Synthesis of Novel Amide Molecular Tweezers under Solvent-Free Conditions Using Microwave Irradiation

Synthesis of Novel Amide Molecular Tweezers under Solvent-Free Conditions Using Microwave Irradiation

Twelve novel amide type molecular tweezer anion receptors based on phenyl-1,4-dioxyacetic acid have been synthesised using microwave irradiation. Their structures were established by 1H NMR, IR, MS spectra and elemental analysis. Their binding properties were examined by UV-Vis spectra titration. Th...

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Veröffentlicht in:Journal of chemical research 2011-10, Vol.35 (10), p.587-591
Hauptverfasser: Zeng, Bitao, Zhou, Lijun, Li, Xiangbiao, Zhao, Xianming, Zhao, Zhigang, Deng, Mei
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Amides
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container_issue 10
container_start_page 587
container_title Journal of chemical research
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creator Zeng, Bitao
Zhou, Lijun
Li, Xiangbiao
Zhao, Xianming
Zhao, Zhigang
Deng, Mei
description Twelve novel amide type molecular tweezer anion receptors based on phenyl-1,4-dioxyacetic acid have been synthesised using microwave irradiation. Their structures were established by 1H NMR, IR, MS spectra and elemental analysis. Their binding properties were examined by UV-Vis spectra titration. The preliminary results indicate that these molecular tweezers show good recognition properties for Cl-, Br-, I-, CH3COO-.
doi_str_mv 10.3184/174751911X13178094714324
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title Synthesis of Novel Amide Molecular Tweezers under Solvent-Free Conditions Using Microwave Irradiation
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