Ionic Liquid-Based One-Step Micellar Extraction of Multiclass Polar Compounds from Hawthorn Fruits by Ultrahigh-Performance Liquid Chromatography Coupled with Quadrupole Time-of-Flight Tandem Mass Spectrometry
An ionic liquid (IL)-based one-step micellar extraction procedure was developed for the extraction of multiclass polar analytes (protocatechuic acid, chlorogenic acid, epicatechin, hyperoside, isoquercitrin, quercetin) from hawthorn fruits and their determination using ultrahigh-performance liquid c...
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| Veröffentlicht in: | Journal of agricultural and food chemistry 2014-06, Vol.62 (23), p.5275-5280 |
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| container_title | Journal of agricultural and food chemistry |
| container_volume | 62 |
| creator | Hu, Shuai-Shuai Yi, Ling Li, Xing-Ying Cao, Jun Ye, Li-Hong Cao, Wan Da, Jian-Hua Dai, Han-Bin Liu, Xiao-Juan |
| description | An ionic liquid (IL)-based one-step micellar extraction procedure was developed for the extraction of multiclass polar analytes (protocatechuic acid, chlorogenic acid, epicatechin, hyperoside, isoquercitrin, quercetin) from hawthorn fruits and their determination using ultrahigh-performance liquid chromatography coupled with quadrupole time-of-flight tandem mass spectrometry (UHPLC-Q-TOF/MS). Compared to conventional organic solvent extractions, this newly proposed method was much easier, more sensitive, environmentally friendly, and effective as well. Several important parameters influencing the micellar extraction efficiency are discussed, such as selection of ILs, surfactant concentration, and extraction time. Under the optimal conditions, good linearity was achieved for each analyte with correlation coefficients (r 2) ranging from 0.9934 to 0.9999, and the recovery values ranged from 89.3 to 106% with relative standard deviations lower than 5.5%. Results suggest that the IL-based one-step micellar extraction could be an alternative and promising means in future food analysis. |
| doi_str_mv | 10.1021/jf501171w |
| format | Article |
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Compared to conventional organic solvent extractions, this newly proposed method was much easier, more sensitive, environmentally friendly, and effective as well. Several important parameters influencing the micellar extraction efficiency are discussed, such as selection of ILs, surfactant concentration, and extraction time. Under the optimal conditions, good linearity was achieved for each analyte with correlation coefficients (r 2) ranging from 0.9934 to 0.9999, and the recovery values ranged from 89.3 to 106% with relative standard deviations lower than 5.5%. Results suggest that the IL-based one-step micellar extraction could be an alternative and promising means in future food analysis.</description><identifier>ISSN: 0021-8561</identifier><identifier>EISSN: 1520-5118</identifier><identifier>DOI: 10.1021/jf501171w</identifier><identifier>PMID: 24845828</identifier><language>eng</language><publisher>United States: American Chemical Society</publisher><subject>Chemical Fractionation - methods ; chlorogenic acid ; Chromatography, High Pressure Liquid - methods ; correlation ; Crataegus ; Crataegus - chemistry ; epicatechin ; food analysis ; Fruit - chemistry ; fruits ; ionic liquids ; Ionic Liquids - chemistry ; isoquercitrin ; Plant Extracts - chemistry ; Plant Extracts - isolation & purification ; polar compounds ; protocatechuic acid ; quercetin ; surfactants ; tandem mass spectrometry ; Tandem Mass Spectrometry - methods ; ultra-performance liquid chromatography</subject><ispartof>Journal of agricultural and food chemistry, 2014-06, Vol.62 (23), p.5275-5280</ispartof><rights>Copyright © 2014 American Chemical Society</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a339t-afb54c24dccb0e35c30a9fa62005c5ea421c748ba722c07b399fd59e0bdfae063</citedby><cites>FETCH-LOGICAL-a339t-afb54c24dccb0e35c30a9fa62005c5ea421c748ba722c07b399fd59e0bdfae063</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/jf501171w$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/jf501171w$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,2765,27076,27924,27925,56738,56788</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/24845828$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Hu, Shuai-Shuai</creatorcontrib><creatorcontrib>Yi, Ling</creatorcontrib><creatorcontrib>Li, Xing-Ying</creatorcontrib><creatorcontrib>Cao, Jun</creatorcontrib><creatorcontrib>Ye, Li-Hong</creatorcontrib><creatorcontrib>Cao, Wan</creatorcontrib><creatorcontrib>Da, Jian-Hua</creatorcontrib><creatorcontrib>Dai, Han-Bin</creatorcontrib><creatorcontrib>Liu, Xiao-Juan</creatorcontrib><title>Ionic Liquid-Based One-Step Micellar Extraction of Multiclass Polar Compounds from Hawthorn Fruits by Ultrahigh-Performance Liquid Chromatography Coupled with Quadrupole Time-of-Flight Tandem Mass Spectrometry</title><title>Journal of agricultural and food chemistry</title><addtitle>J. Agric. Food Chem</addtitle><description>An ionic liquid (IL)-based one-step micellar extraction procedure was developed for the extraction of multiclass polar analytes (protocatechuic acid, chlorogenic acid, epicatechin, hyperoside, isoquercitrin, quercetin) from hawthorn fruits and their determination using ultrahigh-performance liquid chromatography coupled with quadrupole time-of-flight tandem mass spectrometry (UHPLC-Q-TOF/MS). Compared to conventional organic solvent extractions, this newly proposed method was much easier, more sensitive, environmentally friendly, and effective as well. Several important parameters influencing the micellar extraction efficiency are discussed, such as selection of ILs, surfactant concentration, and extraction time. Under the optimal conditions, good linearity was achieved for each analyte with correlation coefficients (r 2) ranging from 0.9934 to 0.9999, and the recovery values ranged from 89.3 to 106% with relative standard deviations lower than 5.5%. Results suggest that the IL-based one-step micellar extraction could be an alternative and promising means in future food analysis.</description><subject>Chemical Fractionation - methods</subject><subject>chlorogenic acid</subject><subject>Chromatography, High Pressure Liquid - methods</subject><subject>correlation</subject><subject>Crataegus</subject><subject>Crataegus - chemistry</subject><subject>epicatechin</subject><subject>food analysis</subject><subject>Fruit - chemistry</subject><subject>fruits</subject><subject>ionic liquids</subject><subject>Ionic Liquids - chemistry</subject><subject>isoquercitrin</subject><subject>Plant Extracts - chemistry</subject><subject>Plant Extracts - isolation & purification</subject><subject>polar compounds</subject><subject>protocatechuic acid</subject><subject>quercetin</subject><subject>surfactants</subject><subject>tandem mass spectrometry</subject><subject>Tandem Mass Spectrometry - methods</subject><subject>ultra-performance liquid chromatography</subject><issn>0021-8561</issn><issn>1520-5118</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNptkb9u2zAQh4WiReOmHfoCLZcCzcCUpERLGlMjbgLYSArbs3CiSIuGJCr8A9eP2TcqHbuZMt1w3313uF-SfKbkmhJGf-wUJ5TmdP8mmVDOCOaUFm-TCYlNXPApvUg-OLcjhBQ8J--TC5YVGS9YMUn-3ptBC7TQT0E3-Cc42aCHQeKVlyNaaiG7Diy6_eMtCK_NgIxCy9B5LTpwDj2aY3tm-tGEoXFIWdOjO9j71tgBzW3Q3qH6gDZdFLR62-JHaZWxPQxCnreiWRunwJuthbE9RFsYu3jGXvsW_Q7Q2DCaTqK17iU2Cs-76PFoDUMje7Q8nrEapfBRIr09fEzeKeic_HSul8lmfrue3eHFw6_72c0CQ5qWHoOqeSZY1ghRE5lykRIoFUwZIVxwCRmjIs-KGnLGBMnrtCxVw0tJ6kaBJNP0Mvl-8o7WPAXpfNVr9_yvQZrgKspTzihjOYvo1QkV1jhnpapGq3uwh4qS6phg9ZJgZL-ctaHuZfNC_o8sAl9PgAJTwdZqV21WjNApiYayoGUkvp0IEK7amWCH-IdXVv0DTqSw6w</recordid><startdate>20140611</startdate><enddate>20140611</enddate><creator>Hu, Shuai-Shuai</creator><creator>Yi, Ling</creator><creator>Li, Xing-Ying</creator><creator>Cao, Jun</creator><creator>Ye, Li-Hong</creator><creator>Cao, Wan</creator><creator>Da, Jian-Hua</creator><creator>Dai, Han-Bin</creator><creator>Liu, Xiao-Juan</creator><general>American Chemical Society</general><general>American Chemical Society, Books and Journals Division</general><scope>FBQ</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20140611</creationdate><title>Ionic Liquid-Based One-Step Micellar Extraction of Multiclass Polar Compounds from Hawthorn Fruits by Ultrahigh-Performance Liquid Chromatography Coupled with Quadrupole Time-of-Flight Tandem Mass Spectrometry</title><author>Hu, Shuai-Shuai ; Yi, Ling ; Li, Xing-Ying ; Cao, Jun ; Ye, Li-Hong ; Cao, Wan ; Da, Jian-Hua ; Dai, Han-Bin ; Liu, Xiao-Juan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a339t-afb54c24dccb0e35c30a9fa62005c5ea421c748ba722c07b399fd59e0bdfae063</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Chemical Fractionation - methods</topic><topic>chlorogenic acid</topic><topic>Chromatography, High Pressure Liquid - methods</topic><topic>correlation</topic><topic>Crataegus</topic><topic>Crataegus - chemistry</topic><topic>epicatechin</topic><topic>food analysis</topic><topic>Fruit - chemistry</topic><topic>fruits</topic><topic>ionic liquids</topic><topic>Ionic Liquids - chemistry</topic><topic>isoquercitrin</topic><topic>Plant Extracts - chemistry</topic><topic>Plant Extracts - isolation & purification</topic><topic>polar compounds</topic><topic>protocatechuic acid</topic><topic>quercetin</topic><topic>surfactants</topic><topic>tandem mass spectrometry</topic><topic>Tandem Mass Spectrometry - methods</topic><topic>ultra-performance liquid chromatography</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hu, Shuai-Shuai</creatorcontrib><creatorcontrib>Yi, Ling</creatorcontrib><creatorcontrib>Li, Xing-Ying</creatorcontrib><creatorcontrib>Cao, Jun</creatorcontrib><creatorcontrib>Ye, Li-Hong</creatorcontrib><creatorcontrib>Cao, Wan</creatorcontrib><creatorcontrib>Da, Jian-Hua</creatorcontrib><creatorcontrib>Dai, Han-Bin</creatorcontrib><creatorcontrib>Liu, Xiao-Juan</creatorcontrib><collection>AGRIS</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Journal of agricultural and food chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hu, Shuai-Shuai</au><au>Yi, Ling</au><au>Li, Xing-Ying</au><au>Cao, Jun</au><au>Ye, Li-Hong</au><au>Cao, Wan</au><au>Da, Jian-Hua</au><au>Dai, Han-Bin</au><au>Liu, Xiao-Juan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Ionic Liquid-Based One-Step Micellar Extraction of Multiclass Polar Compounds from Hawthorn Fruits by Ultrahigh-Performance Liquid Chromatography Coupled with Quadrupole Time-of-Flight Tandem Mass Spectrometry</atitle><jtitle>Journal of agricultural and food chemistry</jtitle><addtitle>J. Agric. Food Chem</addtitle><date>2014-06-11</date><risdate>2014</risdate><volume>62</volume><issue>23</issue><spage>5275</spage><epage>5280</epage><pages>5275-5280</pages><issn>0021-8561</issn><eissn>1520-5118</eissn><abstract>An ionic liquid (IL)-based one-step micellar extraction procedure was developed for the extraction of multiclass polar analytes (protocatechuic acid, chlorogenic acid, epicatechin, hyperoside, isoquercitrin, quercetin) from hawthorn fruits and their determination using ultrahigh-performance liquid chromatography coupled with quadrupole time-of-flight tandem mass spectrometry (UHPLC-Q-TOF/MS). Compared to conventional organic solvent extractions, this newly proposed method was much easier, more sensitive, environmentally friendly, and effective as well. Several important parameters influencing the micellar extraction efficiency are discussed, such as selection of ILs, surfactant concentration, and extraction time. Under the optimal conditions, good linearity was achieved for each analyte with correlation coefficients (r 2) ranging from 0.9934 to 0.9999, and the recovery values ranged from 89.3 to 106% with relative standard deviations lower than 5.5%. Results suggest that the IL-based one-step micellar extraction could be an alternative and promising means in future food analysis.</abstract><cop>United States</cop><pub>American Chemical Society</pub><pmid>24845828</pmid><doi>10.1021/jf501171w</doi><tpages>6</tpages></addata></record> |
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| ispartof | Journal of agricultural and food chemistry, 2014-06, Vol.62 (23), p.5275-5280 |
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| source | MEDLINE; American Chemical Society Journals |
| subjects | Chemical Fractionation - methods chlorogenic acid Chromatography, High Pressure Liquid - methods correlation Crataegus Crataegus - chemistry epicatechin food analysis Fruit - chemistry fruits ionic liquids Ionic Liquids - chemistry isoquercitrin Plant Extracts - chemistry Plant Extracts - isolation & purification polar compounds protocatechuic acid quercetin surfactants tandem mass spectrometry Tandem Mass Spectrometry - methods ultra-performance liquid chromatography |
| title | Ionic Liquid-Based One-Step Micellar Extraction of Multiclass Polar Compounds from Hawthorn Fruits by Ultrahigh-Performance Liquid Chromatography Coupled with Quadrupole Time-of-Flight Tandem Mass Spectrometry |
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