Doped polyaniline/multiwalled carbon nanotube composites: Preparation and characterization
Polyaniline (PANI)/multiwalled carbon nanotube (MWNT) composites with a uniform tubular structure were prepared from in situ polymerization by dissolving amino‐functionalized MWNT (a‐MWNT) in aniline monomer. For this the oxidized multiwalled nanotube was functionalized with ethylenediamine, which p...
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| Veröffentlicht in: | Polymer composites 2013-07, Vol.34 (7), p.1119-1125 |
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| creator | Cui, Liqiang Yu, Junsheng Lv, Yinghai Li, Guijiang Zhou, Shixue |
| description | Polyaniline (PANI)/multiwalled carbon nanotube (MWNT) composites with a uniform tubular structure were prepared from in situ polymerization by dissolving amino‐functionalized MWNT (a‐MWNT) in aniline monomer. For this the oxidized multiwalled nanotube was functionalized with ethylenediamine, which provided ethylenediamine functional group on the MWNT surface confirmed by Fourier‐transform infrared spectra (FT‐IR). The a‐MWNT was dissolved in aniline monomer, and the in situ polymerization of aniline in the presence of these well dispersed nanotubes yielded a novel tubular composite of carbon nanotube having an ordered uniform encapsulation of doped polyaniline. Transmission electron microscopy (TEM) and scanning electron microscopy (SEM) showed that the nanotubes were coated with a PANI layer. The thermal stability and electrical conductivity of the PANI /MWNTs composites were characterized by thermogravimetric analysis (TGA) and conventional four‐probe method respectively. Compared with pure PANI, the electrical conductivity and the decomposition temperature of the MWNTs/PANI composites increased with the enhancement of MWNT content in PANI matrix. POLYM. COMPOS., 34:1119–1125, 2013. © 2013 Society of Plastics Engineers |
| doi_str_mv | 10.1002/pc.22520 |
| format | Article |
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For this the oxidized multiwalled nanotube was functionalized with ethylenediamine, which provided ethylenediamine functional group on the MWNT surface confirmed by Fourier‐transform infrared spectra (FT‐IR). The a‐MWNT was dissolved in aniline monomer, and the in situ polymerization of aniline in the presence of these well dispersed nanotubes yielded a novel tubular composite of carbon nanotube having an ordered uniform encapsulation of doped polyaniline. Transmission electron microscopy (TEM) and scanning electron microscopy (SEM) showed that the nanotubes were coated with a PANI layer. The thermal stability and electrical conductivity of the PANI /MWNTs composites were characterized by thermogravimetric analysis (TGA) and conventional four‐probe method respectively. Compared with pure PANI, the electrical conductivity and the decomposition temperature of the MWNTs/PANI composites increased with the enhancement of MWNT content in PANI matrix. POLYM. COMPOS., 34:1119–1125, 2013. © 2013 Society of Plastics Engineers</description><identifier>ISSN: 0272-8397</identifier><identifier>EISSN: 1548-0569</identifier><identifier>DOI: 10.1002/pc.22520</identifier><identifier>CODEN: PCOMDI</identifier><language>eng</language><publisher>Hoboken, NJ: Blackwell Publishing Ltd</publisher><subject>Aniline ; Applied sciences ; Composites ; Dissolution ; Exact sciences and technology ; Forms of application and semi-finished materials ; Multi wall carbon nanotubes ; Nanostructure ; Polyanilines ; Polymer industry, paints, wood ; Polymer matrix composites ; Polymerization ; Scanning electron microscopy ; Technology of polymers</subject><ispartof>Polymer composites, 2013-07, Vol.34 (7), p.1119-1125</ispartof><rights>2013 Society of Plastics Engineers</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3940-aba05baf2623bc8389806a8d431155ad5ca9be1dc42b23b9e73d87db5585c5d93</citedby><cites>FETCH-LOGICAL-c3940-aba05baf2623bc8389806a8d431155ad5ca9be1dc42b23b9e73d87db5585c5d93</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fpc.22520$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fpc.22520$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,776,780,1411,27901,27902,45550,45551</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=27531236$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Cui, Liqiang</creatorcontrib><creatorcontrib>Yu, Junsheng</creatorcontrib><creatorcontrib>Lv, Yinghai</creatorcontrib><creatorcontrib>Li, Guijiang</creatorcontrib><creatorcontrib>Zhou, Shixue</creatorcontrib><title>Doped polyaniline/multiwalled carbon nanotube composites: Preparation and characterization</title><title>Polymer composites</title><addtitle>Polym. Compos</addtitle><description>Polyaniline (PANI)/multiwalled carbon nanotube (MWNT) composites with a uniform tubular structure were prepared from in situ polymerization by dissolving amino‐functionalized MWNT (a‐MWNT) in aniline monomer. For this the oxidized multiwalled nanotube was functionalized with ethylenediamine, which provided ethylenediamine functional group on the MWNT surface confirmed by Fourier‐transform infrared spectra (FT‐IR). The a‐MWNT was dissolved in aniline monomer, and the in situ polymerization of aniline in the presence of these well dispersed nanotubes yielded a novel tubular composite of carbon nanotube having an ordered uniform encapsulation of doped polyaniline. Transmission electron microscopy (TEM) and scanning electron microscopy (SEM) showed that the nanotubes were coated with a PANI layer. The thermal stability and electrical conductivity of the PANI /MWNTs composites were characterized by thermogravimetric analysis (TGA) and conventional four‐probe method respectively. Compared with pure PANI, the electrical conductivity and the decomposition temperature of the MWNTs/PANI composites increased with the enhancement of MWNT content in PANI matrix. POLYM. COMPOS., 34:1119–1125, 2013. © 2013 Society of Plastics Engineers</description><subject>Aniline</subject><subject>Applied sciences</subject><subject>Composites</subject><subject>Dissolution</subject><subject>Exact sciences and technology</subject><subject>Forms of application and semi-finished materials</subject><subject>Multi wall carbon nanotubes</subject><subject>Nanostructure</subject><subject>Polyanilines</subject><subject>Polymer industry, paints, wood</subject><subject>Polymer matrix composites</subject><subject>Polymerization</subject><subject>Scanning electron microscopy</subject><subject>Technology of polymers</subject><issn>0272-8397</issn><issn>1548-0569</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNp10F1LHDEUgOEgFdxqwZ-wUITejOZj8zHeybZVUaoXtgu9CWcyWcw2m0yTGXT99UZ3XaHQq3AODy_hIHRI8DHBmJ505phSTvEOGhE-URXmov6ARphKWilWyz30MedFkUQINkK_v8bOtuMu-hUE512wJ8vB9-4BvC97A6mJYRwgxH5o7NjEZRez620-Hd8m20GC3hUAodj7MpneJvf0ujxAu3Pw2X7avPvo5_dvd9OL6vrm_HJ6dl0ZVk9wBQ1g3sCcCsoao5iqFRag2gkjhHNouYG6saQ1E9oUUVvJWiXbhnPFDW9rto--rLtdin8Hm3u9dNlY7yHYOGRdKgQrgdkL_fwPXcQhhfK7ohimghAp34MmxZyTnesuuSWklSZYvxxZd0a_HrnQo00QsgE_TxCMy1tPJWeEMlFctXYPztvVf3v6dvrW3XiXe_u49ZD-aCGZ5Hr241xP6dVM_qovtGDPrHCZZQ</recordid><startdate>201307</startdate><enddate>201307</enddate><creator>Cui, Liqiang</creator><creator>Yu, Junsheng</creator><creator>Lv, Yinghai</creator><creator>Li, Guijiang</creator><creator>Zhou, Shixue</creator><general>Blackwell Publishing Ltd</general><general>Wiley</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope><scope>7SP</scope><scope>7U5</scope><scope>L7M</scope></search><sort><creationdate>201307</creationdate><title>Doped polyaniline/multiwalled carbon nanotube composites: Preparation and characterization</title><author>Cui, Liqiang ; Yu, Junsheng ; Lv, Yinghai ; Li, Guijiang ; Zhou, Shixue</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3940-aba05baf2623bc8389806a8d431155ad5ca9be1dc42b23b9e73d87db5585c5d93</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Aniline</topic><topic>Applied sciences</topic><topic>Composites</topic><topic>Dissolution</topic><topic>Exact sciences and technology</topic><topic>Forms of application and semi-finished materials</topic><topic>Multi wall carbon nanotubes</topic><topic>Nanostructure</topic><topic>Polyanilines</topic><topic>Polymer industry, paints, wood</topic><topic>Polymer matrix composites</topic><topic>Polymerization</topic><topic>Scanning electron microscopy</topic><topic>Technology of polymers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Cui, Liqiang</creatorcontrib><creatorcontrib>Yu, Junsheng</creatorcontrib><creatorcontrib>Lv, Yinghai</creatorcontrib><creatorcontrib>Li, Guijiang</creatorcontrib><creatorcontrib>Zhou, Shixue</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Electronics & Communications Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Polymer composites</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Cui, Liqiang</au><au>Yu, Junsheng</au><au>Lv, Yinghai</au><au>Li, Guijiang</au><au>Zhou, Shixue</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Doped polyaniline/multiwalled carbon nanotube composites: Preparation and characterization</atitle><jtitle>Polymer composites</jtitle><addtitle>Polym. Compos</addtitle><date>2013-07</date><risdate>2013</risdate><volume>34</volume><issue>7</issue><spage>1119</spage><epage>1125</epage><pages>1119-1125</pages><issn>0272-8397</issn><eissn>1548-0569</eissn><coden>PCOMDI</coden><abstract>Polyaniline (PANI)/multiwalled carbon nanotube (MWNT) composites with a uniform tubular structure were prepared from in situ polymerization by dissolving amino‐functionalized MWNT (a‐MWNT) in aniline monomer. For this the oxidized multiwalled nanotube was functionalized with ethylenediamine, which provided ethylenediamine functional group on the MWNT surface confirmed by Fourier‐transform infrared spectra (FT‐IR). The a‐MWNT was dissolved in aniline monomer, and the in situ polymerization of aniline in the presence of these well dispersed nanotubes yielded a novel tubular composite of carbon nanotube having an ordered uniform encapsulation of doped polyaniline. Transmission electron microscopy (TEM) and scanning electron microscopy (SEM) showed that the nanotubes were coated with a PANI layer. The thermal stability and electrical conductivity of the PANI /MWNTs composites were characterized by thermogravimetric analysis (TGA) and conventional four‐probe method respectively. Compared with pure PANI, the electrical conductivity and the decomposition temperature of the MWNTs/PANI composites increased with the enhancement of MWNT content in PANI matrix. POLYM. COMPOS., 34:1119–1125, 2013. © 2013 Society of Plastics Engineers</abstract><cop>Hoboken, NJ</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1002/pc.22520</doi><tpages>7</tpages></addata></record> |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Aniline Applied sciences Composites Dissolution Exact sciences and technology Forms of application and semi-finished materials Multi wall carbon nanotubes Nanostructure Polyanilines Polymer industry, paints, wood Polymer matrix composites Polymerization Scanning electron microscopy Technology of polymers |
| title | Doped polyaniline/multiwalled carbon nanotube composites: Preparation and characterization |
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