Dual-frequency ultrasound effect on structure and properties of sweet potato starch

Effects on the structure and properties of sweet potato starch under single frequency ultrasound of 25, 80 kHz and dual‐frequency ultrasound of 25 and 80 kHz were investigated at the same treating conditions else. Dents and pores were found by SEM at the surface of starch with both ultrasounds. Star...

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Veröffentlicht in:Die Stärke 2013-07, Vol.65 (7-8), p.621-627
Hauptverfasser: Zheng, Jie, Li, Qian, Hu, Aijun, Yang, Lin, Lu, Jing, Zhang, Xiaoqinq, Lin, Qiuqian
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container_issue 7-8
container_start_page 621
container_title Die Stärke
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creator Zheng, Jie
Li, Qian
Hu, Aijun
Yang, Lin
Lu, Jing
Zhang, Xiaoqinq
Lin, Qiuqian
description Effects on the structure and properties of sweet potato starch under single frequency ultrasound of 25, 80 kHz and dual‐frequency ultrasound of 25 and 80 kHz were investigated at the same treating conditions else. Dents and pores were found by SEM at the surface of starch with both ultrasounds. Starch–iodine complex analysis showed above ultrasounds destroyed amylopectin and starch chains. FT‐IR indicated that with ultrasonic treatments, the functional groups of starch were not destroyed, but its crystal structure was damaged. As a result, its crystalline index decreased. Brabender curves showed that the peak viscosity of starch with dual‐frequency ultrasound was 14.09% lower than that of the native starch. In addition, the solubility and transmittance of starch increased by ultrasound, and the solubility went up as ultrasonication time was increased. It reached the maximum when the starch was treated for 60 min by dual‐frequency ultrasound, which increased by 2.69% compared to that of native starch. The starch being treated by dual‐frequency ultrasound for 30 min showed maximum transmittance, increasing it by 5.1% compared to the native starch; however, continuously increasing ultrasonic treatment resulted in a decrease of transmittance. Therefore, compared to single frequency ultrasound, dual‐frequency ultrasonic treatment caused more obvious changes to the structure and properties.
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Dents and pores were found by SEM at the surface of starch with both ultrasounds. Starch–iodine complex analysis showed above ultrasounds destroyed amylopectin and starch chains. FT‐IR indicated that with ultrasonic treatments, the functional groups of starch were not destroyed, but its crystal structure was damaged. As a result, its crystalline index decreased. Brabender curves showed that the peak viscosity of starch with dual‐frequency ultrasound was 14.09% lower than that of the native starch. In addition, the solubility and transmittance of starch increased by ultrasound, and the solubility went up as ultrasonication time was increased. It reached the maximum when the starch was treated for 60 min by dual‐frequency ultrasound, which increased by 2.69% compared to that of native starch. The starch being treated by dual‐frequency ultrasound for 30 min showed maximum transmittance, increasing it by 5.1% compared to the native starch; however, continuously increasing ultrasonic treatment resulted in a decrease of transmittance. Therefore, compared to single frequency ultrasound, dual‐frequency ultrasonic treatment caused more obvious changes to the structure and properties.</description><identifier>ISSN: 0038-9056</identifier><identifier>EISSN: 1521-379X</identifier><identifier>DOI: 10.1002/star.201200197</identifier><identifier>CODEN: STRKA6</identifier><language>eng</language><publisher>Weinheim: WILEY-VCH Verlag</publisher><subject>amylopectin ; Applied sciences ; Biological and medical sciences ; Crystal structure ; Dual-frequency ultrasound ; Exact sciences and technology ; Food industries ; Fundamental and applied biological sciences. 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Dents and pores were found by SEM at the surface of starch with both ultrasounds. Starch–iodine complex analysis showed above ultrasounds destroyed amylopectin and starch chains. FT‐IR indicated that with ultrasonic treatments, the functional groups of starch were not destroyed, but its crystal structure was damaged. As a result, its crystalline index decreased. Brabender curves showed that the peak viscosity of starch with dual‐frequency ultrasound was 14.09% lower than that of the native starch. In addition, the solubility and transmittance of starch increased by ultrasound, and the solubility went up as ultrasonication time was increased. It reached the maximum when the starch was treated for 60 min by dual‐frequency ultrasound, which increased by 2.69% compared to that of native starch. 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subjects amylopectin
Applied sciences
Biological and medical sciences
Crystal structure
Dual-frequency ultrasound
Exact sciences and technology
Food industries
Fundamental and applied biological sciences. Psychology
Natural polymers
Physicochemistry of polymers
potato starch
Property
solubility
Starch and polysaccharides
Starch and starchy product industries
Structure
Sweet potato starch
sweet potatoes
transmittance
Ultrasonic imaging
ultrasonic treatment
ultrasonics
viscosity
title Dual-frequency ultrasound effect on structure and properties of sweet potato starch
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