Biodiesel fuel production from waste cooking oil by the inclusion complex of heteropoly acid with bridged bis-cyclodextrin
•CsPW/B is the inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin.•CsPW/B is used as a catalyst for the transesterification of waste cooking oil.•The conversion rate of waste cooking oil is up to 94.2%.•The yield of fatty acid methyl esters reaches 96.9% based on the biodiesel produ...
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| Veröffentlicht in: | Bioresource technology 2013-10, Vol.146, p.785-788 |
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| creator | Zou, Changjun Zhao, Pinwen Shi, Lihong Huang, Shaobing Luo, Pingya |
| description | •CsPW/B is the inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin.•CsPW/B is used as a catalyst for the transesterification of waste cooking oil.•The conversion rate of waste cooking oil is up to 94.2%.•The yield of fatty acid methyl esters reaches 96.9% based on the biodiesel product.•The physical properties of produced biodiesel satisfy ASTM D6751 standards.
The inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin (CsPW/B) is prepared as a highly efficient catalyst for the direct production of biodiesel via the transesterification of waste cooking oil. CsPW/B is characterized by X-ray diffraction, and the biodiesel is analyzed by Gas Chromatography–Mass Spectrometer. The conversion rate of waste cooking oil is up to 94.2% under the optimum experimental conditions that are methanol/oil molar ratio of 9:1, catalyst dosage of 3wt%, temperature of 65°C and reaction time of 180min. The physical properties of biodiesel sample satisfy the requirement of ASTM D6751 standards. The novel CsPW/B catalyst used for the transesterification can lead to 96.9% fatty acid methyl esters and 86.5% of the biodiesel product can serve as the ideal substitute for diesel fuel, indicating its excellent potential application in biodiesel production. |
| doi_str_mv | 10.1016/j.biortech.2013.07.149 |
| format | Article |
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The inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin (CsPW/B) is prepared as a highly efficient catalyst for the direct production of biodiesel via the transesterification of waste cooking oil. CsPW/B is characterized by X-ray diffraction, and the biodiesel is analyzed by Gas Chromatography–Mass Spectrometer. The conversion rate of waste cooking oil is up to 94.2% under the optimum experimental conditions that are methanol/oil molar ratio of 9:1, catalyst dosage of 3wt%, temperature of 65°C and reaction time of 180min. The physical properties of biodiesel sample satisfy the requirement of ASTM D6751 standards. The novel CsPW/B catalyst used for the transesterification can lead to 96.9% fatty acid methyl esters and 86.5% of the biodiesel product can serve as the ideal substitute for diesel fuel, indicating its excellent potential application in biodiesel production.</description><identifier>ISSN: 0960-8524</identifier><identifier>EISSN: 1873-2976</identifier><identifier>DOI: 10.1016/j.biortech.2013.07.149</identifier><identifier>PMID: 23972395</identifier><language>eng</language><publisher>Kidlington: Elsevier Ltd</publisher><subject>Biodiesel ; Biofuel production ; Biofuels - analysis ; Biological and medical sciences ; Biotechnology ; Bridged bis-cyclodextrin ; Catalysis ; Catalysts ; Cooking ; Cyclodextrins - chemistry ; Energy ; Esterification ; Esters - chemistry ; Fatty Acids - chemistry ; Food processing ; Fundamental and applied biological sciences. Psychology ; Gas Chromatography-Mass Spectrometry ; Glucose - chemistry ; Heating ; Heteropoly acid ; Inclusion complexes ; Industrial applications and implications. Economical aspects ; Industry ; Methanol - chemistry ; Oligosaccharides - chemistry ; Plant Oils - metabolism ; Temperature ; Transesterification ; Waste cooking oil ; Waste Disposal, Fluid ; Waste Products - analysis ; Wastes ; X-Ray Diffraction</subject><ispartof>Bioresource technology, 2013-10, Vol.146, p.785-788</ispartof><rights>2013 Elsevier Ltd</rights><rights>2014 INIST-CNRS</rights><rights>Copyright © 2013 Elsevier Ltd. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c431t-d3b44ed3cfe78b9e5e38216d41bcff41c082dcc4c876e5067bd458b526a81f093</citedby><cites>FETCH-LOGICAL-c431t-d3b44ed3cfe78b9e5e38216d41bcff41c082dcc4c876e5067bd458b526a81f093</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.biortech.2013.07.149$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3550,27924,27925,45995</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=27762345$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/23972395$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Zou, Changjun</creatorcontrib><creatorcontrib>Zhao, Pinwen</creatorcontrib><creatorcontrib>Shi, Lihong</creatorcontrib><creatorcontrib>Huang, Shaobing</creatorcontrib><creatorcontrib>Luo, Pingya</creatorcontrib><title>Biodiesel fuel production from waste cooking oil by the inclusion complex of heteropoly acid with bridged bis-cyclodextrin</title><title>Bioresource technology</title><addtitle>Bioresour Technol</addtitle><description>•CsPW/B is the inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin.•CsPW/B is used as a catalyst for the transesterification of waste cooking oil.•The conversion rate of waste cooking oil is up to 94.2%.•The yield of fatty acid methyl esters reaches 96.9% based on the biodiesel product.•The physical properties of produced biodiesel satisfy ASTM D6751 standards.
The inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin (CsPW/B) is prepared as a highly efficient catalyst for the direct production of biodiesel via the transesterification of waste cooking oil. CsPW/B is characterized by X-ray diffraction, and the biodiesel is analyzed by Gas Chromatography–Mass Spectrometer. The conversion rate of waste cooking oil is up to 94.2% under the optimum experimental conditions that are methanol/oil molar ratio of 9:1, catalyst dosage of 3wt%, temperature of 65°C and reaction time of 180min. The physical properties of biodiesel sample satisfy the requirement of ASTM D6751 standards. The novel CsPW/B catalyst used for the transesterification can lead to 96.9% fatty acid methyl esters and 86.5% of the biodiesel product can serve as the ideal substitute for diesel fuel, indicating its excellent potential application in biodiesel production.</description><subject>Biodiesel</subject><subject>Biofuel production</subject><subject>Biofuels - analysis</subject><subject>Biological and medical sciences</subject><subject>Biotechnology</subject><subject>Bridged bis-cyclodextrin</subject><subject>Catalysis</subject><subject>Catalysts</subject><subject>Cooking</subject><subject>Cyclodextrins - chemistry</subject><subject>Energy</subject><subject>Esterification</subject><subject>Esters - chemistry</subject><subject>Fatty Acids - chemistry</subject><subject>Food processing</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Gas Chromatography-Mass Spectrometry</subject><subject>Glucose - chemistry</subject><subject>Heating</subject><subject>Heteropoly acid</subject><subject>Inclusion complexes</subject><subject>Industrial applications and implications. Economical aspects</subject><subject>Industry</subject><subject>Methanol - chemistry</subject><subject>Oligosaccharides - chemistry</subject><subject>Plant Oils - metabolism</subject><subject>Temperature</subject><subject>Transesterification</subject><subject>Waste cooking oil</subject><subject>Waste Disposal, Fluid</subject><subject>Waste Products - analysis</subject><subject>Wastes</subject><subject>X-Ray Diffraction</subject><issn>0960-8524</issn><issn>1873-2976</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkUFv1DAQhS0EokvhL1S-IHFJsGMndm5A1QJSJS5wtpLxuOsliRfbabv8ehJ2C8cebF--N37zHiEXnJWc8eb9rux9iBlhW1aMi5Kpksv2GdlwrURRtap5TjasbVih60qekVcp7RhjgqvqJTmrRKuWU2_I708-WI8JB-rm5drHYGfIPkzUxTDS-y5lpBDCTz_d0uAH2h9o3iL1EwxzWjkI437ABxoc3WLGGPZhONAOvKX3Pm9pH729RUt7nwo4wBAsPuTop9fkheuGhG9O7zn5cX31_fJLcfPt89fLjzcFSMFzYUUvJVoBDpXuW6xR6Io3VvIenJMcmK4sgAStGqxZo3ora93XVdNp7lgrzsm749xlt18zpmxGnwCHoZswzMnwmjGlhV7SeRJdHDVLcH-nNkcUYkgpojP76McuHgxnZq3I7MxjRWatyDC16FfhxemPuR_R_pM9drIAb09Al6AbXOwm8Ok_p9RiQa7chyOHS3h3HqNJ4HECtD4iZGODf8rLH3GRtQc</recordid><startdate>20131001</startdate><enddate>20131001</enddate><creator>Zou, Changjun</creator><creator>Zhao, Pinwen</creator><creator>Shi, Lihong</creator><creator>Huang, Shaobing</creator><creator>Luo, Pingya</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7SU</scope><scope>7TB</scope><scope>8FD</scope><scope>C1K</scope><scope>FR3</scope><scope>KR7</scope></search><sort><creationdate>20131001</creationdate><title>Biodiesel fuel production from waste cooking oil by the inclusion complex of heteropoly acid with bridged bis-cyclodextrin</title><author>Zou, Changjun ; Zhao, Pinwen ; Shi, Lihong ; Huang, Shaobing ; Luo, Pingya</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c431t-d3b44ed3cfe78b9e5e38216d41bcff41c082dcc4c876e5067bd458b526a81f093</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Biodiesel</topic><topic>Biofuel production</topic><topic>Biofuels - analysis</topic><topic>Biological and medical sciences</topic><topic>Biotechnology</topic><topic>Bridged bis-cyclodextrin</topic><topic>Catalysis</topic><topic>Catalysts</topic><topic>Cooking</topic><topic>Cyclodextrins - chemistry</topic><topic>Energy</topic><topic>Esterification</topic><topic>Esters - chemistry</topic><topic>Fatty Acids - chemistry</topic><topic>Food processing</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Gas Chromatography-Mass Spectrometry</topic><topic>Glucose - chemistry</topic><topic>Heating</topic><topic>Heteropoly acid</topic><topic>Inclusion complexes</topic><topic>Industrial applications and implications. Economical aspects</topic><topic>Industry</topic><topic>Methanol - chemistry</topic><topic>Oligosaccharides - chemistry</topic><topic>Plant Oils - metabolism</topic><topic>Temperature</topic><topic>Transesterification</topic><topic>Waste cooking oil</topic><topic>Waste Disposal, Fluid</topic><topic>Waste Products - analysis</topic><topic>Wastes</topic><topic>X-Ray Diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zou, Changjun</creatorcontrib><creatorcontrib>Zhao, Pinwen</creatorcontrib><creatorcontrib>Shi, Lihong</creatorcontrib><creatorcontrib>Huang, Shaobing</creatorcontrib><creatorcontrib>Luo, Pingya</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Environmental Engineering Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Engineering Research Database</collection><collection>Civil Engineering Abstracts</collection><jtitle>Bioresource technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zou, Changjun</au><au>Zhao, Pinwen</au><au>Shi, Lihong</au><au>Huang, Shaobing</au><au>Luo, Pingya</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Biodiesel fuel production from waste cooking oil by the inclusion complex of heteropoly acid with bridged bis-cyclodextrin</atitle><jtitle>Bioresource technology</jtitle><addtitle>Bioresour Technol</addtitle><date>2013-10-01</date><risdate>2013</risdate><volume>146</volume><spage>785</spage><epage>788</epage><pages>785-788</pages><issn>0960-8524</issn><eissn>1873-2976</eissn><abstract>•CsPW/B is the inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin.•CsPW/B is used as a catalyst for the transesterification of waste cooking oil.•The conversion rate of waste cooking oil is up to 94.2%.•The yield of fatty acid methyl esters reaches 96.9% based on the biodiesel product.•The physical properties of produced biodiesel satisfy ASTM D6751 standards.
The inclusion complex of Cs2.5H0.5PW12O40 with bridged bis-cyclodextrin (CsPW/B) is prepared as a highly efficient catalyst for the direct production of biodiesel via the transesterification of waste cooking oil. CsPW/B is characterized by X-ray diffraction, and the biodiesel is analyzed by Gas Chromatography–Mass Spectrometer. The conversion rate of waste cooking oil is up to 94.2% under the optimum experimental conditions that are methanol/oil molar ratio of 9:1, catalyst dosage of 3wt%, temperature of 65°C and reaction time of 180min. The physical properties of biodiesel sample satisfy the requirement of ASTM D6751 standards. The novel CsPW/B catalyst used for the transesterification can lead to 96.9% fatty acid methyl esters and 86.5% of the biodiesel product can serve as the ideal substitute for diesel fuel, indicating its excellent potential application in biodiesel production.</abstract><cop>Kidlington</cop><pub>Elsevier Ltd</pub><pmid>23972395</pmid><doi>10.1016/j.biortech.2013.07.149</doi><tpages>4</tpages></addata></record> |
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| ispartof | Bioresource technology, 2013-10, Vol.146, p.785-788 |
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| subjects | Biodiesel Biofuel production Biofuels - analysis Biological and medical sciences Biotechnology Bridged bis-cyclodextrin Catalysis Catalysts Cooking Cyclodextrins - chemistry Energy Esterification Esters - chemistry Fatty Acids - chemistry Food processing Fundamental and applied biological sciences. Psychology Gas Chromatography-Mass Spectrometry Glucose - chemistry Heating Heteropoly acid Inclusion complexes Industrial applications and implications. Economical aspects Industry Methanol - chemistry Oligosaccharides - chemistry Plant Oils - metabolism Temperature Transesterification Waste cooking oil Waste Disposal, Fluid Waste Products - analysis Wastes X-Ray Diffraction |
| title | Biodiesel fuel production from waste cooking oil by the inclusion complex of heteropoly acid with bridged bis-cyclodextrin |
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