GC models for separation optimization in pressure-tunable tandem capillary columns operated isothermally
In the previous part of this study, a significant improvement of the fundamental relationships that control GC resolution in a pressure‐tunable assembly operating in isothermal conditions inside a single oven was made. A theoretical approach for the correct choice of the working temperature was prop...
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Veröffentlicht in: | Journal of separation science 2014-02, Vol.37 (4), p.412-418 |
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Hauptverfasser: | , |
Format: | Artikel |
Sprache: | eng |
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Online-Zugang: | Volltext |
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Zusammenfassung: | In the previous part of this study, a significant improvement of the fundamental relationships that control GC resolution in a pressure‐tunable assembly operating in isothermal conditions inside a single oven was made. A theoretical approach for the correct choice of the working temperature was proposed for the first time. In this second part of our report, a new interfacing device has been proposed for a rapid and reliable alignment of the two columns at the midpoint junction. Moreover, the results of a series of experimental tests have confirmed the validity of the proposed mathematical models. |
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ISSN: | 1615-9306 1615-9314 |
DOI: | 10.1002/jssc.201301045 |