Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material

ODS steels are promising materials for Sodium cooled Fast Reactors since their fine distribution of nano-clusters confers excellent mechanical properties. However, the nano-feature stability needs to be assessed under neutron irradiation. Before irradiation, the characterizations show that nano-part...

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Veröffentlicht in:Journal of nuclear materials 2014-01, Vol.444 (1-3), p.314-322
Hauptverfasser: Ribis, J., Lozano-Perez, S.
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description ODS steels are promising materials for Sodium cooled Fast Reactors since their fine distribution of nano-clusters confers excellent mechanical properties. However, the nano-feature stability needs to be assessed under neutron irradiation. Before irradiation, the characterizations show that nano-particles are finely distributed within the ferritic matrix and are identified to have a pyrochlore type structure. After irradiation of the MA957 alloy in the Phenix French reactor at 412°C up to 50dpa and 430°C up to 75dpa, transmission electron microscopy characterization reveals a very slight density fall but no distinguishable difference in nano-features size before and after irradiation. In addition, after both irradiations, the nano-oxides are still (Y, Ti, O) compounds with orientation relationship with the matrix. A multislice simulation of high resolution images suggests that nano-particles still have a fcc pyrochlore type structure after irradiation. A possible change of lattice parameter seems to be highlighted, possibly due to disordering by cascade effect.
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However, the nano-feature stability needs to be assessed under neutron irradiation. Before irradiation, the characterizations show that nano-particles are finely distributed within the ferritic matrix and are identified to have a pyrochlore type structure. After irradiation of the MA957 alloy in the Phenix French reactor at 412°C up to 50dpa and 430°C up to 75dpa, transmission electron microscopy characterization reveals a very slight density fall but no distinguishable difference in nano-features size before and after irradiation. In addition, after both irradiations, the nano-oxides are still (Y, Ti, O) compounds with orientation relationship with the matrix. A multislice simulation of high resolution images suggests that nano-particles still have a fcc pyrochlore type structure after irradiation. 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source Elsevier ScienceDirect Journals
subjects Applied sciences
Condensed matter: structure, mechanical and thermal properties
Energy
Energy. Thermal use of fuels
Exact sciences and technology
Ferrous alloys
Fission nuclear power plants
Installations for energy generation and conversion: thermal and electrical energy
Irradiation
Metals and alloys
Nanostructure
Neutron irradiation
Nuclear power generation
Nuclear reactor components
Nuclear reactors
Physics
Pyrochlores
Radiation effects on specific materials
Stability
Structure of solids and liquids
crystallography
Superalloys
title Nano-cluster stability following neutron irradiation in MA957 oxide dispersion strengthened material
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