High-performance liquid chromatographic screening method for mycotoxins using new retention indexes and diode array detection
A reversed-phase high-performance liquid chromatographic (RP-HPLC) screening method for the determination of mycotoxins has been developed. The toxins were characterized by retention indexes and on-line UV spectra produced with a diode array detector (DAD). Retention indexes of mycotoxins exhibiting...
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| Veröffentlicht in: | Archives of environmental contamination and toxicology 1989-05, Vol.18 (3), p.336-348 |
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| creator | Kuronen, P |
| description | A reversed-phase high-performance liquid chromatographic (RP-HPLC) screening method for the determination of mycotoxins has been developed. The toxins were characterized by retention indexes and on-line UV spectra produced with a diode array detector (DAD). Retention indexes of mycotoxins exhibiting a wide range of polarities and chemical structures were determined during linear gradient elution with an acetonitrile/water solvent system. The retention index scale was based on the use of a new homologous series of 1-[4-(2,3-dihydroxypropoxy)phenyl]-1-alkanones (D-compounds) as internal standards. The mycotoxins studied were: five trichothecenes of group A: T-2 toxin (T-2), HT-2 toxin (HT-2), diacetoxyscirpenol (DAS), neosolaniol (NEO), and an isomer of neosolaniol (NEO isomer); three trichothecenes of group B: nivalenol (NIV), deoxynivalenol (DON), and fusarenon-X (FUS-X); four aflatoxins: B1, B2, G1, and G2; and five other mycotoxins: sterigmatocystin (STE), zearalenone (ZEA), ochratoxin A (OCH A), citrinin (CIT), and patulin (PAT). |
| doi_str_mv | 10.1007/BF01062358 |
| format | Article |
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The toxins were characterized by retention indexes and on-line UV spectra produced with a diode array detector (DAD). Retention indexes of mycotoxins exhibiting a wide range of polarities and chemical structures were determined during linear gradient elution with an acetonitrile/water solvent system. The retention index scale was based on the use of a new homologous series of 1-[4-(2,3-dihydroxypropoxy)phenyl]-1-alkanones (D-compounds) as internal standards. The mycotoxins studied were: five trichothecenes of group A: T-2 toxin (T-2), HT-2 toxin (HT-2), diacetoxyscirpenol (DAS), neosolaniol (NEO), and an isomer of neosolaniol (NEO isomer); three trichothecenes of group B: nivalenol (NIV), deoxynivalenol (DON), and fusarenon-X (FUS-X); four aflatoxins: B1, B2, G1, and G2; and five other mycotoxins: sterigmatocystin (STE), zearalenone (ZEA), ochratoxin A (OCH A), citrinin (CIT), and patulin (PAT).</description><subject>Biological and medical sciences</subject><subject>Chemical Phenomena</subject><subject>Chemistry</subject><subject>CHROMATOGRAPHIE</subject><subject>CHROMATOGRAPHY</subject><subject>Chromatography, High Pressure Liquid</subject><subject>CROMATOGRAFIA</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>MICOTOXINAS</subject><subject>Microbiology</subject><subject>Morphology, structure, chemical composition</subject><subject>Mycology</subject><subject>MYCOTOXINE</subject><subject>MYCOTOXINS</subject><subject>Mycotoxins - analysis</subject><subject>Reference Standards</subject><subject>Spectrophotometry, Ultraviolet</subject><issn>0090-4341</issn><issn>1432-0703</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1989</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpF0L9vEzEYxnELgUoaWBiRkDwgBqSD17_ufCNUlCJVYqDMJ8d-nRjd2al9pzYD_zuOEpXJw_PxO3wJecPgEwPoPn-9BgYtF0o_IysmBW-gA_GcrAB6aKSQ7CW5LOUPAONaywtywTsBTMkV-XsTtrtmj9mnPJlokY7hfgmO2l1Ok5nTNpv9LlhabEaMIW7phPMuOVo_0Olg05weQyx0Kcct4gPNOGOcQ4o0RIePWKiJjrqQHFKTszlQV4U9ilfkhTdjwdfnd03urr_dXd00tz-__7j6cttY0bK5EU5qLkFC73spUWrGOymEtZ4rphC93ZhOMmx1qztUZiNwY3rkwnDwSok1-XA6u8_pfsEyD1MoFsfRRExLGZhiumtruDX5eII2p1Iy-mGfw2TyYWAwHFMP_1NX_O58ddlM6J7ouW3d3593U6wZfa55Q3liba-0EryytyfmTRrMNlfy-5fuWd068Q8-do_d</recordid><startdate>19890501</startdate><enddate>19890501</enddate><creator>Kuronen, P</creator><general>Springer-Verlag</general><scope>FBQ</scope><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7T7</scope><scope>7U7</scope><scope>8FD</scope><scope>C1K</scope><scope>FR3</scope><scope>M7N</scope><scope>P64</scope></search><sort><creationdate>19890501</creationdate><title>High-performance liquid chromatographic screening method for mycotoxins using new retention indexes and diode array detection</title><author>Kuronen, P</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c361t-3d48240409f944e48127433ccf2515eefcba741e68687e5ab3eba9e23a20f553</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1989</creationdate><topic>Biological and medical sciences</topic><topic>Chemical Phenomena</topic><topic>Chemistry</topic><topic>CHROMATOGRAPHIE</topic><topic>CHROMATOGRAPHY</topic><topic>Chromatography, High Pressure Liquid</topic><topic>CROMATOGRAFIA</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>MICOTOXINAS</topic><topic>Microbiology</topic><topic>Morphology, structure, chemical composition</topic><topic>Mycology</topic><topic>MYCOTOXINE</topic><topic>MYCOTOXINS</topic><topic>Mycotoxins - analysis</topic><topic>Reference Standards</topic><topic>Spectrophotometry, Ultraviolet</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kuronen, P</creatorcontrib><collection>AGRIS</collection><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Toxicology Abstracts</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Engineering Research Database</collection><collection>Algology Mycology and Protozoology Abstracts (Microbiology C)</collection><collection>Biotechnology and BioEngineering Abstracts</collection><jtitle>Archives of environmental contamination and toxicology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kuronen, P</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>High-performance liquid chromatographic screening method for mycotoxins using new retention indexes and diode array detection</atitle><jtitle>Archives of environmental contamination and toxicology</jtitle><addtitle>Arch Environ Contam Toxicol</addtitle><date>1989-05-01</date><risdate>1989</risdate><volume>18</volume><issue>3</issue><spage>336</spage><epage>348</epage><pages>336-348</pages><issn>0090-4341</issn><eissn>1432-0703</eissn><coden>AECTCV</coden><abstract>A reversed-phase high-performance liquid chromatographic (RP-HPLC) screening method for the determination of mycotoxins has been developed. The toxins were characterized by retention indexes and on-line UV spectra produced with a diode array detector (DAD). Retention indexes of mycotoxins exhibiting a wide range of polarities and chemical structures were determined during linear gradient elution with an acetonitrile/water solvent system. The retention index scale was based on the use of a new homologous series of 1-[4-(2,3-dihydroxypropoxy)phenyl]-1-alkanones (D-compounds) as internal standards. The mycotoxins studied were: five trichothecenes of group A: T-2 toxin (T-2), HT-2 toxin (HT-2), diacetoxyscirpenol (DAS), neosolaniol (NEO), and an isomer of neosolaniol (NEO isomer); three trichothecenes of group B: nivalenol (NIV), deoxynivalenol (DON), and fusarenon-X (FUS-X); four aflatoxins: B1, B2, G1, and G2; and five other mycotoxins: sterigmatocystin (STE), zearalenone (ZEA), ochratoxin A (OCH A), citrinin (CIT), and patulin (PAT).</abstract><cop>Heidelberg</cop><cop>Berlin</cop><cop>New York, NY</cop><pub>Springer-Verlag</pub><pmid>2730154</pmid><doi>10.1007/BF01062358</doi><tpages>13</tpages></addata></record> |
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| ispartof | Archives of environmental contamination and toxicology, 1989-05, Vol.18 (3), p.336-348 |
| issn | 0090-4341 1432-0703 |
| language | eng |
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| source | MEDLINE; SpringerLink Journals - AutoHoldings |
| subjects | Biological and medical sciences Chemical Phenomena Chemistry CHROMATOGRAPHIE CHROMATOGRAPHY Chromatography, High Pressure Liquid CROMATOGRAFIA Fundamental and applied biological sciences. Psychology MICOTOXINAS Microbiology Morphology, structure, chemical composition Mycology MYCOTOXINE MYCOTOXINS Mycotoxins - analysis Reference Standards Spectrophotometry, Ultraviolet |
| title | High-performance liquid chromatographic screening method for mycotoxins using new retention indexes and diode array detection |
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