</collection><collection>ABI/INFORM Global (PDF only)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ABI/INFORM Global (Alumni Edition)</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ABI/INFORM Collection (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Business Premium Collection</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Business Premium Collection (Alumni)</collection><collection>ABI/INFORM Global (Corporate)</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>ProQuest Business Collection (Alumni Edition)</collection><collection>ProQuest Business Collection</collection><collection>Materials Science Database</collection><collection>ABI/INFORM Professional Advanced</collection><collection>ABI/INFORM Professional Standard</collection><collection>ABI/INFORM Global</collection><collection>Materials Science Collection</collection><collection>ProQuest One Business</collection><collection>ProQuest One Business (Alumni)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central Basic</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Qing-Dong</au><au>Gu, Jian-Feng</au><au>Li, Chuan-Wei</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Regulation of Cu precipitation by intercritical tempering in a HSLA steel</atitle><jtitle>Journal of materials research</jtitle><stitle>Journal of Materials Research</stitle><addtitle>J. Mater. Res</addtitle><date>2014-04-28</date><risdate>2014</risdate><volume>29</volume><issue>8</issue><spage>950</spage><epage>958</epage><pages>950-958</pages><issn>0884-2914</issn><eissn>2044-5326</eissn><coden>JMREEE</coden><abstract>A multistep heat treatment process consisting of intercritical tempering between quenching and conventional tempering contributed to the development of a ferrite–martensite dual-phase structure in a Ni- and Cu-containing high-strength low-alloy steel. By using electron backscatter diffraction and scanning transmission electron microscopy, the microstructures were found to have an elongated lathlike morphology with carbide and Cu precipitates located especially at the boundaries of ferrite and martensite crystals. Atom probe tomography reveals at atomic scale the existence of solute-diluted ferrite and solute-rich martensite, and the later phase was considered to be transformed from the reverse austenite that was formed during intercritical tempering. Cu precipitation greatly correlates with the microconstituents, resulting in different distributional characteristics of Cu precipitates within these two phases and at their boundaries. It is a promising process to utilize Cu precipitation strengthening and phase transformation toughening simultaneously in alloy steels.</abstract><cop>New York, USA</cop><pub>Cambridge University Press</pub><doi>10.1557/jmr.2014.66</doi><tpages>9</tpages></addata></record> |
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subjects | Applied and Technical Physics Biomaterials Boundaries Copper Experiments Ferrite Grain boundaries Heat treating High strength low alloy steels Inorganic Chemistry Martensite Materials Engineering Materials research Materials Science Metalworking industry Microstructure Morphology Nanotechnology Precipitates Precipitation Precipitation hardening Steel Studies Tempering |
title | Regulation of Cu precipitation by intercritical tempering in a HSLA steel |
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