One-pot synthesis of monoclinic ZrO2 nanocrystals under subcritical hydrothermal conditions

•ZrO2 nanocrystals from a ZrO(NO3)2 precursor were synthesized by a one-pot hydrothermal method utilizing subcritical water.•The reaction temperature and time strongly affected the crystalline phase of ZrO2 products.•A single-phase monoclinic ZrO2 product was synthesized at 250°C for the reaction ti...

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Veröffentlicht in:	The Journal of supercritical fluids 2014-01, Vol.85, p.57-61
Hauptverfasser:	Taguchi, Minori, Nakane, Takayuki, Matsushita, Akiyuki, Sakka, Yoshio, Uchikoshi, Tetsuo, Funazukuri, Toshitaka, Naka, Takashi
Format:	Artikel
Sprache:	eng
Schlagworte:	Crystallites Heat treatment Monoclinic ZrO2 Nanocrystals One-pot hydrothermal method Precursors Reactors Subcritical water Synthesis Zirconium Zirconium dioxide
Online-Zugang:	Volltext
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